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排序方式: 共有163条查询结果,搜索用时 15 毫秒
1.
现场抽样调查中,由于测量误差的存在,使得所测变量实测值的方差增大,通过增加每个体的测量次数可以控制测量误差,但这样每个体调查费用增大。本文对测量信度R,每个体测量次数m与相应所需的样本含量nm、调查费用Tn的关系进行了探讨,并介绍了如何根据R,及每个体测量费用占其总费用构成比C,确定最佳测量次数m值,以达到最佳控制调查费用的目的,这对我们在大型现场调查中进行经济效益分析具有重大的理论指导意义。 相似文献
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MingZhuLIU ShengYiZHANG YuHuaSHEN MingLiangZHANG 《中国化学快报》2004,15(10):1249-1252
Selenium nanoparticles were prepared by a reverse microemulsion system. Sodium selenosulfate was used as selenium source. The results showed that hydrochloric acid concentration and reaction temperature had great influence on the morphology of products. The crystalline selenium nanowires and amorphous selenium nanorods were obtained in given condition. 相似文献
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Fei Ye Xiaoyan Qiao Anhui Gui Panpan Liu Shengpeng Wang Xueping Wang Jin Teng Lin Zheng Lin Feng Hanshan Han Binghua Zhang Xun Chen Zhiming Gao Shiwei Gao Pengcheng Zheng 《Molecules (Basel, Switzerland)》2022,27(13)
Roasting is crucial for producing Yuan An yellow tea (YAYT) as it substantially affects sensory quality. However, the effect of roasting time on YAYT flavor quality is not clear. To investigate the effect of roasting time on the sensory qualities, chemical components, odor profiles, and metabolic profile of YAYTs produced with 13 min roasting, 16 min roasting, 19 min roasting, 22 min roasting, and 25 min roasting were determined. The YAYTs roasted for 22 min got higher sensory scores and better chemical qualities, such as the content of gallocatechin (GC), gallocatechin gallate (GCG), free amino acids, solutable sugar, meanwhile the lightness decreased, the hue of tea brew color (b) increased, which meant the tea brew got darker and yellower. YAYTs roasted for 22 min also increased the contents of key odorants, such as benzaldehyde, nonanal, β-cyclocitral, linalool, nerol, α-cedrol, β-ionone, limonene, 2-methylfuran, indole, and longiborneol. Moreover, non-targeted metabolomics identified up to 14 differentially expressed metabolites through pair-wise comparisons, such as flavonoids, phenolic acids, sucrose, and critical metabolites, which were the main components corresponding to YAYT roasted for 22 min. In summary, the current results provide scientific guidance for the production of high quality YAYT. 相似文献
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Wei Sun Yuanyuan Zhang Anhui Hu Yongxi Lu Fan Shi Bingxin Lei Zhenfan Sun 《Electroanalysis》2013,25(6):1417-1424
In this work a partially reduced graphene oxide (p‐RGO) modified carbon ionic liquid electrode (CILE) was prepared as the platform to fabricate an electrochemical DNA sensor, which was used for the sensitive detection of target ssDNA sequence related to transgenic soybean A2704‐12 sequence. The CILE was fabricated by using 1‐butylpyridinium hexafluorophosphate as the binder and then p‐RGO was deposited on the surface of CILE by controlling the electroreduction conditions. NH2 modified ssDNA probe sequences were immobilized on the electrode surface via covalent bonds between the unreduced oxygen groups on the p‐RGO surface and the amine group at the 5′‐end of ssDNA, which was denoted as ssDNA/p‐RGO/CILE and further used to hybridize with the target ssDNA sequence. Methylene blue (MB) was used as electrochemical indicator to monitor the DNA hybridization. The reduction peak current of MB after hybridization was proportional to the concentration of target A2704‐12 ssDNA sequences in the range from 1.0×10?12 to 1.0×10?6 mol/L with a detection limit of 2.9×10?13 mol/L (3σ). The electrochemical DNA biosensor was further used for the detection of PCR products of transgenic soybean with satisfactory results. 相似文献
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本文讨论了自适应光学中非等晕域对补偿效果的影响,提出了一种减小非等晕性误差的新方法—位相梯度法。分析结果表明,该方法可显著增大有效校正的角范围,使非等晕性误差的影响大大减小。我们预期位相梯度法有望解决自适应光学中信标的非等晕性问题。 相似文献
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LeYuWANG HongQiCHEN LingLI LingDONG TingTingXIA LunWANG 《中国化学快报》2004,15(3):319-321
Functionalized nano-PbS has been prepared and characterized. The functionalized nanoparticles have good dispersibility in water. Reaction of functionalized nano-PbS with γ-globulin (γ-IgG) results an enhanced resonance light scattering (RLS) around 385nm.However, when the content of HSA is lower than 0.5μg/ml^-1 the RLS enhancement is very weak and is nonlinear to concentration of HSA. Based on these results, a new direct quantitative determination method for γ-globulin in blood serum samples without separation is established.Under optimal conditions, the enhanced RLS intensity is in proportion to the γ-IgG concentration in the range 10-500ng/mL. The limit of detection is 2.75ng/mL. This method is proved to be very sensitive, rapid, simple and selective for detection of γ-IgG in blood serum. 相似文献
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Chen Li Wendong Wang Congying Xu Yuanxu Liu Bo He Chusheng Chen .CAS Key Laboratory of Materials for Energy Conversion University of Science Technology of China Hefei Anhui China 《天然气化学杂志》2011,(4):345-349
The double perovskite oxides Sr2Mg1-xF exMoO6-δ were investigated as catalysts for the methane oxidation.The structural properties of catalysts were characterized in detail by X-ray diffraction,X-ray photoelectron spectroscopy and X-ray absorption spectroscopy.The catalytic property was strongly influenced by the Fe substitution.The relation between catalytic performance and the degree of Fe substitution was examined with regard to the structure and surface characteristics of the mixed oxides.The Fe-containing catalysts exhibited higher activity attributable to the possible(Fe2+,Mo6+) and (Fe3+,Mo5+)valency pairs,and the highest activity was observed for Sr2Mg0.2Fe0.8MoO6-δ.The enhancement of the catalytic activity may be correlated with the Fe-relating surface lattice oxygen species and was discussed in view of the presence of oxygen vacancies. 相似文献