Thermal buckling analysis of truss-core sandwich plates

Truss-core sandwich plates have received much attention in virtue of the high values of strength-to-weight and stifness-to-weight as well as the great ability of impulseresistance recently. It is necessary to study the stability of sandwich panels under the influence of the thermal load. However, the sandwich plates are such complex threedimensional(3D) systems that direct analytical solutions do not exist, and the finite element method(FEM) cannot represent the relationship between structural parameters and mechanical properties well. In this paper, an equivalent homogeneous continuous plate is idealized by obtaining the efective bending and transverse shear stifness based on the characteristics of periodically distributed unit cells. The first order shear deformation theory for plates is used to derive the stability equation. The buckling temperature of a simply supported sandwich plate is given and verified by the FEM. The efect of related parameters on mechanical properties is investigated. The geometric parameters of the unit cell are optimized to attain the maximum buckling temperature. It is shown that the optimized sandwich plate can improve the resistance to thermal buckling significantly.     

Vibration analysis of foam plates based on cell volume distribution

In this paper, vibration analysis of irregular-closed-cell foam plates is per-formed. A cell volume distribution coefficient is introduced to modify the original Gibson-Ashby equations of effective Young’s modulus of foam materials. A Burr distribution is imported to describe the cell volume distribution situation. Three Burr distribution pa-rameters are obtained and related to the cell volume range and the diversity. Based on the plate theory and the effective modulus theory, the natural frequency of foam plates is calculated with the change of the cell volume distribution parameters. The relationship between the frequencies and the cell volumes are derived. The scale factor of the average cell size is introduced and proved to be an important factor to the performance of the foam plate. The result is shown by the existing theory of size effects. It is determined that the cell volume distribution has an impact on the natural frequency of the plate structure based on the cell volume range, the diversity, and the average size, and the impact can lead to optimization of the synthesis procedure.     

高速逆流色谱分离纯化EGCG3"Me的研究

首次采用高速逆流色谱法对经自制聚酰胺初步分离的表没食子儿茶素-3-(3″-O-甲基)没食子酸酯( EGCG3"Me)样品中的EGCG3"Me单体进行分离纯化.结果表明,选择水-甲醇-乙酸乙酯-正己烷(体积比5:2:9:1)为高速逆流色谱分离的两相溶剂系统,上相为固定相,下相为流动相,在主机转速700 r／min、流速2.0 mL/min、检测波长254 nm的条件下,可对EC CG3"Me实现良好分离.经高效液相色谱检测,分离纯化后的EC CG3"Me纯度可达90%以上,产物的收率为76.53%.     

基于孔洞分布理论的多孔材料板振动分析

主要研究了不规则几何结构多孔材料制备的板材的振动分析．基于Gibson-Ashby等效模量计算,引入了分布因子加以改进原有的理论．对于材料的孔洞分布情况,提出了Burr分布的概率密度拟合,获得了Burr分布的3个自变量参数并用实际的孔洞几何参数进行了比对与描述．基于平板振动理论和等效模量理论,计算出了随着孔洞分布情况变化下的平板固有振动频率,并分析了孔洞尺寸与频率间的关系．之后引入了尺度因子来量化描述平均孔洞尺寸对多孔平板的频率影响．结论证明了改进的等效理论能够有效地体现孔洞的分布对平板力学性能的改变,论述了孔洞尺寸范围,孔洞离散度以及平均孔洞尺寸对多孔方板结构固有频率的影响．这种影响将会对多孔材料结构的优化设计起指导作用．     

高速逆流色谱分离纯化EGCG3"Me的研究

首次采用高速逆流色谱法对经自制聚酰胺初步分离的表没食子儿茶素-3-(3″-O-甲基)没食子酸酯( EGCG3"Me)样品中的EGCG3"Me单体进行分离纯化.结果表明,选择水-甲醇-乙酸乙酯-正己烷(体积比5:2:9:1)为高速逆流色谱分离的两相溶剂系统,上相为固定相,下相为流动相,在主机转速700 r／min、流速2...     

疏水性磁性微球的制备及对盐藻的吸附研究

采用疏水性材料制备微米级磁性微球,并应用于对盐藻的吸附分离研究,考察了pH值,吸附作用时间,NaCl浓度以及磁性微球添加量对盐藻吸附的影响.结果显示磁性微球对盐藻的吸附受溶液的离子强度影响较大;pH值在一定范围内对盐藻的吸附有较大影响;延长吸附作用时间和加大磁性微球的添加量可以增加对盐藻的吸附量.通过调节pH和施加机械搅拌,磁性微球上吸附的盐藻可以很好被洗脱下来,磁性微球可以多次重复使用.