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调查问卷中含缺失数据的等级变量的补缺方法 总被引:1,自引:0,他引:1
讨论了调查问卷中等级变量缺失数据的补缺问题.基于多元统计学理论,并结合总体趋势和个体偏差,提出一种新的补缺方法,方法使得补缺值更加准确、真实,并且将此方法扩展到变量等级数不相等的调查问卷之中. 相似文献
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基于氟钛配合物的原位水解以及硝酸镧电位滴定法建立了测定钛合金化铣腐蚀溶液中总氟化物浓度的新方法。在六次甲基四胺(HMTA)缓冲溶液中,氟钛配合物发生原位水解并释放出游离氟离子,以氟离子选择电极(F-ISE)为指示电极进行测定。对影响测定的各项参数(如p H值、HMTA溶液用量、钛离子浓度等)做了条件实验并予以优化。实验结果表明Ti(Ⅳ)浓度在0~20 g/L范围内对于氟离子测定无干扰,方法的相对标准偏差(RSDs,n=6)在0.27%~0.62%之间,加标回收率在99.5%~101.1%之间。此外,本文对氟钛配合物原位水解反应的机理也进行了探讨,溶液中氟钛配合物的主要存在形式为TiF_6~(2-),适宜的酸度是水解反应进行的必要条件,HMTA作为缓冲溶液为水解反应持续进行提供恒定的p H环境,La(NO_3)_3作为氟清除剂降低游离氟离子浓度促进水解反应的进行,伴随滴定过程氟钛配合物发生完全水解。 相似文献
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移取铬酸阳极化溶液5.00 mL置于150 mL烧杯中,加入硝酸(1+1)溶液10 mL,100g·L~(-1)抗坏血酸溶液10.0mL,摇匀,使Cr~(6+)完全还原为Cr~(3+)以消除铬酸的干扰,加水至体积为60mL,在40~50r·min~(-1)的搅拌速率下,以0.010mol·L~(-1)硝酸银标准溶液作为滴定剂,采用自动电位滴定法测定溶液中的氯离子。采用该方法分析氯离子质量浓度为0.200,0.500,1.00g·L~(-1)的铬酸阳极化溶液以及3批生产线实际样品,测定值的相对标准偏差(n=6)在0.51%~3.0%之间。针对3批生产线实际样品进行加标回收试验,回收率在97.0%~102%之间。 相似文献
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研究由三个方程耦合的非线性Schr?dinger方程组,它们源于非线性光学和Bose-Einstein凝聚.考虑了两种类型:含有周期位势的方程组和含有势阱位势的方程组.借助于广义的Nehari流形以及精细的能量估计,证明了当相互作用位势适当小时,这两类非线性Schr?dinger方程组存在正的基态. 相似文献
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We investigate the existence and stability of different families of spatial solitons in optical waveguide arrays whose amplitudes obey a disordered distribution. The competition between focusing nonlinearity and linearly disordered refractive index modulation results in the formation of spatial localized nonlinear states. Solitons originating from Anderson modes with few nodes are robust during propagation. While multi-peaked solitons with in-phase neighboring components are completely unstable, multipole-mode solitons whose neighboring components are out-of-phase can propagate stably in wide parameter regions provided that their power exceeds a critical value. Our findings, thus, provide the first example of stable higher-order nonlinear states in disordered systems. 相似文献
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ADC border effect and suppression of quantization error in the digital dynamic measurement 下载免费PDF全文
The digital measurement and processing is an important direction in the measurement and control field. The quantization error widely existing in the digital processing is always the decisive factor that restricts the development and applications of the digital technology. In this paper, we find that the stability of the digital quantization system is obviously better than the quantization resolution. The application of a border effect in the digital quantization can greatly improve the accuracy of digital processing. Its effective precision has nothing to do with the number of quantization bits, which is only related to the stability of the quantization system. The high precision measurement results obtained in the low level quantization system with high sampling rate have an important application value for the progress in the digital measurement and processing field. 相似文献