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采用气相色谱法测定碳酸甘油酯粗产品中碳酸甘油酯和残余甘油的含量。选择HP1701毛细管柱,程序升温及四甘醇内标物作为色谱条件,在此条件下碳酸甘油酯和残余甘油能很好地分离。碳酸甘油酯和甘油的线性范围分别为23.30~116.6 g.L-1和3.70~18.40 g.L-1。方法的回收率在99.1%~100.9%之间,相对标准偏差(n=6)在0.61%~1.93%之间。 相似文献
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There are two general methods in radiometric calibration of detectors, one is based on radiation sources and the other based on detectors. Because the two methods need to establish a primary standard of high precision and a transfer chain, precision of the standard will be reduced by extension of the chain. A new calibration method of detectors can be realized by using correlated photons generated in spontaneous parametric down-conversion (SPDC) effect of nonlinear crystal, without needing transfer chain. Using 351.1-nm output of a tunable laser to pump β-barium borate (BBO) crystal, an absolute calibration experimental system of single photon detectors based on correlated photons is performed. The quantum efficiency of photomultiplier (PMT) at 702.2 nm is measured by the setup. Advantages of this method over traditional methods are also pointed out by comparison. 相似文献
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GeTe基稀磁半导体材料因具有可独立调控载流子浓度和磁性离子浓度的特性而受到广泛关注.本文利用脉冲激光沉积技术制备了该体系的单晶外延薄膜,并通过高价态Bi元素部分取代Ge元素的方法实现了材料中载流子类型从空穴向电子的转变,即制备出N型GeTe基稀磁半导体.测量结果表明,无论是室温还是低温下的Hall电阻曲线皆呈现负斜率,说明体系中载流子是电子;并且当Bi掺杂量达到32%时,电子浓度为10~(21)/cm~3.变温输运性质的测量证明体系的输运行为呈现半导体特征.通过测量低温10 K下的绝热磁化曲线,在高Bi掺杂体系中观测到了明显的铁磁行为,而低于32%Bi掺杂量的体系中未观察到.这一结果说明,高掺杂Bi的替代导致载流子浓度的增加,促进了载流子传递Ruderman-Kittel-Kasuya-Yoshida相互作用,使得分散的Fe-Fe之间产生磁耦合作用,进而形成铁磁有序态. 相似文献
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一、问题的提出
新课标人教版的数学选修2-3课本的第二章是随机变量及其分布.其中第二节是:事件的相互独立.事件的相互独立在老教材中就有,只是教材的引入和定义均不同. 相似文献
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