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V. Naveen Kumar P. Someshwar P. Narsimha Reddy Y. Thirupathi Reddy B. Rajitha 《Journal of heterocyclic chemistry》2005,42(5):1017-1019
The condensation reaction of aldehydes, β‐ketoesters and urea/thiourea in presence of a catalytic amount of CuPy2Cl2 complex proceeded under very mild reaction conditions in high yield (80‐90%). 相似文献
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Ravibabu Velpula Rajitha Deshineni Rajitha Gali Rajitha Bavantula 《Research on Chemical Intermediates》2016,42(3):1729-1740
A series of novel 1-thiazolyl-5-coumarin-3-yl-pyrazole derivatives (4a–l) were synthesized via one-pot multicomponent reaction of 5-substituted salicylaldehydes (1a–c), 4-hydroxy-6-methyl-2H-pyran-2-one (2) and 2-hydrazinyl-4-arylthiazoles (3a–d) in acetonitrile using a catalytic amount of piperidine under reflux conditions. This multicomponent approach has advantages such as reduced reaction time and a high product yield percentage when compared with corresponding multistep approaches. All the synthesized compounds were evaluated for their cytotoxic activity against Hep G2 (hepatocellular liver carcinoma) and MCF-7 (breast cancer) cell lines and compared with the standard drug Doxorubicin. Among all the compounds, compounds 4d against Hep G2, 4k against MCF-7 and 4e against both Hep G2 & MCF-7 showed excellent cytotoxic activity. 相似文献
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M. Amaravathi B. Rajitha M. Kanakalingeswara Rao P. Sitadevi 《Journal of heterocyclic chemistry》2007,44(4):821-825
meso‐Tetrakis(4‐chlorocoumarin‐3‐yl)porphyrins were prepared by condensation of corresponding 4‐chlorocoumarin‐3‐carboxaldehydes and pyrrole in the presence of trifluoro acetic acid (TFA) in dichloromethane followed by oxidation with 2,3‐dichloro‐5,6‐dicyano‐1,4‐benzoquinone (DDQ). These porphyrins exhibited the atropisomerism due to ortho substituent of meso aryl groups. The atropisomers of meso‐tetrakis(4‐chloro‐6‐methylcoumarin‐3‐yl)porphyrin were separated and identified by 1H‐nmr spectra. Zinc complexes of these porphyrins were synthesized and characterized by ms, 1H nmr, ir and uv‐vis spectra. 相似文献
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Synthesis of Novel Fused Thiazolo[3,2‐a]pyrimidin‐3‐ols and Evaluation for their Antibacterial Activity 下载免费PDF全文
Ravibabu Velpula Janardhan Banothu Rajitha Gali Rajitha Bavantula 《Journal of heterocyclic chemistry》2016,53(1):51-55
A series of novel fused thiazolo[3,2‐a]pyrimidin‐3‐ol derivatives have been synthesized by reaction of fused pyrimidine‐thiones with 4‐substituted phenacyl bromide/3(2‐bromoacetyl)coumarin in refluxing acetic acid with good yields. All the synthesized compounds were confirmed by spectral studies and screened for their in vitro antibacterial activity against Staphylococcus aureus, Bacillus thuringiensis (Gram positive), Escherichia coli, and Klebsiella pneumoniae (Gram negative) bacterial strains. Activity results revealed that all the compounds were weak to good active against the tested bacterial strains on comparing with the standard drug gentamicin. 相似文献
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Xanthan sulfuric acid is an efficient solid acid catalyst for the preparation of 2‐aryl benzimidazoles in excellent yields. This method is applicable for the reaction of benzo[c][1,2,5]thiadiazole‐4,5‐diamine with aldehydes by simple physical grinding at room temperature. The salient features of the present methodology is cheaper process, easy synthesis of stable catalyst and the catalyst can be easily recycled without significant loss of activity. 相似文献
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Eddie Wadbro Rajitha Udawalpola Martin Berggren 《Journal of Computational and Applied Mathematics》2010,234(6):1781-1787
Using gradient-based optimization combined with numerical solutions of the Helmholtz equation, we design an acoustic device with high transmission efficiency and even directivity throughout a two-octave-wide frequency range. The device consists of a horn, whose flare is subject to boundary shape optimization, together with an area in front of the horn, where solid material arbitrarily can be distributed using topology optimization techniques, effectively creating an acoustic lens. 相似文献
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Reddy P. Malla Venugopal M. Rajitha G. 《Journal of Applied Mechanics and Technical Physics》2022,63(2):259-267
Journal of Applied Mechanics and Technical Physics - In this paper, SH-wave propagation in an initially stressed triclinic layer welded between two half-spaces is investigated. The upper half-space... 相似文献
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The standard molar Gibbs free energy of formation of Co2TiO4, CoTiO3, and CoTi2O5 as a function of temperature over an extended range (900 to 1675) K was measured using solid-state electrochemical cells incorporating yttria-stabilized zirconia as the electrolyte, with CoO as reference electrode and appropriate working electrodes. For the formation of the three compounds from their component oxides CoO with rock-salt and TiO2 with rutile structure, the Gibbs free energy changes are given by:Accurate values for enthalpy and entropy of formation were derived. The compounds Co2TiO4 with spinel structure and CoTi2O5 with pseudo-brookite structure were found to be entropy stabilized. The relatively high entropy of these compounds arises from the mixing of cations on specific crystallographic sites. The stoichiometry of CoTiO3 was confirmed by inert gas fusion analysis for oxygen. Because of partial oxidation of cobalt in air, the composition corresponding to the compound Co2TiO4 falls inside a two-phase field containing the spinel solid solution Co2TiO4–Co3O4 and CoTiO3. The spinel solid solution becomes progressively enriched in Co3O4 with decreasing temperature. 相似文献