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1.
Summary Experiments and simulations prove that correlation chromatography can greatly reduce the disadvantage of a non-linear response of the chromatographic column. A factor that has been accepted as being an important source of error in correlation or multiplex chromatography, has been shown not to be. Separations affected, improve dramatically when correlation chromatography is used, and a substantial amount of correlation noise only arises when there is a large difference in separation between a conventional chromatogram and a correlogram.A model has been developed for simulating these nonlinearities. It is shown that, especially for correlation chromatography, the simulation results match the practical measurements very well. 相似文献
2.
We present here a methodology for searching a robust pore size distribution (PSD) for adsorbent materials. The method is based on a combination of individual adsorption isotherms, obtained from Grand Canonical Monte Carlo simulations, a regularization procedure to invert the adsorption integral equation (Tikhonov regularization solved by singular value decomposition), and the needed experimental adsorption isotherm. The selection of several parameters from the available choices to start the procedure are discussed here: the size of the kernel (number of individual pores and number of experimental adsorption points to be included), the fulfillment of the Discrete Picard condition, and the L-curve criteria, all leading to find a reliable and robust PSD. The procedure is applied to plugged hexagonal templated silicas (PHTS), synthesized, and characterized in our laboratory. 相似文献
3.
Pascher W. Den Besten J. H. Caprioli D. Leijtens X. Smit M. van Dijk R. 《Optical and Quantum Electronics》2003,35(4-5):453-464
Based on a rigorous vectorial analysis, a fast travelling-wave Mach–Zehnder modulator is modelled and designed. The cross-section of the semiconductor layer stack and the lossy electrodes are carefully modelled using the method of lines in order to investigate propagation characteristics, velocity and losses. This yields an accurate microwave and optical field distribution to explain the behaviour of the component. In order to enhance the modulation efficiency, design curves are derived and the cross-sectional dimensions for minimum microwave loss are determined. The loss of the optimized modulator agrees very well with small-signal measurements up to 40 GHz and HFSS simulations. The layerstack of the fabricated device is suitable for integration with InP multi-wavelength lasers. 相似文献
4.
5.
Azuelos G. Benslama K. Costanzo D. Couture G. Garcia J.E. Hinchliffe I. Kanaya N. Lechowski M. Mehdiyev R. Polesello G. Ros E. Rousseau D. 《The European Physical Journal C - Particles and Fields》2004,39(2):13-24
The European Physical Journal C - We discuss possible searches for the new particles predicted by Little Higgs Models at the LHC. By using a simulation of the ATLAS detector, we demonstrate how the... 相似文献
6.
C. Vaca‐Garcia G. Gozzelino W. G. Glasser M. E. Borredon 《Journal of Polymer Science.Polymer Physics》2003,41(3):281-288
The main transitions of cellulose fatty esters with different degrees of substitution (DSs) were investigated with dynamic mechanical thermal analysis. Two distinct main relaxations were observed in partially substituted cellulose esters (PSCEs). They were attributed to the glass‐transition temperature and to the chain local motion of the aliphatic substituents. The temperatures of both transitions decreased when DS or the number of carbon atoms (n) of the acyl substituent increased. Conversely, all the transitions of fully substituted cellulose esters occurred within a narrow temperature range, and they did not vary significantly with n. This phenomenon was explained by the formation of a crystalline phase of the fatty substituents. The presence of few residual OH groups in PSCEs was responsible for a large increase in the storage bending modulus, and it eliminated the effect of n on damping. © 2002 Wiley Periodicals, Inc. J Polym Sci Part B: Polym Phys 41: 281–288, 2003 相似文献
7.
Marilena Vasilescu Titus Constantinescu Mariana Voicescu Helge Lemmetyinen Elina Vuorimaa 《Journal of fluorescence》2003,13(4):315-322
The spectrophotometric study of luminol (LH2) in dimethyl sulfoxide (DMSO), DMSO-water solutions, and alkaline DMSO and DMSO-water solutions has been done, focusing on the effect of the KOH additon on LH2 absorption and fluorescence properties. The absorption spectra indicate an acid-base equilibrium, and the luminol dianion (L2–) formation at 3 × 10–4 – 2.4 × 10–3
M KOH. The decrease of the fluorescence intensity and the variation of the excitation spectra of LH2-DMSO-KOH solutions with KOH concentration have been similarly explained. The acid-base process is reversible. The addition of HCl to the solution with 3.0 × 10–3 M KOH leads to an increase of the fluorescence intensity to its highest value, observed in pure DMSO. The addition of HCl to the LH2-DMSO solution leads to the decrease of the fluorescence intensity as a result of the LH+
3 cation formation. In LH2-DMSO-water, the fluorescence band is shifted from 405 nm to 424 nm and increased in the intensity. In the presence of KOH (in LH2-DMSO-water-KOH solution) a new band appears, with the maximum at 485 nm and the band at 405 nm decreased. The changes in fluorescence lifetimes also evidence the different chemical species formed. 相似文献
8.
Alvaro P. Raposo Hans J. Weber David E. Alvarez-Castillo Mariana Kirchbach 《Central European Journal of Physics》2007,5(3):253-284
We briefly review the five possible real polynomial solutions of hypergeometric differential equations. Three of them are
the well known classical orthogonal polynomials, but the other two are different with respect to their orthogonality properties.
We then focus on the family of polynomials which exhibits a finite orthogonality. This family, to be referred to as the Romanovski
polynomials, is required in exact solutions of several physics problems ranging from quantum mechanics and quark physics to
random matrix theory. It appears timely to draw attention to it by the present study. Our survey also includes several new
observations on the orthogonality properties of the Romanovski polynomials and new developments from their Rodrigues formula. 相似文献
9.
V. A. Sadovnichy V. V. Alexandrov E. Soto T. B. Alexandrova T. G. Astakhova R. Vega N. V. Kulikovskaya V. I. Kurilov S. S. Migunov N. E. Shulenina 《Journal of Mathematical Sciences》2007,146(3):5938-5947
A mathematical model of the system composed of two sensors, the semicircular canal and the sacculus, is suggested. The model
is described by three lines of blocks, each line of which has the following structure: a biomechanical block, a mechanoelectrical
transduction mechanism, and a block describing the hair cell ionic currents and membrane potential dynamics. The response
of this system to various stimuli (head rotation under gravity and falling) is investigated. Identification of the model parameters
was done with the experimental data obtained for the axolotl (Ambystoma tigrinum) at the Institute of Physiology, Autonomous
University of Puebla, Mexico. Comparative analysis of the semicircular canal and sacculus membrane potentials is presented.
__________
Translated from Fundamentalnaya i Prikladnaya Matematika, Vol. 11, No. 7, pp. 207–220, 2005. 相似文献
10.
We introduce new classes of 2-weight cyclic codes which are direct sums of 1-weight irreducible cyclic codes
相似文献