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1.
Tikhonova I. A. Shubina E. S. Dolgushin F. M. Tugashov K. I. Teplitskaya L. N. Filin A. M. Sivaev I. B. Petrovskii P. V. Furin G. G. Bregadze V. I. Epstein L. M. Shur V. B. 《Russian Chemical Bulletin》2003,52(3):594-600
The reaction of cyclic trimeric perfluoro-o-phenylenemercury (o-C6F4Hg)3 (1) with the polyhedral [B12H11SCN]2– anion in THF at 20 °C affords the {[(o-C6F4Hg)3](B12H11SCN)}2– (4) and {[(o-C6F4Hg)3]2(B12H11SCN)}2– (5) complexes. Complex 5 was isolated as the tetrabutylammonium salt. X-ray diffraction analysis showed that this complex has a bent-sandwich structure in which the [B12H11SCN]2– anion is located between the planes of two molecules 1 and is coordinated to both these molecules through B—H—Hg bridges and S—Hg bonds. The stability constants of complexes 4 and 5 in THF (20 °C), which were determined from the IR spectroscopic data, are 16 L mol–1 and 992 L2 mol–2, respectively. 相似文献
2.
V. M. Filin V. F. Gorbunov S. A. Ulanov 《Journal of Radioanalytical and Nuclear Chemistry》1990,143(1):125-134
Emission Mössbauer (nuclear gamma-resonance) spectra of237Np resulting from the alpha-decay of241Am in solid solutions AmO2–ThO2 and AmO2–UO2 prepared by precipitation from LiF–NaF eutectic melts under fluorine-oxygen exchange were first investigated in the temperature range from 77 to 296 K. The resonant absorbers are NpO2 and NpAl2. The possibility is stated of managing the form of the emission Mössbauer spectra of237Np in dioxides by the directed change of the matrix stoichiometry or by its irradiation by visible light. At temperatures from 77 to 230 K the authors measured for the first time the NGR absorption spectra of237Np in solid solution NpO2–ThO2 with various concentrations of neptunium dioxide. An increase of the absorption line width (approximately by a factor of 4) with a decrease in the NpO2 contents (to 10 mol.%) was explained by the influence of fast electron exchange between Np4+ and Np5+ states observed in the NpO2–ThO2 solid solution at low concentrations of neptunium dioxide. 相似文献
3.
4.
L. A. Molokhina V. E. Rogalin S. A. Filin I. A. Kaplunov 《Russian Journal of Physical Chemistry A, Focus on Chemistry》2017,91(12):2302-2309
A mathematical model of the diffusion interaction of a binary system with several phases on the equilibrium phase diagram is presented. The theoretical and calculated dependences of the layer thickness of each phase in the multiphase diffusion zone on the isothermal annealing time and the ratio of the diffusion parameters in the neighboring phases with an unlimited supply of both components were constructed. The phase formation and growth in the diffusion zone during “reactive” diffusion corresponds to the equilibrium state diagram for two components, and the order of their appearance in the diffusion zone depends only on the ratio of the diffusion parameters in the phases themselves and on the duration of the incubation periods. The dependence of phase appearance on the incubation periods, annealing time, and difference in the movement rates of the components across the interface boundaries was obtained. An example of the application of the model for processing the experimental data on phase growth in a two-component three-phase system was given. 相似文献
5.
S. A. Akimenko V. N. Bolotov G. I. Britvich K. V. Datsko V. A. Duk A. P. Filin E. N. Gushchin A. V. Inyakin V. A. Khmelnikov A. S. Konstantinov V. F. Konstantinov I. Yu. Korolkov S. V. Laptev V. A. Lebedev V. M. Leontiev A. E. Mazurov V. P. Novikov V. F. Obraztsov V. A. Polyakov A. Yu. Polyarush V. E. Postoev V. I. Romanovsky V. I. Shelikhov O. G. Tchikilev V. A. Uvarov O. P. Yushchenko 《Physics of Atomic Nuclei》2007,70(4):702-708
Results of study of the $K^ - \to \pi ^0 e^ - \overline \nu \gamma $ decay at the ISTRA+ setup are presented. We observed 4476 events of this decay. The branching ratio is found to be $R = \frac{{Br(K^ - \to \pi ^0 e^ - \overline \nu _e \gamma )}}{{Br(K^ - \to \pi ^0 e^ - \overline \nu _e )}}$ = (1.81±0.03(stat.)±0.07(syst.)) × 10?2 for E*γ > 10 MeV and θ*eγ > 10°. For comparison with the previous experiment the branching ratio with cuts E*γ > 10 MeV, 0.6 < cos θ*eγ < 0.9 is calculated: R = $\frac{{Br(K^ - \to \pi ^0 e^ - \overline \nu _e \gamma )}}{{Br(K^ - \to \pi ^0 e^ - \overline \nu _e )}}$ = (0.47±0.02(stat.) ± 0.03(syst.)) × 10?2. For the cuts E*γ > 30 MeV and θ*eγ > 20°, used in most theoretical papers, Br = (3.06 ± 0.09(stat.) ± 0.14(syst.)) × 10?4. For the asymmetry we get A ξ = ?0.015 ± 0.021. At present it is the best estimate of this asymmetry. 相似文献
6.
Photochromic visualization has been used to investigate the hydrodynamic flow which arises inside a sliding valve during its operation. The experimental setup and results of observations of the flows are described. Unsteady flows with different amplitudes and frequencies of the oscillations of the flow rate through the valve were investigated. The method makes is possible to determine the flow structure, construct profiles of the velocities and tangential stresses in the complete region within the valve, and also obtain data for calculating the hydrodynamic characteristics of valves.Translated from Izvestiya Rossiiskoi Akademii Nauk, Mekhanika Zhidkosti i Gaza, No. 3, pp. 113–117, May–June, 1993. 相似文献
7.
We report observation and control of the spatial-spectral distributions of coherent, dynamic Rabi sideband radiation. The Rabi sidebands result from the interaction of a shaped picosecond probe laser of intensity 10(10) W cm(-2), with neutral excited atomic oxygen generated in a laser-induced microplasma. The spatial-spectral distribution is measured and compared for picosecond laser pulses having either an asymmetric temporal shape or a Gaussian temporal shape. The resulting spatial-spectral distributions are in quantitative agreement with theoretical predictions that account for the radial intensity distribution of the picosecond probe pulse. 相似文献
8.
9.
E. D. Aluker N. L. Aluker G. M. Belokurov A. G. Krechetov B. G. Loboiko D. R. Nurmukhametov A. V. Tupitsyn V. P. Filin 《Russian Journal of Physical Chemistry B, Focus on Physics》2010,4(1):63-65
A comparative study of the efficiency of the laser initiation of PETN by the first and second harmonics (1060 and 530 nm)
of a neodymium-doped phosphate glass laser was performed. A significant difference in the efficiency of PETN initiation by
the different harmonics was revealed: as the initial temperature of the sample increased from 373 to 450 K, the threshold
initiation fluence decreased from 3.0 to 0.5 J/cm2; at the same time, the second harmonic failed to initiate PETN even at a fluence of 10 J/cm2. The absorption spectrum of PETN was found to have a weak absorption band with a maximum at λ
m
= 1020 nm. It was assumed that the high efficiency of initiation by the first harmonic is associated with light absorption
(photo-initiation) by this band 相似文献
10.
In thin ferromagnetic films with perpendicular anisotropy, there exist stable large-radius dynamic topological solitons, which are stabilized owing to conservation of the orbital angular momentum of the magnetization field. The solitons can also exist if the projection of the total spin moment of the magnet onto the easy axis is not conserved, i.e., in the absence of pure uniaxial symmetry of the model. Even in the pure uniaxial case, the magnetization distribution in a soliton with a sufficiently large radius differs significantly from centrosymmetric. 相似文献