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Alexander E. Drukker Claude I. Judd Donald D. Dusterhoft 《Journal of heterocyclic chemistry》1966,3(2):206-208
The reaction of hydrazines and amines with 6-chloromorphanthridine was investigated. Grignard coupling of aminoalkyl halides with 6-chloromorphanthridine afforded 6-amino-alkylmorphanthridines. Cyclization of 6-(2-chloroethylamino)morphanthridine yielded the new ring system 5′H-imidazo[5, 6-a]dibenz[b, ejazepine, which was aminoalkylated by generation of the 11-position anion with butyllithium, followed by treatment with a tertiary aminoalkyl halide. 相似文献
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