排序方式: 共有55条查询结果,搜索用时 31 毫秒
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建立惰气熔融-热导法测定钕铁硼永磁材料中氢的分析方法。当氧-氢比例大于50:1时,CO对氢的测定结果产生一定的干扰,加入舒茨试剂可消除此干扰。采用标准坩埚,称样0.05g,熔融功率为2.85 kW,选择高纯镍篮和锡片做助熔剂,钕铁硼中氢释放完全。以普通钢铁参考物质建立氢校准曲线,线性相关系数r~2=0.9999,检出限为0.75μg/g。该法用于钕铁硼样品中氢的测定,测定结果与脉冲熔融飞行时间质谱-气体元素分析仪测定结果基本一致,测定结果的相对标准偏差为1.4%(n=5)。该方法可以准确测定钕铁硼永磁材料中的氢,能满足日常分析的要求。 相似文献
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以4-吡啶甲酸、芳香醛为原料,经缩合、氧化成环和酰化等反应,合成了4个未见文献报道的吡啶甲酰胺噁二唑类化合物,通过红外、核磁共振和元素分析对化合物的结构进行了表征.研究了这4个化合物的荧光性质和生物活性;荧光测试结果表明Cu2+可以使此系列化合物的荧光猝灭,Zn2+可以增强此系列化合物2-(吡啶-4-甲酰胺基)-5-对甲氧基苯基-1,3,4-噁二唑(2b)的荧光;生物活性测试结果表明这4个化合物对所测的5种病原菌都具有较好的杀菌活性,其中2-(吡啶-4-甲酰胺基)-5-对甲基苯基-1,3,4-噁二唑(2d)对小麦赤霉病菌的抑制活性可达到100%. 相似文献
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针对极端环境下耐辐照半导体核探测器的研制需求,采用耐高温、耐辐照的4H碳化硅(4H-SiC)宽禁带材料制成肖特基二极管,研究了该探测器对241Am源粒子的电荷收集效率。从电容-电压曲线得出该二极管外延层净掺杂数密度为1.991015/cm3。从正向电流-电压曲线获得该二极管肖特基势垒高度为1.66 eV,理想因子为1.07,表明该探测器具备良好的热电子发射特性。在反向偏压高达700 V时,该二极管未击穿,其漏电流仅为21 nA,具有较高的击穿电压。在反向偏压为0~350 V范围内研究了该探测器对3.5 MeV 粒子电荷收集效率,在0 V时为48.7%,在150 V时为99.4%,表明该探测器具有良好的电荷收集特性。 相似文献
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利用ANSYS中路径映射方法将压电陶瓷辐射超声波的声压值分布映射到对应的路径上;通过改变路径和角度,并提取数据,分析在79k Hz频率下埋入混凝土中的压电陶瓷进行超声无损检测时声场声能量特性的变化规律。研究结果表明:随着压电陶瓷辐射的声场中扩散角逐渐增加,散射区域增大,声压下降,声能衰减均呈非线性变化,且半扩散角为60°时,声能衰减速度相对较慢;随着压电陶瓷辐射声波传播的距离增大,最大声压和最小声压分布也在发生非线性变化,当半径大于0.09m时,最大声压对应的位置偏离主声轴;当路径对应的半径小于0.08m时,最小声压值对应角度变化较小;当路径对应的半径大于0.08m时,角度变化幅度比较大,大体上是在45°~61°范围内变化;等长度地增加路径对应的半径时,超声波的声能并不是等量减小而是开始时衰减最快,然后逐渐减小。 相似文献
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Employing the approximation theory based on refraction and the definition of the total point-spread-function of the imaging system, the variation in the edge contrast of simple model samples is discussed with different source-to-sample and sample-to-detector distances, which actually means different spatial resolutions of the imaging system. The experiments were carried out with the Beamline 4W1A imaging setup at the Beijing Synchrotron Radiation Facility for simple model and insect samples. The results show that to obtain clear phase-contrast images of biologic tissues for the X-ray in-line imaging setup, with determined parameters such as the size of the X-ray source, the pixel size of the detector and the fixed source-to-sample distance, there is a range of optimized sample-to-detector distances. The analysis method discussed in this article can be helpful in optimizing the setup of X-ray in-line phase-contrast imaging. 相似文献
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Influence of defect states on band gaps two-dimensional phononic crystal in the of4340 steel in an epoxy
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The band structures of a new two-dimensional triangle-shaped array geometry of 4340 steel cylinders of square cross section in an epoxy resin were studied by the plane-wave expansion and supercell calculation method. The band gaps of this type of phononic crystals with different defects were calculated such as defect-free, 60 crystal linear defect states, 120 crystal linear defect states, and 180 crystal linear defect states. It was found that the band gap will emerge in different linear defects of the phononic crystals and the bandwidth of linear defect states is larger than that of the free-defect crystal by about 2.14 times within the filling fraction F = 0.1-0.85. In addition, the influence of the filling fraction on the relative width of the minimum band gap is discussed. 相似文献
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