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Namiq G. Shikhaliyev Abel M. Maharramov Khanim N. Bagirova Gulnar T. Suleymanova Biligma D. Tsyrenova Valentine G. Nenajdenko Alexander S. Novikov Victor N. Khrustalev Alexander G. Tskhovrebov 《Mendeleev Communications》2021,31(2):191-193
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Aytan R. Asgarova Ali N. Khalilov Ivan Brito Abel M. Maharramov Namiq G. Shikhaliyev Jonathan Cisterna Alejandro Crdenas Atash V. Gurbanov Fedor I. Zubkov Kamran T. Mahmudov 《Acta Crystallographica. Section C, Structural Chemistry》2019,75(3):342-347
Cooperative action of hydrogen and halogen bonding in the reaction of 3‐(3,5‐di‐tert‐butyl‐4‐hydroxyphenyl)‐1‐phenylprop‐2‐en‐1‐one with HCl or HBr in alcohol medium under microwave irradiation (20 W, 80 °C, 10 min) allows the isolation of the haloetherification products (2S,3S)‐3‐(3‐tert‐butyl‐5‐chloro‐4‐hydroxyphenyl)‐2‐chloro‐3‐ethoxy‐1‐phenylpropan‐1‐one, C21H24Cl2O3, (2S,3S)‐2‐bromo‐3‐(3‐tert‐butyl‐5‐bromo‐4‐hydroxyphenyl)‐3‐methoxy‐1‐phenylpropan‐1‐one, C20H22Br2O3, and (2S,3S)‐2‐bromo‐3‐(3‐tert‐butyl‐5‐bromo‐4‐hydroxyphenyl)‐3‐ethoxy‐1‐phenylpropan‐1‐one, C21H24Br2O3, in good yields. Both types of noncovalent interactions, e.g. hydrogen and halogen bonds, are formed to stabilize the obtained products in the solid state. 相似文献
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