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M. Khalaj M. Ghazanfarpour-Darjani F. B. Seftejani A. Lalegani 《Crystallography Reports》2017,62(7):1060-1062
The title compound [Zn(dip)Br2] was synthesized using the Schiff base bidentate ligand (E)-4-tert-butyl-N-(pyridine-2-ylmethylene)benzeneamine (dip) and zinc(II) bromide salts. It has been characterized by elemental analysis, X-ray diffraction, and optical spectroscopy. The X-ray diffraction analysis demonstrates that in this structure, the zinc(II) ion is located on an inversion center and exhibits a ZnN2Br2 tetrahedral geometry. In this structure the dip ligand is coordinated with zinc(II) ion in a cyclic-bidentate fashion forming a five-membered metallocyclic ring. The compound crystallizes in the monoclinic sp. gr. P21/m with a = 9.2700(13) Å, b = 7.6128(11) Å, c = 12.3880(17) Å, and β = 97.021(3)°. 相似文献
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M. Khalaj F. B. Seftejani M. Ghazanfarpour-Darjani A. Lalegani 《Crystallography Reports》2017,62(7):1063-1065
The centrosymmetric dinuclear title complex [Hg2Cl4(dip)2] was synthesized using the Schiff base bidentate ligand (E)-4-ethyl-N-(pyridine-2-ylmethylene)benzeneamine (dip) and mercury(II) chloride salts. It has been characterized by elemental analysis, X-ray diffraction, and UV-Visible and infrared spectroscopic techniques. The X-ray analysis shows that the title compound crystallizes in the monoclinic sp. gr. P21/n, Z = 2 with a = 7.8233(17) Å, b = 15.178(3) Å, c = 12.559(3) Å, β = 97.021(3)°. The Hg(II) ion has a distorted trigonal–bipyramidal coordination environment formed by the bischelating N-heterocyclic ligands, two bridging Cl atoms and one terminal Cl atom. 相似文献
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Khalaj M. Jamali B. Lalegani A. Olyai M. R. Talei Bavil Seftejani F. B. 《Crystallography Reports》2019,64(7):1080-1083
Crystallography Reports - A coordination polymer [Hg(L)Cl2]n consisting of HgCl2 and Schiff base bidentate ligand (4-methoxyphenyl) pyridine-2yl methyleneamine (L) was prepared and structurally... 相似文献
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