排序方式: 共有28条查询结果,搜索用时 0 毫秒
1.
调味品中氯丙醇的GC/ECD和GC/MS/MS衍生化检测方法研究及应用 总被引:8,自引:0,他引:8
报道了调味品中氯丙醇的衍生化气相色谱(GC/ECD)和衍生化气相色谱双串联质谱法(GC/MS/MS)测定。GC/ECD测定酱油中3—氯—1,2—丙二醇(3—MCPD)的检出限达到0.01mg/kg,回收率为91%~104%,变异系数为2.27%~7.96%;GC/MS/MS同时测定酱油中1,3—二氯—2—丙醇、2,3—二氯—1—丙醇和3—氯—1,2—丙二醇,1,3—二氯—2—丙醇、2,3—二氯—1—丙醇的检出限为0.02mg/kg,3—氯—1,2—丙二醇的检出限为0.01mg/kg,回收率在92%~106%,变异系数为3.51%~13.33%。 相似文献
2.
国内附件类产品的自动化检测水平不高,对于变压器产品认证,传统人工测试方式采样速度难以达到规定要求,造成数据后期计算和处理难、误差率高、在线时间长、测试效率低下等问题;针对GB19212.1(IEC61558-1)标准关于电子电力类变压器产品中温升和异常状态型式试验项目的要求,研究开发了一套智能自动化测量与控制系统,采用以软件为核心的模块化架构,配合研制出的集成控制模块组,通过用户自定义需求,可完成包括试验设备控制、数据分析、实时监测、定时采集与算法处理、试验方案保存与原始记录生成等一系列功能,真正实现了变压器测试的“试前一次配置,全流程自动化”的试验过程;试验结果表明,该系统的应用可大幅降低人工测量环节的不确定度、提高测试结果准确率,并有效地保证了试验可复制性、结果一致性和可追溯性。 相似文献
3.
本文研究了单位圆盘上从$L^{\infty}(\mathbb{D})$空间到Bloch型空间 $\mathcal{B}_\alpha$ 一类奇异积分算子$Q_\alpha, \alpha>0$的范数, 该算子可以看成投影算子$P$ 的推广,定义如下$$Q_\alpha f(z)=\alpha \int_{\mathbb{D}}\frac{f(w)}{(1-z\bar{w})^{\alpha+1}}\d A(w),$$ 同时我们也得到了该算子从 $C(\overline{\mathbb{D}})$空间到小Bloch型空间$\mathcal{B}_{\alpha,0}$上的范数. 相似文献
4.
Wavefront correction of Ti:sapphire terawatt laser with varying precision of phase conjugation between deformable mirror and wavefront sensor
下载免费PDF全文
![点击此处可从《中国物理 B》网站下载免费的PDF全文](/ch/ext_images/free.gif)
The phase conjugation between the deformable mirror and the wavefront sensor in the aberration correction of a terawatt Ti:sapphire laser is studied experimentally and theoretically in this paper. At varying values of phase-conjugation precision, we focus the corresponding beams into spots of the same size of 5.1 μm×5.3 μm with a f/4 parabola in the 32 TW/36 fs Ti:sapphire laser system. The results show that the precision of conjugation can induce an intensity modulation but does not significantly affect the wavefront correction. 相似文献
5.
本文利用交叉偏振波产生技术(XPW)对800 nm波段钛宝石飞秒激光器输出的激光脉冲进行时域净化, 提高脉冲时域对比度, 并测量验证了1011对比度的脉冲, 达到测量仪器的动态范围极限, 比初始脉冲时域对比度有三个量级的提高, XPW的效率为22%. 同时发现净化后脉冲光谱宽度也得到一定展宽, 进一步利用啁啾镜对和补偿片对净化后的脉冲进行色散补偿, 得到25 fs脉宽的脉冲. 利用该净化后的激光脉冲作为种子注入已有的太瓦级钛宝石啁啾脉冲放大系统中, 在输出脉冲能量250 mJ, 宽度50 fs, 对应峰值功率5 TW的情况下, 在主脉冲前100 ps以外的范围内测量验证了1011的脉冲对比度. 相似文献
6.
A novel tiled Ti:sapphire(Ti:S)amplifier was experimentally demonstrated with>1 J amplified chirped pulse output.Two Ti:S crystals having dimensions of 14 mm×14 mm×25 mm were tiled as the gain medium in a four-pass amplifier.Maximum output energy of 1.18 J was obtained with 2.75 J pump energy.The energy conversion efficiency of the tiled Ti:S amplifier was comparable with a single Ti:S amplifier.The laser pulse having the maximum peak power of 28 TW was obtained after the compressor.Moreover,the influence of the beam gap on the far field was discussed.This novel tiled Ti:S amplifier technique can provide a potential way for 100 PW or EW lasers in the future. 相似文献
7.
反义c-Ha-ras寡聚核苷酸对转化细胞的生长抑制及其p21蛋白合成的抑制 总被引:3,自引:0,他引:3
本文合成了两个15聚核苷酸AS-1和AS-2,前者与c-Ha-ras mRNA的前三个密码子及其上游的核蛋白体结合点附近的单链区互补,后者与细胞核内未成熟c-Ha-rag RNA第一内含子3′端及第二外显子5′端区域互补,它们可分别阻断c-Ha-ras mRNA的翻译和拼接过程,从而降低c-Ha-ras癌基因的表达水平,抑制了转化细胞的增殖。这种抑制作用随浓度的增加(从4μmol/L至10μmol/L)而增加,加入AS-1或AS-2 12h后抑制作用达到高峰,以后逐渐下降。用ELISA方法测定转化细胞中c-Ha-ras产物p21蛋白水平,结果显示增殖受抑制细胞p21水平较对照细胞降低30%左右。 相似文献
8.
Effective diode-pumped continuous wave (CW) tunable laser action of a new alloyed crystal Yb:LYSO is demonstrated. The alloyed LYSO crystal possesses the desirable physical and laser performance of La2SiO5 (LSO), as well as the favorable growth properties and costs of Y2SiO5 (YSO) in the same time. With a 5 at.-% Yb:LYSO sample, the output power of 2.84 W at 1085 nm and an optical-to-optical conversion efficiency of 54.5% are achieved. Its laser wavelength can be tuned over a broad range of 81 nm, from 1030 to 1111 nm. 相似文献
9.
The spatial chirp generated in the Ti:sapphire multipass amplifier is numerically investigated based on the onedimensional(1D) and two-dimensional(2D) Frantz–Nodvik equations. The simulation indicates that the spatial chirp is induced by the spatially inhomogeneous gain, and it can be almost eliminated by utilization of proper beam profiles and spot sizes of the signal and pump pulses, for example, the pump pulse has a top-hatted beam profile and the signal pulse has a super-Gaussian beam profile with a relatively larger spot size. In this way, a clear understanding of spatial chirp mechanisms in the Ti:sapphire multipass amplifier is proposed, therefore we can effectively almost eliminate the spatial chirp and improve the beam quality of a high-power Ti:sapphire chirped pulse amplifier system. 相似文献
10.
A 2.0 kb fragment DNA plasmid which expresses antisense to the upstream first exon of c-Ha-ras oncogene was transfected into Ha-ras transformed cell lines, GCM-3T3 and REF-4.3. The transfection leads to the inhibition of malignant behaviour, shown by decreasing of growth speed, colony forming ability on soft agar, tumorigenicity in nude mice and increasing ot differentiation degree. In GCM-3T3 cells the lung metastasis frequency became much less (from 60% to 12.5%) after the transfection and the expression of ras oncogene product, and p21 protein was obviously decreased in the transfected cells. This work has first shown the inhibitory effect of antisense RNA on neoplastic behaviour in China. 相似文献