茄黄斑螟性信息素化学的结构签定(英文)

本文采用TLC、GC、微量臭氧化和GC-MS等分析方法,从茄黄斑螟雌蛾性腺体提取物中,分离和鉴定出性信息素反-11-十六碳烯醇乙酸酯(1a)。触角电位和田间试验证明,天然提取物和合成样品均有强烈的生物活性。     

Optical strong coupling in hybrid metal-graphene metamaterial for terahertz sensing

We propose a terahertz hybrid metamaterial composed of subwavelength metallic slits and graphene plasmonic ribbons for sensing application. This special design can cause the interaction between the plasmon resonances of the metallic slits and graphene ribbons, giving rise to a strong coupling effect and Rabi splitting. Intricate balancing in the strong coupling region can be perturbed by the carrier concentration of graphene, which is subject to the analyte on its surface. Thereby, the detection of analyte can be reflected as a frequency shift of resonance in terahertz transmission spectra. The result shows that this sensor can achieve a theoretical detection limit of 325 electrons or holes per square micrometer. Meanwhile, it also works well as a refractive index sensor with the frequency sensitivity of 485 GHz/RIU. Our results may contribute to design of ultra-micro terahertz sensors.     

高质量非晶金刚石薄膜的制备研究

利用自行研制的磁过滤等离子体技术(FCAP),并创造性地对衬底施加低频率周期性负偏压,在室温下的单晶硅表面上制备了高质量的非晶金刚石薄膜。用扫描电子显微镜(SEM),原子力显微镜(AFM),红外吸收光谱(IR),纳米硬度计和摩擦试验仪对制备的非晶金刚石薄膜进行了结构和性能表征。实验结果表明:制备的非晶金刚石薄膜表面十分光滑,表面粗糙度仅为0.1nm;薄膜中sp3键成份高达70.7%,对应薄膜硬度达到74.8GPa,接近金刚石的硬度;薄膜摩擦系数在0.12~0.16之间。文中也讨论了偏压类型对沉积薄膜结构的影响。     

纳米结构TiN薄膜的制备与性能研究

利用自行研制的磁过滤等离子体设备,在室温条件下的不锈钢基底上成功地制备了性能良好的纳米结构TiN薄膜.运用原子力显微镜和X射线衍射仪对其结构和形貌进行了表征.利用纳米硬度仪测量了TiN薄膜的硬度和弹性模量.结果显示:沉积的TiN薄膜表面非常平整光滑,致密而无缺陷;硬度远高于粗晶TiN的硬度;TiN晶粒尺寸在30～50nm;沉积过程中在基底上施加的负偏压会影响纳米结构TiN薄膜的结构和性能.     

茄黄斑螟性信息素化学结构的毛细管色谱/质谱测定

本文介绍用毛细管色谱/质谱联用技术,测定出茄黄斑螟性信息素化学结构为E_n—16:Ac。     

茄黄斑螟性信息素化学的结构鉴定

本文采用TLC、.GC、微量臭氧化和GC-MS等分析方法, 从茄黄斑螟雌蛾性腺体提取物中, 分离和鉴定出性信息素反-11-十六碳烯醇乙酸酯(1a)。触角电位和田间试验证明, 天然提取物和合成样品均有强烈的生物活性。