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V. L. Mikhailenko V. N. Kizhnyaev S. I. Verkhoturova K. A. Apartsin N. K. Gusarova E. G. Grigor’ev B. A. Trofimov 《Doklady Chemistry》2015,465(2):286-290
Polyquaternization reactions of bis[2-(4-pyridyl)ethyl]phenylethylphosphine oxide and tris[2-(4-pyridyl)ethyl]phosphine oxide with 1,4-dibromobutane were implemented for the first time to give linear (water-soluble) and cross-linked (limitedly water swelling), respectively, representatives of new phosphorus- and nitrogen-containing ionenes. The synthesized linear ionenes react with heparin and polyacrylic acid yielding water-insoluble polyelectrolyte complexes. 相似文献
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N. K. Gusarova S. F. Malysheva N. A. Belogorlova S. I. Verkhoturova L. A. Oparina S. N. Arbuzova N. A. Chernysheva A. M. Nalibayeva G. K. Bishimbayeva S. V. Yasko B. A. Trofimov 《Russian Journal of General Chemistry》2020,90(5):839-844
Two ways for the synthesis of new representatives of non-symmetric organic
phosphites with polyfluoroalkyl substituents were developed based on organic
dichlorophosphites. The reaction of polyfluoroalkyl dichlorophosphites with
allyl alcohol, proceeding at a temperature of –10–22°C (2 h) in the presence of
triethylamine, gave diallyl polyfluoroalkyl phosphites in a yield of 75–77%.
Under similar conditions (–30–22°C, 2–4 h, Et3N), alkyl
(or aryl) dichlorophosphites reacted with polyfluoroalkanols to form alkyl (or
aryl) bis(polyfluoroalkyl) phosphites (yield 56–67%). Unlike
diallylpolyfluoroalkyl- and alkylbis(polyfluoroalkyl) phosphites,
arylbis(polyfluoroalkyl) phosphites are symmetrized under storage conditions
(room temperature, inert atmosphere), forming the corresponding triaryl- and
tris(polyfluoroalkyl) phosphites. 相似文献
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N.?K.?Gusarova S.?I.?Verkhoturova S.?N.?Arbuzova T.?I.?Kazantseva A.?I.?Albanov A.?M.?Nalibaeva G.?K.?Bishimbaeva K.?A.?Apartsin V.?V.?Kireeva B.?A.?TrofimovEmail author 《Russian Journal of General Chemistry》2018,88(4):705-712
Polyfluoroalkanols readily reacted with 2-chloro-1,3,2-dioxaphospholanes and 2-chloro-1,3,2-dioxaphosphinanes in hexane in the presence of triethylamine (–10 to 25°C, 5 h) to give 2-polyfluoroalkoxy-1,3,2- dioxaphospholanes and 2-polyfluoroalkoxy-1,3,2-dioxaphosphinanes in 48–72% yield. The products were found to exist as mixtures of cis and trans isomers with the trans isomer predominating for the phospholanes and cis isomer predominating for the phosphinanes according to the 1H, 13C, 19F, and 31P NMR data. 相似文献
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N. K. Gusarova S. I. Verkhoturova T. I. Kazantseva S. N. Arbuzova A. I. Albanov A. A. Tatarinova B. A. Trofimov 《Russian Journal of General Chemistry》2013,83(10):1895-1899
Secondary phosphine sulfides and phosphine selenides react with allylamine under the conditions of radical initiation (UV or AIBN) to form the anti-Markovnikov adducts in up to 93 % yield. 相似文献
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Arbuzova S. N. Verkhoturova S. I. Borodina T. N. Artem΄ev A. V. 《Journal of Structural Chemistry》2022,63(9):1383-1389
Journal of Structural Chemistry - By the interaction of CuI with bis(2-pyridyl)phosphine oxides (2-Py)2RP(O) containing E-1-phenyl-2-aroylethenyl–C(Ph)=CHC(O)R′... 相似文献
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Gusarova N. K. Malysheva S. F. Belogorlova N. A. Verkhoturova S. I. Arbuzova S. N. Chernysheva N. A. Volkov P. A. Nalibayeva A. M. Bishimbayeva G. K. Trofimov B. A. 《Russian Chemical Bulletin》2021,70(11):2195-2199
Russian Chemical Bulletin - Polyfluoroalkyl dichlorophosphites reacted with propargyl alcohol in Et3N/hexane to give di(2-propynyl) polyfluoroalkyl phosphites, which are transformed into... 相似文献