3D-measurement using a scanning electron microscope

In this paper the improved photometric or the so called “Shape From Shading” method is presented. In comparison to known and established approaches the efficiency of the detector system was considered and the requirements of the cosine Lambert’s law for the angle distribution of the emitted electrons are suppressed. The method retrieves more accurate data of sub-micrometer substructures like diffractive optical elements (DOE) due to an increased lateral resolution and works more efficiently than widely used comparable techniques.     

Existence and uniqueness of solutions of sequential nonlinear fractional difference equations with three‐point fractional sum boundary conditions

In this paper, we consider a discrete fractional boundary value problem of the form: where 0 < α,β≤1, 1 < α + β≤2, λ and ρ are constants, γ > 0, , is a continuous function, and E_βx(t) = x(t + β ? 1). The existence and uniqueness of solutions are proved by using Banach's fixed point theorem. An illustrative example is also presented. Copyright © 2014 John Wiley & Sons, Ltd.     

Investigation of structural,morphological, optical,and magnetic properties of Sm-doped LaFeO3 nanopowders prepared by sol–gel method

Journal of Sol-Gel Science and Technology - Pure orthorhombic phase of La1?xSmxFeO3 (x?=?0, 0.1, 0.2, and 0.3) nanoparticles can be obtained by sol–gel method after...     

Effect of annealing on electrical responses of electrode and surface layer in giant-permittivity CuO ceramic

The effect of heat treatments on the electrical responses of the electrode and surface layer in a giant-permittivity CuO ceramic is investigated. It is found that the giant low-frequency relative permittivity of the CuO ceramic can be tuned by annealing in Ar and O₂—it can be reduced by annealing in Ar, and then it can be enhanced up to the initial value by annealing in O₂. The results indicate to the effect of oxygen vacancy concentration on the giant dielectric properties of the CuO ceramic. Interestingly, three sets of dielectric relaxations are observed in the O₂–annealed sample, which can be assigned as the effects of outmost surface layer, electrode, and grain boundary. Our results reveal that the giant low-frequency dielectric response in the CuO ceramic is associated with both of the interfacial polarization at the sample–electrode interface resulted from a non-Ohmic electrode contact and the outmost surface layer-inner part interface.     

Positive solutions of three-point fractional sum boundary value problem for Caputo fractional difference equations via an argument with a shift

In this paper, we study a new class of three-point boundary value problem of nonlinear Caputo fractional difference equation. Our problem contain an argument with a shift. The existence of at least one positive solution is proved by using the Guo-Krasnoselskii’s fixed point theorem. Some illustrative examples are given.     

Dielectric properties of Ni-doped Ba0.5Sr0.5TiO3 ceramics prepared with hydrothermal synthesized nanopowders

Ba_0.5Sr_0.5Ti_1?xNi_xO₃ (BSTN) ceramics were prepared from BSTN nanopowders synthesized by a hydrothermal method. The phase and microstructure of samples were characterized by X-ray diffraction (XRD) and scanning electron microscopy. XRD results indicate a cubic structure of the pure BST nanopowders. The cubic structure can be converted to the orthorhombic phase with increasing of Ni content to x = 0.01 and returned to the cubic structure with the presence of Ni(OH)₂ impurity phase for x = 0.03 and 0.05. However, the BSTN ceramics sintered at 1,200 °C for 3 h revealed the orthorhombic phase structure with NiO impurity phase for all Ni content. The doping of Ni in Ba_0.5Sr_0.5TiO₃ structure can increase the grain size of samples from 1.47 to 3.26 μm. The dielectric constant, loss tangent (tanδ) and phase transition temperature of BSTN ceramics were reduced with increasing Ni content.     

Boundary value problem for p−Laplacian Caputo fractional difference equations with fractional sum boundary conditions

In this paper, we consider a discrete fractional boundary value problem of the form where 0 < α,β≤1, 1 < α + β≤2, 0 < γ≤1, , ρ is a constant, and denote the Caputo fractional differences of order α and β, respectively, is a continuous function, and ?_p is the p‐Laplacian operator. The existence of at least one solution is proved by using Banach fixed point theorem and Schaefer's fixed point theorem. Some illustrative examples are also presented. Copyright © 2015 John Wiley & Sons, Ltd.