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O. A. Luk´yanov G. V. Pokhvisneva T. V. Ternikova G. A. Smirnov 《Russian Chemical Bulletin》2015,64(5):1062-1064
Chlorides and anhydrides of carboxylic (including dicarboxylic) acids react with salts of 1-methoxy-3-methyl-1-triazene 2-oxides to give the corresponding 3-acyl-1-methoxy-3-methyl-1-triazene 2-oxides. 相似文献
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G. A. Smirnov P. B. Gordeev S. V. Nikitin G. V. Pokhvisneva T. V. Ternikova I. M. Chistokhvalov O. A. Luk’yanov 《Russian Chemical Bulletin》2018,67(11):2010-2015
A method for synthesizing new compounds capable of releasing NO within living organisms, namely, 2-azidoethyl derivatives of methylenebis(1-oxytriaz-1-ene 2-oxides) bearing one or few 2-azidoethyl moieties, was developed. The synthesis involves nucleophilic substitution of the bromine atoms of the parent 2-bromoethyl derivatives of methylenebis(1-oxytriaz-1-ene 2-oxides) with the azide group. Some of the synthesized compounds are of interest as promising energetic materials. 相似文献
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S. V. Nikitin G. V. Pokhvisneva T. V. Ternikova P. B. Gordeev I. M. Chistokhvalov G. A. Smirnov O. A. Luk’yanov 《Russian Chemical Bulletin》2018,67(8):1445-1451
Synthetic procedures towards new N-β-hydroxyethyl- and N-β-bromoethylated 1,1’-[methyl enebis(oxy)]bis(triaz-1-ene 2-oxides) were developed. N-β-Nitroxyethyl[methylenebis(oxy)]- bis(triaz-1-ene 2-oxides) were first synthesized by nitration of N-β-hydroxyethyl derivatives and nucleophilic substitution of the bromine atom of N-β-bromoethyl derivatives. The first representative of a new class of energetic compounds, namely, (1-nitroxymethoxy)triaz-1-ene 2-oxide, was synthesized. 相似文献
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G. A. Smirnov P. B. Gordeev S. V. Nikitin G. V. Pokhvisneva T. V. Ternikova O. A. Luk’yanov 《Russian Chemical Bulletin》2016,65(11):2644-2649
Synthetic procedure to access the first representatives of a new series of 3-monosubstitued functional derivatives of 1-alkoxy-1-triazene 2-oxides, i.e., 1-alkoxy-3-(2-hydroxyethyl)- and 1-alkoxy-3-(2-acetoxyethyl)-1-triazene 2-oxides, were elaborated. 1-Alkoxy-3,3-bis(2-hydroxyethyl)-1-triazene 2-oxides were used to derive 3-(2-acetoxyethyl)-, 3-(2-bromoethyl)- and 3-(2-cyanoethyl)substituted 1-alkoxy-3-(2-acetoxyethyl)-1-triazene 2-oxides. 相似文献
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T. V. Ternikova G. V. Pokhvisneva G. A. Smirnov S. V. Nikitin P. B. Gordeev O. A. Luk’yanov 《Russian Chemical Bulletin》2016,65(12):2873-2878
Synthetic procedures to access new potential NO donors that can generate NO in living systems, 3,3-bis(2-hydroxyethyl) and 3,3,3’-tris(2-hydroxyethyl) derivatives of 1,1’-[methylenebis(oxy)]bis(3,3-dialkyltriaz-1-ene 2-oxides), were elaborated. 3,3-Bis(2-acetoxyethyl)-1(chloromethoxy)triaz-1-ene 2-oxide reacts with 1-hydroxytriaz-1-ene 2-oxide sodium salts to give a series of alkylated 3,3-bis(2-acetoxyethyl) derivatives. Deacetylation of the latter produces 3-(2-hydroxyethyl)-11,11-dialkyl-6,8-dioxa-3,4,5,9,10,11-hexaazaundeca-4,9-dien-1-ol 4,10-dioxides and 11-alkyl-3-(2-hydroxyethyl)-6,8-dioxa-3,4,5,9,10,11-hexaazatrideca-4,9-diene-1,13-diol 4,10-dioxides. 相似文献
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O. A. Luk’yanov G. V. Pokhvisneva T. V. Ternikova N. I. Shlykova 《Russian Chemical Bulletin》2012,61(2):360-365
Reaction of pseudonitroles and their derivatives with diaminofurazan in the presence of dibromoisocyanuric acid (DBI) resulted in symmetrical 3,4-bis(-nitroalkyl-ONN-azoxy)-furazans or their derivatives. For the synthesis of bis(nitroalkyl-ONN-azoxy)furazans bearing various a-nitroalkyl-ONN-azoxy groups, the method based on the reaction of ??-nitronitroso compounds with 3-amino-4-(nitroalkyl)-ONN-azoxy)furazans (in the presence of DBI) was developed. Synthetic procedures towards aforementioned compounds with nitromethyl-, dibromonitromethyl-, trinitromethyl-ONN-azoxy and other groups were described. 相似文献
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Luk′yanov O. A. Shlykova N. I. Pokhvisneva G. V. Ternikova T. V. Monogarov K. A. Meerov D. B. Nelyubina Yu. V. Dorovatovskii P. V. Kon′kova T. S. 《Russian Chemical Bulletin》2019,68(1):110-115
Russian Chemical Bulletin - Methods for the syntheses of a series of high-energy 4(10)-2-fluoro-2,2-dinitroethyl and 4(10)-2,2-dinitroethyl derivatives of polynitrohexaazaisowurtzitanes were... 相似文献
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G. V. Pokhvisneva P. B. Gordeev S. V. Nikitin G. A. Smirnov T. V. Ternikova O. A. Luk’yanov 《Russian Chemical Bulletin》2018,67(9):1655-1661
3,3-Bis(2-nitroxyethyl) derivatives of 1,1′-[methylenebis(oxy)]bis(triaz-1-ene 2-oxides) were synthesized by either nucleophilic substitution of the bromine atoms of parent 3,3-bis(2- bromoethyl) compounds or nitration of structurally related 3,3-bis(2-hydroxyethyl) derivatives. The synthesized compounds comprise two different NO donating moieties, namely, oxytriaz- 1-ene 2-oxide and nitrate groups, and, therefore, can be regarded as a new type of NO-donating agents. 相似文献