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1.
R. Szymczak K. Zaveta H. Szymczak H. -Q. Guo H. Kronmü ller 《Journal of magnetism and magnetic materials》1994,130(1-3):363-366
The temperature dependence of magnetization of a nanocrystalline Fe60Co30Zr10 alloy annealed at various temperatures to varying crystal sizes was investigated down to 5 K in the field range up to 5 T. The fitting procedure gave T3/2 as the leading term irrespective of the crystal size. We suggest that the increase of the coefficient by this term for smaller crystals may be connected to an increased relative volume of their surface. 相似文献
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S. V. Trukhanov V. V. Fedotova A. V. Trukhanov S. G. Stepin H. Szymczak 《Crystallography Reports》2008,53(7):1177-1180
Nanocrystalline manganite La0.50Ba0.50MnO3 was synthesized by the soft-chemical method. For this purpose, the sol-gel method was modified and improved. A trihydric saturated alcohol, e.g., glycerol, was suggested as a new organic matrix. The crystal structure of the composite was studied by X-ray powder diffraction at room temperature. A La0.50Ba0.50MnO3 powder annealed in air at T = 500°C is characterized by a perovskite-like cubic structure with the unit-cell parameter a = 3.869 Å. The chemical composition of the sample was studied by electron-probe X-ray microanalysis. The La: Ba: Mn cation ratio in the material was 1: 1: 2. The surface topography was examined with a scanning electron microscope. The crystallite size was ~30 nm. The dependence of the crystal structure and the surface topology on the annealing temperature was studied. The high-temperature treatment in air resulted in the growth of larger, micrometer-size, crystallites. 相似文献
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Soderstrom E McKenna JA Abrams GS Adolphsen CE Averill D Ballam J Barish BC Barklow T Barnett BA Bartelt J Bethke S Blockus D Bonvicini G Boyarski A Brabson B Breakstone A Bulos F Burchat PR Burke DL Cence RJ Chapman J Chmeissani M Cords D Coupal DP Dauncey P DeStaebler HC Dorfan DE Dorfan JM Drewer DC Elia R Feldman GJ Fernandes D Field RC Ford WT Fordham C Frey R Fujino D Gan KK Gero E Gidal G Glanzman T Goldhaber G Gomez Cadenas JJ Gratta G Grindhammer G Grosse-Wiesmann P Hanson G Harr R 《Physical review letters》1990,64(25):2980-2983
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Komamiya S Abrams GS Adolphsen CE Averill D Ballam J Barish BC Barklow T Barnett BA Bartelt J Bethke S Blockus D Bonvicini G Boyarski A Brabson B Breakstone A Bulos F Burchat PR Burke DL Cence RJ Chapman J Chmeissani M Cords D Coupal DP Dauncey P DeStaebler HC Dorfan DE Dorfan JM Drewer DC Elia R Feldman GJ Fernandes D Field RC Ford WT Fordham C Frey R Fujino D Gan KK Gatto C Gero E Gidal G Glanzman T Goldhaber G Gomez Cadenas JJ Gratta G Grindhammer G Grosse-Wiesmann P Hanson G Harr R 《Physical review letters》1990,64(24):2881-2884
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Rode MF Roszak S Szymczak JJ Sadlej J Leszczynski J 《The Journal of chemical physics》2004,121(13):6277-6281
The results of the theoretical study of ground state potential energy surfaces for the chlorine-acetonitrile anion and its photodetachment product are presented. The shallow potential surfaces allow for the nondefinitive position of the chlorine within the complex. The dissociation energy of the neutral complex, estimated through the thermodynamic cycle, indicates significant structural changes due to the photodetachment process. The excess negative charge is localized mostly on the chlorine atom, and the electron detachment proceeds as an electron is removed from chlorine. The process leads to drastic changes in the electrostatic interactions within the complex. The first electronic excited state corresponds to the excess electron transfer from chlorine to acetonitrile fragment. This state is a precursor of the observed charge-transfer-to-solvent state. 相似文献
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