HL—1装置SiC涂层辐照实验的表面分析

本文应用表面分析技术研究HL-1装置中SiC涂层的等离子体辐照性能。结果表明,SiC材料应用于孔栏和壁涂层有利于减少杂质和提高等离子体品质。     

离子色谱柱切换技术同时测定食品中的多种成分

采用离子色谱柱切换技术同时测定了保留性质差别较大的有机酸以及不同价态的无机阴离子。由于柱切换基本不影响色谱基线,该法有较高的灵敏度。同时测定了食品中的乙酸,山梨酸、苯甲酸、糖精、氯离子和磷酸根。     

镉（Ⅱ）－2－（2－苯并噻唑偶氮）－5－二甲氨基苯甲酸配合物的吸附伏安法研究及应用

镉（Ⅱ）－２－（２－苯并噻唑偶氮）－５－二甲氨基苯甲酸配合物的吸附伏安法研究及应用徐素君，施清照，张培敏，吴念慈（杭州大学化学系３１００２８）关键词：２－（２－苯并噻唑偶氮）－５－二甲氨基苯甲酸（ＢＴＡＭＢ），镉，吸附伏安法杂环偶氮试剂的极谱性质及其...     

镓在氨基吡啶树脂上的吸附行为及机理

前文已报道了氨基吡啶树脂对AuCl_4~-、PtCl_6~(2-)的吸附性。本文报道4-氨基吡啶树脂对镓的吸附行为与机理。在6mol/L HCl条件下,对镓的氯络阴离子(GaCl_4~-)有很好的吸附性。并能定量洗脱。测得静态吸附容量为351.15mg/g树脂,用化学法及红外光谱等方法,测得4-氨基吡啶树脂吸附镓(Ⅲ)的基本参数。     

Molybdenum Carbide‐Embedded Multichannel Hollow Carbon Nanofibers as Bifunctional Catalysts for Water Splitting

With the environmental pollution and non‐renewable fossil fuels, it is imperative to develop eco‐friendly, renewable, and highly efficient electrocatalysts for sustainable energy. Herein, a simple electrospinning process used to synthesis Mo₂C‐embedded multichannel hollow carbon nanofibers (Mo₂C‐MCNFs) and followed by the pyrolysis process. As prepared lotus root‐like nanoarchitecture could offer rich porosity and facilitate the electrolyte infiltration, the Mo₂C‐MCNFs delivered favourable catalytic activity for HER and OER. The resultant catalysts exhibit low overpotentials of 114 mV and 320 mV at a current density of 10 mA cm^?2 for HER and OER, respectively. Furthermore, using the Mo₂C‐MCNFs catalysts as a bifunctional electrode toward overall water splitting, which only needs a small cell voltage of 1.68 V to afford a current density of 10 mA cm^?2 in the home‐made alkaline electrolyzer. This interesting work presents a simple and effective strategy to further fabricating tunable nanostructures for energy‐related applications.     

HL—1装置等离子体辐照Tic涂层实验分析

一、引言在聚变等离子体中控制杂质的污染被认为是获得高温等离子体的重要问题之一。因此对材料要进行优化选择,例如石墨和碳就是目前有利的孔栏材料和结构材料。但是由于碳的自溅射作用和化学活性,在高温溅射时可形成易挥发的碳化物,如甲烷等从而增加了化学腐蚀。某些含碳的化合物如TiC,SiC和BC以及氮化物如TiN和Si_3N_4等是目前研究的一些有用途的材料。实际上TiC或TiN已经用于孔栏,壁内衬涂层或高频加热天线。     

A 1.107 μm Yb3+-doped Phosphate Fiber Laser Pumped by a Ti:sapphire

Lasers and amplifiers in a single fiber have been developed rapidly, especially for optical fiber communication and various sensors, in the recent years. However, remarkable progress and achievement have been made mainly in silica fiber doped with rare earth elements. In this paper, we report the progress on the development of the Yb3+-doped phosphate fiber laser.     

HL—1装置表面分析站的研制

等离子体与表面相互作用的重要性是人们公认的。我们试图在HL-1装置上原位测量表面状态,本文叙述了为HL-1研制的表面分析站及测得的一些结果。为装置提供了实验数据。     

Three kinds of horizon-like hypersurface of a uniformly accelerating, non-stationary charged black hole

Three kinds of horizon-like hypersurface of a uniformly rectilinearly accelerating, non-stationary charged black hole: event horizon, apparent horizon and time-like limit surface are studied. The result is that the event horizon is apart from the time-like limit surface and the apparent horizon in the case where the black hole is charged, uniformly accelerating and its mass is varying (evaporating and accreting). Some other new results are also given. Project supported by the National Natural Science Foundation of China.