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The acidic and neutral impurities in heroin samples (46 Purified South-East Asian (PSEA) and 8 non-PSEA samples) were analysed using gas chromatography. Mass spectral detection allowed the construction of a comprehensive library of over 649 impurities. A variety of statistical procedures were used to select 70 viable profiling parameters. Cluster analyses were used to investigate the similarities between samples using organic parameters. A blended PSEA profile was constructed for comparison with samples of unknown origins. Resolution between samples of PSEA/non-PSEA origins was demonstrated with a selection of 25 (18 continuous and 7 dichotomised) discriminating factors. Several predictive logistic models were created using up to 18 parameters, explaining 85-100% of the variation in the experimental data. 相似文献
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G Fuchs K-H Müller J Freudenberger K Nenkov S-L Drechsler SV Shulga D Lipp A Gladun T Cichorek P Gegenwart 《Pramana》2002,58(5-6):791-797
The effect of substitutional disorder on the superconducting properties of YNi2B2C was studied by partially replacing yttrium and nickel by Lu and Pt, respectively. For the two series of (Y, Lu)Ni2B2C and Y(Ni, Pt)2B2C compounds, the upper critical field H
c2(T) and the specific heat c
p(T, H) in the superconducting mixed state have been investigated. Disorder is found to reduce several relevant quantities such
as T
c, the upper critical field H
c2(0) at T=0 and a characteristic positive curvature of H
c2(T) observed for these compounds near T
c. The H
c2(T) data point to the clean limit for (Y, Lu) substitutions and to a transition to the quasi-dirty limit for (Ni, Pt) substitutions.
The electronic specific heat contribution γ(H) exhibits significant deviations from the usual linear γ(H) law. These deviations reduce with growing substitutional disorder but remain even in the quasidirty limit which is reached
in the Y(Ni1−x
, Pt
x
)2B2C samples for x=0.1. 相似文献
3.
Non-resonant microwave absorption (NRMA) studies of superconducting MgB2 and a sample containing ∼10% by weight of MgO in MgB2 are reported. The NRMA results indicate near absence of intergranular weak links in the pure MgB2 sample. A linear temperature dependence of the lower critical field H
c1 is observed indicating a non-s wave superconductivity. However, the phase reversal of the NRMA signal which could suggest d wave symmetry is also not observed. In the MgB2 + MgO sample, much larger low field dependent absorption is observed indicating the presence of intergranular weak links.
The hysteretic behavior of NRMA is compared and contrasted in the two samples. In the pure MgB2 sample, a large hysteresis is observed between the forward and the reverse scans of the magnetic field indicating strong
pinning of flux lines. This hysteresis saturates a few degrees below T
c while in the MgB2 + MgO sample, a much slower increase of hysteresis with decreasing temperature is observed, a signature of weaker pinning. 相似文献
4.
Lawson W. Calame J.P. Hogan B.P. Skopec M. Striffler C.D. Granatstein V.L. 《IEEE transactions on plasma science. IEEE Nuclear and Plasma Sciences Society》1992,20(3):216-223
The operating characteristics of a two-cavity X -band gyroklystron experiment are reported. Beam voltages and currents up to 440 kV and 200 A, respectively, are generated in 1 μs pulses by a thermionic magnetron injection gun. Velocity ratios (ν⊥ /νz) near one in the output cavity are used to achieve peak powers of 24 MW near 9.87 GHz. The maximum saturated efficiency of more than 33% occurs at a beam voltage of 425 kV and a current of 150 A. A large signal gain in excess of 34 dB is realized by operating the input cavity just below the start oscillation threshold. Details of tube stability and the dependence of amplification on magnetic field profile, input signal parameters, and various beam quantities are presented 相似文献
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