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Jiang Yuqi Gao Shuaibo Li Peng Ma Yongsong Yin Huayi Wang Dihua 《Journal of Radioanalytical and Nuclear Chemistry》2022,331(7):2919-2928
Journal of Radioanalytical and Nuclear Chemistry - The waste LiCl–Li2O oxide reduction salt was solidified and transformed into sodalite by the spark plasma sintering method. Compared with... 相似文献
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Shuaibo Zhang Dong Li Bangzhong Wang Wuding Sun Haojun Ma Kai Di Luyang Sun Jinfeng Zhao Jingping Qu Yuhan Zhou 《European journal of organic chemistry》2023,26(36):e202300593
An efficient strategy for asymmetric trifluoromethylated allylic alkylation of easily available N-substituted glycine ethyl esters with α-(trifluoromethyl)alkenyl acetates has been developed. Catalyzed by a [Pd(C3H5)Cl]2/(R)-BINAP, various trifluoromethyl-containing N-substituted glycine ethyl ester derivatives are afforded with good yields and excellent enantioselectivities. The product can be readily converted into diverse fluoro-substituted species, which shows the practicability of this method. 相似文献
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Fu Qingjin Wang Yanyun Liang Shuaibo Liu Qian Yao Chunli 《Journal of Solid State Electrochemistry》2020,24(3):533-544
Journal of Solid State Electrochemistry - Nowadays, supercapacitors based on cellulose nanofibril (CNF) films have attracted extensive interest due to their excellent flexibility, light weight, and... 相似文献
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We have developed an efficient, metal-free, convenient and relatively cheap method for iodine-induced direct alkylation of azoles via in situ formed alkyliodide. A series of heterocyclic derivatives are readily prepared under mild conditions in moderate to good yields and high regioselectivity. 相似文献
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建立黄曲霉毒素测定仪的校准方法。黄曲霉毒素测定仪校准项目主要包括仪器的动态基线漂移、长期基线噪声、线性相关系数、最小检测浓度、定性与定量重复性。选用C18色谱柱,以甲醇为流动相,流量为1.0 mL/min,其长期基线噪声不大于1500 counts/(30 min),动态基线漂移不大于5000 counts/h;当选用甲醇中黄曲霉毒素B1溶液标准物质,以乙腈-甲醇(1∶1)为流动相,仪器最小检测浓度不大于0.03 ng/mL,线性相关系数不小于0.998,定性重复性不大于1.0%,定量重复性不大于3.0%,仪器的计量性能正常。据此对影响仪器主要性能的各个参数进行全面评价,确认各项性能指标控制在合理范围内。该校准方法切实可行,可用于黄曲霉毒素测定仪的校准。 相似文献
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