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1.
The thermal decomposition of four commercial powders and of differently stored single crystals of sodium hydrogen carbonate is studied by power compensation DSC and by optical and FT-IR microscopy. Independently of manufacturer, specified purity and price, the thermal curves of all the commercial powders show a more or less pronounced low temperature peak preceding the one due to the main decomposition. Such small peak is not observed when samples of laboratory recrystallized material are used. However the thermal behaviour of the latter preparation differs remarkably depending on storage conditions: the material kept in closed glass containers decomposes at temperatures higher than those of the material stored in a dessiccator in the presence of concentrated H2SO4. The observation by optical microscopy of the behaviour of the surfaces of single crystals coming from different storage conditions when the temperature is raised in a Kofler heater helps the interpretation of the data collected. The mechanism of the decomposition is discussed and the relevant kinetic parameters reported. 相似文献
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Stability criteria for crack propagation have been analysed which are based on the second law of thermodynamics. The isothermal case has been studied both for elastic and viscoelastic materials. The non-isothermal criteria have been considered with particular attention to a fast adiabatic loading process.The thermodynamic constitutive equations which are demanded and their relationships with the elastic energy have been analyzed. 相似文献
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Samuel Boissière Marc Nieper-Wißkirchen Alessandra Sarti 《Journal de Mathématiques Pures et Appliquées》2011,95(5):553-563
We define Enriques varieties as a higher dimensional generalization of Enriques surfaces and construct examples by using fixed point free automorphisms on generalized Kummer varieties. We also classify all automorphisms of generalized Kummer varieties that come from an automorphism of the underlying abelian surface. 相似文献
5.
During adiabatic deformation experiments on polyisobutylene of various molecular weights and on polyvinylacetate, the temperature change was measured. The thermal effects occurring during the subsequent stress relaxation were also recorded. From all data, the conclusion was drawn that the entropic elasticity theory is obeyed for temperatures sufficiently above the glass transition temperature. When the value of Tg is approached, some interesting energy effects become appreciable. 相似文献
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Michela Artebani Samuel Boissière Alessandra Sarti 《Mathematische Nachrichten》2015,288(14-15):1581-1591
We prove that the Borcea–Voisin mirror pairs of Calabi–Yau threefolds admit projective birational models that satisfy the Berglund–Hübsch–Chiodo–Ruan transposition rule. This shows that the two mirror constructions provide the same mirror pairs, as soon as both can be defined. 相似文献
9.
Noncollinear difference frequency mixing of dye laser and Nd:YAG second harmonic (fundamental) radiation from a commercial
laser system is employed for the generation of 2.7–5.3 μm (1.6–1.7 μm) radiations in a flux-grown KTiOAsO1 crystal. The generated radiation is used to scan the methane absorption in the fundamental (v
3) and its first overtone (2v
3) band at pressure 90 torr in a laboratory made single pass gas cell of length 33 cm. 相似文献
10.
Cristiana Boi Valentina Busini Matteo Salvalaglio Carlo Cavallotti Giulio C. Sarti 《Journal of chromatography. A》2009,1216(50):8687-8696
Affinity chromatography with Protein A beads has become the conventional unit operation for the primary capture of monoclonal antibodies. However, Protein A activated supports are expensive and ligand leakage is an issue to be considered. In addition, the limited production capabilities of the chromatographic process drive the research towards feasible alternatives. The use of synthetic ligands as Protein A substitutes has been considered in this work. Synthetic ligands, that mimic the interaction between Protein A and the constant fragment (Fc) of immunoglobulins, have been immobilized on cellulosic membrane supports. The resulting affinity membranes have been experimentally characterized with pure immunoglobulin G (IgG). The effects of the membrane support and of the spacer arm on the ligand–ligate interaction have been studied in detail. Experimental data have been compared with molecular dynamic simulations with the aim of better understanding the interaction mechanisms. Molecular dynamic simulations were performed in explicit water, modelling the membrane as a matrix of overlapped glucopyranose units. Electrostatic charges of the ligand and spacer were calculated through ab initio methods to complete the force field used to model the membrane. The simulations enabled to elucidate how the interactions of surface, spacer and ligand with IgG, contribute to the formation of the bond between protein and affinity membrane. 相似文献