Some results on fractionaln-factor-critical graphs

A simple graphG is said to be fractionaln-factor-critical if after deleting anyn vertices the remaining subgraph still has a fractional perfect matching. For fractionaln-factor-criticality, in this paper, one necessary and sufficient condition, and three sufficient conditions related to maximum matching, complete closure are given.     

Oscillation of certain partial difference equations

In this paper we consider a class of nonlinear delay partial difference equations and a class of linear delay partial difference equations with variable coefficients, which may change sign. We obtain oscillation criteria for these equations. There are no results for the oscillation of these equations up to now.     

一种新型温度自补偿高灵敏度折射率计

基于高频CO2激光脉冲写入的新型超长周期光纤光栅(ULPFG),提出了一种可实现温度自补偿的新型高灵敏度折射率计。理论与实验表明,新型超长周期光纤光栅不同闪耀阶次谐振峰对外界折射率与温度变化的灵敏度各自不同,特别的是,该光栅存在对外界折变不敏感的谐振峰,测量中除了可以利用该峰实现温度同时测量外,还可以补偿另一个测量折变的谐振峰因温度变化带来的测量误差。该折射率计具有制作简单、成本低、强度好,灵敏度高等优点,当外界折射率在1.43~1.45范围内变化时,其折射率测量灵敏度可达每单位折射率240 nm,在实际工业应用中具有较大的潜在实用价值。     

温度/应变/扭曲三参量同时测量低成本传感系统

提出了一种利用布喇格光纤光栅反射光作信号源、高频CO2激光脉冲写入的长周期光纤光栅和超周期光纤光栅作传感器实现温度、应变和扭曲同时测量的全光栅型低成本强度解调传感方案.文中利用长周期光纤光栅边缘滤波效应实现了温度、应变和扭曲传感信号的实时解调.实验结果表明,其温度和应变的测量灵敏度分别为－0.211 dB/℃和－0.012 dB/10με;而扭曲率的测量灵敏度为0.4394 dB/(rad·m－1),是该法写入普通LPFG的4倍以上.     

利用ABEEMσπ模型研究哺乳类催产素及其衍生物

哺乳类催产素及其衍生物是一系列包含S—S键的多肽分子. 应用原子-键电负性均衡σπ(ABEEMσπ)模型, 我们研究了该系列多肽分子的分子内氢键和整体软度与生物活性关系. 首先利用点电荷模型计算了该系列多肽分子的分子内氢键能, 并与实验值对比, 得到了基本一致的结果. 再根据整体软度与生物活性的关系: 即整体软度越大, 分子生物活性越大, 我们成功解释了催产素及其衍生物的分子生物活性的变化关系. 将ABEEMσπ模型初步应用于研究含 S—S键多肽的相关性质方面, 并取得了和实验以及其它理论计算较为一致的结果. 因此, 以上研究为该模型进一步探讨其它多肽的相关性质提供了一定的理论基础.     

Plutonium concentration and <Superscript>240</Superscript>Pu/<Superscript>239</Superscript>Pu isotopic ratio in the surface soils from the Jiuquan region in northwestern China

Surface soil samples collected in the Jiuquan region in the downwind area of the Chinese nuclear test site (CNTs) were analyzed for Pu isotopes. The ^239+240Pu activities ranged from 0.025 ± 0.009 to 0.89 ± 0.16 mBq g^?1, varying significantly with different sampling sites. The Dunhuang city that is located in the southwestern part of the Jiuquan region received the heaviest Pu deposition (^239+240Pu activities, 0.23–0.89 mBq g^?1). Most of the ²⁴⁰Pu/²³⁹Pu isotopic ratios were similar with that of the global fallout. However, the low values (0.080–0.147) observed in three sampling sites further supported the finding of Pu originated from CNTs in that region.     

改进的Faster-RCNN算法在聚乙烯管接头内部缺陷检测中的应用

超声相控阵技术是目前聚乙烯管道热熔接头内部缺陷检测的一种主流方法。提出了基于注意力机制的改进Faster-RCNN目标检测网络用于超声相控阵D扫图聚乙烯管接头内部缺陷检测。针对聚乙烯管道热熔接头内部超声相控阵D扫图小缺陷较多、特征信息容易丢失的问题,将残差网络(ResNet50)与特征金字塔网络(FPN)相结合作为骨干网络,并引入卷积注意力模块(CBAM)自适应细化特征。将SSD网络框架和Faster-RCNN网络框架用于模型训练和测试,使用VGG16、ResNet50、ResNet50+FPN、ACBM+ResNet50+FPN作为骨干网络依次对超声相控阵聚乙烯管道热熔对接接头内部缺陷样本进行训练对比。结果表明,改进的Faster-RCNN网络模型在聚乙烯管接头内部缺陷检测和分类方面有明显改进,对小缺陷的检测性能有了显著的提高。     

Monosaccharide compositional analysis of marine polysaccharides by hydrophilic interaction liquid chromatography-tandem mass spectrometry

A simple and sensitive method was developed using hydrophilic interaction liquid chromatography coupled to tandem mass spectrometry for determination of monosaccharides liberated from marine polysaccharides by acidic hydrolysis. Optimal separation of diastereomeric monosaccharides including hexoses, pentoses, and deoxyhexoses was achieved using an aminopropyl bonded column with mobile phase containing ternary solvents (acetonitrile/methanol/water) in conjunction with MS/MS in SRM mode. Mechanisms for fragmentation of deprotonated monosaccharides with regard to cross-ring cleavage were proposed. Matrix effects from coeluting interferences were observed and isotopic-labeled internal standard was used to compensate for the signal suppression. The method demonstrated excellent instrumental limits of detection (LOD), ranging from 0.7 to 4.2 pg. Method LODs range from 0.9 to 5.1 nM. The proposed method was applied to the analysis of polysaccharides in seawater collected from the open leads of the central Arctic Ocean in the summer of 2008.     

Phase transition in polyamide‐66/montmorillonite nanocomposites on annealing

The crystalline‐phase transition in polyamide‐66/montmorillonite nanocomposites before melting was investigated by in situ X‐ray diffraction and is reported for the first time in this work. The phase‐transition temperature in the nanocomposites was 170 °C, 20 °C lower than that in polyamide‐66. The lower phase‐transition temperature of the nanocomposites could be attributed to the γ‐phase‐favorable environment caused by silicate layers. Meanwhile, the addition of silicate layers changed the crystal structure of the polyamide‐66 matrix and influenced the phase‐transition behavior. © 2002 Wiley Periodicals, Inc. J Polym Sci Part B: Polym Phys 41: 63–67, 2003