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Sarıkaya Yüksel Önal Müşerref Pekdemir Abdullah Devrim 《Journal of Thermal Analysis and Calorimetry》2020,140(6):2667-2672
Journal of Thermal Analysis and Calorimetry - A method was proposed to use XRD-data for thermal analyses of crystalline solids. Therefore, the XRD-pattern was recorded for natural and preheated... 相似文献
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Surfactants treatment of crude oil contaminated soils 总被引:4,自引:0,他引:4
This study reports experimental measurements investigating the ability of a biological (rhamnolipid) and a synthetic (sodium dodecyl sulfate, SDS) surfactant to remove the North Sea Ekofisk crude oil from various soils with different particle size fractions under varying washing conditions. The washing parameters and ranges tested were as follows: temperature (5 to 50 degrees C), time (5 to 20 min), shaking speed (80 to 200 strokes/min), volume (5 to 20 cm3), and surfactant concentration (0.004 to 5 mass%). The contaminated soils were prepared in the laboratory by mixing crude oil and soils using a rotating cylindrical mixer. Two contamination cases were considered: (1) weathered contamination was simulated by keeping freshly contaminated soils in a fan assisted oven at 50 degrees C for 14 days, mimicking the weathering effect in a natural hot environment, and (2) nonweathered contamination which was not subjected to the oven treatment. The surfactants were found to have considerable potential in removing crude oil from different contaminated soils and the results were comparable with those reported in literature for petroleum hydrocarbons. The removal of crude oil with either rhamnolipid or SDS was within the repeatability range of +/-6%. The most influential parameters on oil removal were surfactant concentration and washing temperature. The soil cation exchange capacity and pH also influenced the removal of crude oil from the individual soils. However, due to the binding of crude oil to soil during weathering, low crude oil removal was achieved with the weathered contaminated soil samples. 相似文献
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Mustafa Ersin Pekdemir Mediha Kök Muhammed Sait Kanca Ecem Özen Öner Sibel Pekdemir Şule Inci Sevda Kirbağ Beyhan Tatar 《先进技术聚合物》2023,34(2):605-612
Recently, there has been a great demand for boron-containing compounds (BCCs) with unique biological properties. The demand for the use of these compounds not alone but as additives in composite materials is increasing day by day. In this study, the effect of adding B2O3 compound to the blend of PLA and PEG polymers, which is an important biocompatible shape memory polymer, was investigated. In order to examine the effect of increasing B2O3 additive on the thermal properties of PLA-PEG blend, it was determined by using a Differential Scanning Calorimetry (DSC) and thermogravimetric analyzer (TGA), and it was seen that while the melting temperature of PEG decreased, the melting temperature of PLA increased. In addition, when the thermal stability of the composites was examined, increasing of thermal stability was observed with the addition of B2O3 and a three-step degradation occurred. It was determined that the B2O3/PLA-PEG composite was homogeneous by taking X-ray measurements and SEM measurements. The antimicrobial property of the PLA-PEG blend improved with the increasing B2O3 contribution were observed from the antimicrobial activity measurements of the composite against 4 different bacteria. However, it was determined that the PLA-PEG blend preserved its shape memory effect with increasing diboron trioxide contribution. 相似文献
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