排序方式: 共有23条查询结果,搜索用时 15 毫秒
1.
Nuray Ulusoy Muammer Kiraz Ömer Küçükbasmacı 《Monatshefte für Chemie / Chemical Monthly》2002,133(10):1305-1315
Summary. New 4-alkyl/aryl-1-((6-(4-bromophenyl)-imidazo[2,1-b]thiazol-3-yl)-acetyl)-3-thiosemicarbazides and 3-alkyl/aryl-2-(((6-(4-bromophenyl)-imidazo[2,1-b]thiazol-3-yl)-acetyl)-hydrazono)-4-thiazolidinones were synthesized from 6-(4-bromophenyl)-imidazo[2,1-b]thiazole-3-acetic acid hydrazide. Their structures were elucidated by elemental analyses and spectroscopic data. All compounds
were tested for antibacterial and antifungal activities. The antimicrobial activities of the compounds were assessed by the
microbroth dilution technique. The compounds were also evaluated for antituberculosis activity against Mycobacterium tuberculosis H37Rv (ATCC 27294); they exhibited varying degrees of inhibition in the in vitro primary screening at 6.25 μg · cm−3. The most active compound was 3-(4-nitrophenyl)-2-(((6-(4-bromophenyl)-imidazo[2,1-b]thiazol-3-yl)-acetyl)-hydrazono)-4-thiazolidinone.
Corresponding author. E-mail: nurayulusoy@yahoo.com
Received December 10, 2001. Accepted (revised) March 1, 2002 相似文献
2.
Lipomatous tumors of the uterus are unusual, benign neoplasms seen in postmenopausal women. Although many of the mixed-type cases such as lipoleiomyoma and fibrolipoma have been reported, pure uterine lipomas are extremely rare. In the literature, a few cases with pure uterine lipoma have been reported. We first present the advanced magnetic resonance findings of pure uterine lipoma, followed by those of ultrasonography (US) and computed tomography (CT). We markedly detected lipid peaks on the magnetic resonance spectroscopy (MRS) and the apparent diffusion coefficient value to be 0.00 due to chemical-shift effects with diffusion-weighted imaging (DWI). Although pelvic lipomatous tumors can be diagnosed with US and CT, in some cases, further workup may be required to localize the lesion. MRI may yield more valuable data for differential diagnosis. MRS and DWI findings provide additional clues on the nature of the lesion. 相似文献
3.
Firat AK Karakaş HM Yakinci C Altinok T Alkan A Biçak U 《Magnetic resonance imaging》2004,22(9):1329-1332
Acute disseminated encephalomyelitis (ADEM) is an immune-mediated demyelinating disorder usually encountered in children or adolescents and characterized by multifocal neurological deficits of rapid onset. Typical target areas of demyelination include the corona radiata, centrum semiovale, periventricular white matter, cerebellar peduncles and brainstem. Involvement of deep gray matter nuclei is also frequent. We report a 6-year-old boy with ADEM who had only brainstem involvement. Serial magnetic resonance images representing the stage of disease and response to steroid treatment are presented. 相似文献
4.
Selçuk Demir Hamide Merve Çepni Małgorzata Hołyńska Muammer Kavanoz Fatih Yilmaz Yunus Zorlu 《Journal of Coordination Chemistry》2017,70(19):3422-3433
Via an oxidation reaction of Cu(I) iodide with pyridine-2,6-dicarboxylic acid (H2L) in DMF three copper(II) complexes, [(CH3)2NH2]2[CuL2] (1), K2[CuL2]?H2L?H2O (2) and [Cu(L)(H2O)]n (3), were synthesized and characterized. The structures of 1–3 were determined by single crystal X-ray diffraction studies. In-situ DMF decomposition produces dimethylamine base under solvothermal conditions and a proton transfer reaction takes place for the complex formation of 1. 3-D networks are stabilized in 1 and 2 via hydrogen bonds. Complex 3 is a 1-D coordination polymer with Cu-O semi-coordination bonds. Thermal decomposition of the complexes results in the corresponding metal oxides. Also, the electrochemical behavior of 1 was determined to be a metal-centered and diffusion-controlled, one-electron reduction process. 相似文献
5.
Muammer Kula 《Acta Mathematica Hungarica》2011,133(1-2):14-32
In previous papers, various notions of (strongly) closed subobject, (strongly) open subobject, connected, compact and T i , i=0,1,2 objects in a topological category were introduced and compared. The main objective of this paper is to characterize each of these classes of objects in the category of Cauchy spaces as well as to examine how these generalizations are related. 相似文献
6.
Alkan A Sahin I Keskin L Cikim AS Karakas HM Sigirci A Erdem G 《Magnetic resonance imaging》2008,26(4):446-450
PURPOSE: Obesity is characterized by an altered distribution of body fluid. However, distribution of fluid (extracellular/intracellular) in brain tissues has not been studied in obese subjects yet. The purpose of this study was to detect possible brain diffusion changes especially in satiety and hunger related centers in obese subjects by diffusion weighted imaging (DWI). METHODS: Conventional MRI and DWI of the brain was obtained from 81 obese patients (obese=68, morbid obese=13) and 29 age-matched, nonobese. The apparent diffusion coefficient (ADC) values were calculated in hypothalamus; amygdala; hippocampal gyrus; thalamus; insula; cingulate gyrus; orbitofrontal, dorsomedial and dorsolateral frontal, middle temporal and occipital cortex; cerebellum; midbrain and corpus striatum. RESULTS: The ADC values of hypothalamus, hippocampal gyrus, amygdala, insula, cerebellum and midbrain were significantly increased in patients (n:81) when compared to nonobese subjects. The ADC values of thalamus, hippocampal gyrus, amygdala, orbitofrontal, occipital, dorsolateral and middle temporal cortex, insula and midbrain were significantly increased in morbid obese when compared to nonobese subjects. The ADC values of orbitofrontal and occipital cortex were significantly higher in morbid obese than the values in the obese. The body mass index positively correlated with ADC values of amygdala, insula, orbitofrontal and middle temporal cortex. CONCLUSION: We observed increased ADC values of distinct locations related to satiety and hunger that suggest altered fluid distribution and/or vasogenic edema in obese subjects. Awareness of this abnormalities in brain tissue composition/function in obesity may contribute to better understanding of the underlying mechanisms. 相似文献
7.
8.
Synthesis of a novel crosslinked superabsorbent copolymer with diazacyclooctadecane crown ether and its sorption capability 总被引:1,自引:0,他引:1
Sevil Sava?kan Y?lmaz Dilek Kul Muammer Erdöl Mustafa Özdemir R?za Abbaso?lu 《European Polymer Journal》2007,43(5):1923-1932
A novel crosslinked poly(acrylic acid-copolymer-Kryptofix-22-DM) superabsorbent copolymer, poly(AA-co-Kry22-DM), was synthesised by the reaction of 4,13-dimethylacryloyl-1,7,10,16-tetraoxa-4,13-diazacyclooctadecane (Kyrptofix-22-DM) and acrylic acid (AA). Characterisation of the polymers was achieved by FTIR and 1H NMR techniques. Sorption capacity of the crosslinked poly(AA-co-Kry22-DM) superabsorbent copolymer was investigated for Pb2+, Cu2+, Cr3+, Cd2+, Mn2+, Zn2+, and Ni2+ heavy metal ions at different pH values using Freundlich and Langmuir isotherms. Swelling ratio, qv, and distribution ratio, log D, values of the crosslinked poly(AA-co-Kry22-DM) superabsorbent copolymer were calculated at various pH values. 相似文献
9.
The quantitative effects on chromatographic resolution of FTIR flow-cells for detection in capillary SFC have been determined. A suitably designed cell with a volume of 500 nl was shown to cause only modest broadening of chromatographic peaks obtained from the surfactant mixture Triton X-100, showing that subsequent detection methods can therefore be used in a multi-hyphenated chromatographic ensemble. A larger-volume (980 nl) cell was found to give satisfactory results with 100 μ columns, but not with 50 μm columns. The practicability of a multi-hyphenated system was illustrated by a preliminary capillary SFC-UV-FTIR-FID study on a plant extract. Good infrared spectra were obtained, together with well-resolved UV and (subsequent) FID chromatograms. 相似文献
10.
Rahim Hassanzadeh Muammer Ozgoren 《International Journal of Computational Fluid Dynamics》2013,27(10):535-545
A numerical investigation of flow around a sphere is performed and compared with previous studies. Here, a second-order accurate, finite volume method is used in order to predict the instantaneous and time-averaged flow characteristics using large eddy simulation (LES) on the multi-block grid system. Namely, the objectives of this article are: (i) the presentation of flow structures in the wake region downstream of the sphere with a wide variety of flow properties such as the distribution of velocity vectors, patterns of streamlines, Reynolds stress correlations, root mean square of velocity components and other time-averaged flow data in order to reveal the vortical flow structures in detail and (ii) to demonstrate the abilities of computational methods in simulation of vortical flow data. Finally, it has been concluded that there are good agreements between the experimental results and numerical predictions. 相似文献