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1.
Satyanarayana A. V. S. Rao M. Jagannadha Mouli K. Chandra 《Journal of Radioanalytical and Nuclear Chemistry》2022,331(3):1509-1513
Journal of Radioanalytical and Nuclear Chemistry - 相似文献
2.
Madhava Rao Mannam Chandra Mouli Pavuluri Naga Raju Chamarthi 《Phosphorus, sulfur, and silicon and the related elements》2013,188(9):922-932
AbstractAn efficient and robust synthetic procedure was developed primarily for the synthesis of a precursor compound; 3-(trifluoromethyl)-5,6,7,8-tetrahydro-[1, 2, 4]triazolo[4,3-a]pyrazine (11), from 2-chloropyrazine (7) through the chemical transformations such as hydrazine substitution, trifluoroacetyl group induction, cyclization and pyrazine ring reduction. A new series of urea derivatives 13a-e and thiourea derivatives 13f-j of compound 11 have been synthesized and the structures of all the compounds were confirmed using spectroscopic analyses such as IR, 1H NMR, 13C NMR, LC-MS and HRMS. The newly synthesized compounds were screened for their in vitro antimicrobial activity against five bacteria and two fungi, in which compounds 13d, 13i and 13j displayed potential activity against bacterial strains and 13a, 13d, 13g and 13j against fungal strains with the MIC values in the range of 6.25–25.0 µg/mL. An overall comparison of the activity results revealed that thiourea derivatives contain better activity than that of urea compounds. Molecular docking studies on poly (ADP-ribose) polymerase 15 (ARTD7, BAL3) demonstrated that all the synthesized compounds possess significant binding energies (-8.1 to -9.8?kcal/mol) with no adverse effect in the active site of protein. 相似文献
3.
ESR and optical absorption studies have been carried out on Cu2+-doped lithium hydrazinium sulphate single crystals at 303 K. The spin-Hamiltonian parameters evaluated indicate a N2O2 square planar environment for Cu2+ ion in this lattice. The correlation ofESR and crystal structure data leads us to conclude that Cu2+ ion enters the lattice interstitially. Charge compensation is achieved by the release of protons. Using the optical absorption
andESR data, bonding parameters and orbital reduction factors are also evaluated. 相似文献
4.
Electron spin resonance studies have been carried out on Cu2+ ion doped in single crystals of cadmium maleate dihydrate at 303 and 77K. It has been found that Cu2+ enters this lattice interstitially. The spin Hamiltonian parameters have been evaluated and the ground state wave function
is found to be predominantly |X
2 −Y
2〉 with a slight admixture of |3Z
2 −r
2〉. 相似文献
5.
A total synthesis of the 16-membered macrolides, macrosphelides C and F has been achieved starting from l-(+)-arabinose. 相似文献
6.
Electron spin resonance studies were carried out on Cu2+ doped triglycine calcium bromide. The spectra recorded at room temperature revealed well-resolved hyperfine spectra of63Cu superposed with super-hyperfine lines due to14N nuclei. The spin Hamiltonian parameters are evaluated. It was concluded that the Cu2+ enters the lattice interstitially. 相似文献
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8.
Fluid Dynamics - The phenomenon of air core vortexing in liquid draining through cylindrical tanks can have serious adverse effects on many engineering systems. Hence, suppression of such vortices... 相似文献
9.
G. V. P. Chandra Mouli T. Giridhar D. Mohan Rao R. B. Reddy 《Journal of heterocyclic chemistry》1996,33(1):5-8
The synthesis of a series of derivatives of 4-hydroxycoumarin analogues of aflatoxin and a preliminary testing of their anticoagulant activity is described. 相似文献
10.
Chandra Mouli Pandey Srishti Dewan Seema Chawla Birendra Kumar Yadav Gajjala Sumana Bansi Dhar Malhotra 《Analytica chimica acta》2016
We report results of the studies relating to controlled deposition of the amino-functionalized silica-coated zinc oxide (Am-Si@ZnO) nano-assemblies onto an indium tin oxide (ITO) coated glass substrate using Langmuir-Blodgett (LB) technique. The monolayers have been deposited by transferring the spread solution of Am-Si@ZnO stearic acid prepared in chloroform at the air-water interface, at optimized pressure (16 mN/m), concentration (10 mg/ml) and temperature (23 °C). The high-resolution transmission electron microscopic studies of the Am-Si@ZnO nanocomposite reveal that the nanoparticles have a microscopic structure comprising of hexagonal assemblies of ZnO with typical dimensions of 30 nm. The surface morphology of the LB multilayer observed by scanning electron microscopy shows uniform surface of the Am-Si@ZnO film in the nanometer range (<80 nm). These electrodes have been utilized for chronic myelogenous leukemia (CML) detection by covalently immobilizing the amino-terminated oligonucleotide probe sequence via glutaraldehyde as a crosslinker. The response studies of these fabricated electrodes carried out using electrochemical impedance spectroscopy show that this Am-Si@ZnO LB film based nucleic acid sensor exhibits a linear response to complementary DNA (10−6–10−16 M) with a detection limit of 1 × 10−16 M. This fabricated platform is validated with clinical samples of CML positive patients and the results demonstrate its immense potential for clinical diagnosis. 相似文献