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Mogilevkina M. F. Shipachev V. A. Tkachev S. V. Troshkova G. P. Martynets L. D. 《Russian Journal of Coordination Chemistry》2002,28(6):419-422
The reaction between cis-[Pt(NH3)2Cl2], N1-(2"-tetrahydrofuranyl)-5-fluorouracil (HL), and NaOH (taken in a molar ratio of 1 : 1 : 1) or between cis-[Pt(NH3)2Cl2], HL, and Ag2O (taken in the molar ratio of 1 : 1 : 0.5) was used to synthesize complexes Ia (in the case of NaOH) or Ib (in the case of Ag2O) with composition Pt(NH3)2LCl. The model complex [Pt(NH3)3L]NO3 (II) was synthesized by the reaction between [Pt(NH3)3Cl]Cl, HL, AgNO3, and Ag2O (1 : 1 : 1 : 0.5). The obtained compounds were characterized by chemical analysis, chromatography, thermogravimetry, conductometry, potentiometry, IR, electronic, and NMR spectroscopies. Complexes Ia and Ib were found to have both similar and different properties. The structures of the compounds and the type of L– coordination to platinum(II) were suggested. Cytotoxic properties of Iaand Ib were studied. 相似文献
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