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The Diels-Alder adduct of ethyl (E)-3-nitroacrylate and furan provides a versatile template for the stereoselective synthesis of mono and dihydroxylated derivatives of 2-aminocyclohexanecarboxylic acid (ACHC). The hydroxylated ACHC derivatives can be considered to be useful building blocks for β-peptides. 相似文献
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[reaction: see text] A short asymmetric synthesis of (2'S,5R,6R)-2'-[6-amino-5-hydroxy-1,3-cyclohexadiene-1-carbonyloxy]propionic acid, the enantiomer of the reported structure of (+)-oryzoxymycin is described. The reported spectral data does not match that obtained for synthetic "oryzoxymycin". 相似文献
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An efficient total synthesis of flavans from the reactions of salicylaldehyde and acetophenone derivatives is reported. The synthesis involves preparation of chalcones through an aldol reaction followed by reduction of both the double bond and the ketone using NaBH4 and an acetic acid mediated cyclization. Methoxy groups on the aromatic rings did not affect significantly the yields of the procedure. 相似文献
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The preparation of substituted 2-amino-4H-chromenes by a Na2CO3-catalyzed reaction of malononitrile, benzaldehydes, and phloroglucinol or resorcinol in aqueous medium and at room temperature is reported. The merits of this procedure include limited use of organic solvents, easy workup technique, and high purity of products. The 2-amino-4H-chromenes were prepared in yields of 54–96%. 相似文献
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LUCINIO JÚDEZ ROSARIO DE ANDRÉS MIGUEL IBÁÑEZ ELVIRA URZAINQUI 《Natural Resource Modeling》2011,24(3):297-315
Abstract This paper aims to determine the minimum agri‐environmental premium per hectare that farmers should receive to reduce crop irrigation. To this end, the authors develop a mixed‐integer quadratic model using a new methodology based on traditional positive mathematical programming, which allows the inclusion in the model of crop variants that are not present in the baseline situation of the farms. What is shown is that the results obtained with this new methodology, using the cost average approach of calibration, are the same as those obtained with an empirical method, when there is no change of crop distribution after the changeover from irrigated to nonirrigated farms. The theoretical results are compared with those obtained using the calibration with exogenous elasticities and are illustrated numerically for a representative farm of an area around Spain's Tablas de Daimiel in which the use of groundwater for crop irrigation has led to the ongoing deterioration of wetlands that depend on the same source of water, endangering the region's environmental sustainability. 相似文献
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In this study, 12 compounds, which include a new flavanone 5-methoxy mundulin, were isolated from the leaves, stem bark and twigs of Mundulea sericea (Willd.) A. Chev. (Fabaceae; Papilionoideae). The structures of the compounds were identified based on spectral data analyses. The constituents of M. sericea also showed antimicrobial activities (MIQ?=?0.01-100?μg) against Staphylococcus aureus, Bacillus subtilis, Escherichia coli, Pseudomonas aeruginosa and Candida albicans. 相似文献
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The Zeeman effect of the R absorption lines for the pure compound 2[Cr(en)3Cl3]KCl.6H2O has been measured photographically, using a strong pulsed magnet with fields of up to 200 000 gauss at 77 K. The results indicate g ∥ (4 A 2) = 1·82 , g ⊥(4 A 2) = 1·90 with g ∥(ē) = -1·82 and g ∥ (2ā) = 1·82. The uncertainties are of the order of ± 0·05. 相似文献
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