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Scientific investigations of the Imperial Gates from the Petrindu wooden church,Salaj County,Romania 下载免费PDF全文
Olivia Florena Marutoiu Ioan Bratu Constantin Marutoiu Dana Luminita Postolache Mihai Dragomir Claudiu Tanaselia Sorina Garabagiu 《X射线光谱测定》2018,47(2):176-185
In order to preserve and restore the Imperial Gates from the Petrindu wooden church, Salaj County, Romania, (map location—latitude, longitude: 46.97, 23.19), the scientific investigation of the wooden support and painting materials (ground and pigments) was performed, employing Fourier‐transform infrared spectroscopy (FTIR), X‐ray fluorescence spectroscopy, and 3D scanning. FTIR spectroscopy offered information about the wooden degradation stage, whereas X‐ray fluorescence and FTIR spectroscopic methods were employed for structural painting materials characterization. The structural data can be correlated with the artistic, theological, and historical analysis of this religious patrimony object. After obtaining information about the wooden support and painting materials, the Imperial Gates were 3D digitized using state of the art laser scanning technology. The digital 3D model obtained was restored in a virtual environment and converted into an interactive 3D model that can be used for Romanian cultural heritage digital dissemination. 相似文献
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Rusu Mihai Lucian Marutoiu Constantin Sandu Ion Tita Dumitru Gogoasa Ioan Barbu Constantin-Horia Popescu Andreea 《平面色谱法杂志一现代薄层色谱法》2007,20(2):139-140
JPC – Journal of Planar Chromatography – Modern TLC - Samples of clove, nutmeg, and cinnamon have been extracted by maceration with ethanol for 24 h and with aqueous ethanol 48 h.... 相似文献
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Hernanz A Bratu I Marutoiu OF Marutoiu C Gavira-Vallejo JM Edwards HG 《Analytical and bioanalytical chemistry》2008,392(1-2):263-268
The external sixteenth century wall paintings of St. Dumitru's Church in Suceava (Romania) are suffering visually from deterioration. Fragments of these paintings spallated from the external wall have been studied by micro-Raman microscopy in order to elucidate possible causes of this process. Calcite and alpha-quartz are the components of the substratum indicating that the artists used the Roman fresco technique comprising a limewash putty. No organic binders have been detected in the substrate or pigment application. Amorphous carbon and goethite, alpha-FeOOH, have been identified in areas containing residues of grey and yellow pigments, respectively. Small amounts of gypsum have been detected in the grey areas which we attribute to special attention being given to surface preparation and pigment application in these areas. An abundance of sodium nitrate, nitratine, microcrystals have been observed on the surfaces of many fragments which suggests that a biodeterioration process originating from guano deposits could have been operating in these frescoes. 相似文献
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Kreibik Stefan Coman Virginia Marutoiu Constantin Mihailescu Gheorghe Pruneanu Stela 《平面色谱法杂志一现代薄层色谱法》2001,14(5):355-359
JPC – Journal of Planar Chromatography – Modern TLC - In normal TLC practice, migration of the mobile phase through the layer is controlled by capillary forces. Under these conditions... 相似文献
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Moise Maria-Ioana Marutoiu Constantin Badea Delia Nica Gavrila Cornelia-Anca Patroescu Constantin 《平面色谱法杂志一现代薄层色谱法》2004,17(2):147-148
JPC – Journal of Planar Chromatography – Modern TLC - Capsaicin was extracted from red hot pepper (Capsicum annuum) fruits and from commercial red hot pepper powder and separated on... 相似文献
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Marutoiu Constantin Gogoasa Ioan Oprean Ioan Marutoiu Olivia-Florena Moise Maria-Ioana Tigae Cristian Rada Maria 《平面色谱法杂志一现代薄层色谱法》2006,19(3):250-252
JPC – Journal of Planar Chromatography – Modern TLC - 相似文献
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Three sample preparation methods (wet grinding followed by centrifugation, ultrasonic-assisted extraction and microwave-assisted solvent extraction) for extracting ascorbic acid (AA) from parsley, dill and celery were evaluated. AA was extracted into 8% aqueous solutions of acetic acid, metaphosphoric acid and trichloroacetic acid, respectively. An efficient and precise high-performance liquid chromatography method was used for detecting AA. The best extraction technique was ultrasonic-assisted extraction, and acetic acid was the best extractant. A new and original pulse microwave-extraction procedure for AA extraction was also developed. Ascorbate from the plant extracts obtained was quantified and the linearity, precision, recovery, limit of detection (LOD) and limit of quantification (LOQ) were studied. LOD and LOQ were 0.2 and 0.22 mg/L for the established method, respectively. The mean recovery ranged from 90.7 to 102.3% with higher variation in the case of celery. Parsley contains the highest amount of ascorbic acid (264 mg AA/100 g of fresh plant), followed by dill (121 mg AA/100 g of fresh plant) and celery (103 mg AA/100 g of fresh plant). 相似文献
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