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(+/-)-4,12-Dihydroxy[2.2]paracyclophane [(+/-)-PHANOL] is readily prepared from [2.2]paracyclophane by an improved synthetic protocol. Enzymatic kinetic resolution of its bis-acetate proceeds with good enantioselection. Separation, hydrolysis, and recrystallization provides both enantiomers of PHANOL in high enantiopurity. 相似文献
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We obtain an existence theorem for monotone positive solutions of nonlinear second-order nonlinear differential equations via principal and nonprincipal solutions of the corresponding homogeneous equation. 相似文献
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The development of a scheme to treat two-dimensional electromagneticscattering by electrically large, perfectly conducting bodiesis described. It incorporates the effects of surface curvatureand non-local phenomena and has the potential to provide thebasis for a general technique yielding more accurate predictionsthan the widely used physical optics method. 相似文献
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Zoran Samard?ijaRID=""ID="" To whom correspondence should be addressed Darko Makovec Miran ?eh 《Mikrochimica acta》2000,132(2-4):383-386
Yttrium-doped BaTiO3 ceramics have been studied as a potential material for positive temperature coefficient resistors (PTCR). The mechanism of
Y incorporation into BaTiO3 plays an important role for displaying good electrical properties. Determination of the amount of yttrium in the BaTiO3 as well as microstructure characterization of the samples were performed using SEM, EDS and WDS analysis. An optimized trace
element WDS quantitative analysis was applied to determine elemental concentrations for Ba, Ti and Y in the samples as accurately
as possible. BaTiO3 and Y2O3 were used as standards. Analysis was undertaken using a JEOL JXA 840A electron probe microanalyzer. WDS X-ray intensity measurements
were performed under 20 kV, 50 nA beam current and 0.2% preset standard counting deviation (σc) using a PET crystal. Measured k-ratios were quantified by ZAF matrix correction. Average results of WDS quantitative analysis showed 20.17 ± 0.08 at % Ti,
19.95 ± 0.09 at % Ba, 0.22 ± 0.03 at % Y, and 59.66 at % O. The results suggest incorporation of yttrium in the BaTiO3 preferentially at the Ba-sites, however partial incorporation of Y at Ti-sites could not be excluded. 相似文献
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M.?Gabriel M.?St?hr R.?M?llerRID=""ID=""Corresponding author. 《Applied Physics A: Materials Science & Processing》2002,74(2):303-305
. The structure of thin 3,4,9,10-perylenetetracarb-oxylic-dianhydride (PTCDA) films on Cu(110) was studied by scanning tunnelling microscopy (STM) from submonolayer to monolayer coverage. While no long-range ordering was found after deposition at room temperature, the formation of a well-defined superstructure is observed after thermal annealing. It appears that the formation of the superstructure is driven by the interaction between the oxygen atoms of the PTCDA and the copper atoms of the substrate. While the distance between the molecules fits well to the atomic lattice of the Cu(110) surface along the [1[`([¯])]1[¯]\bar\Box1\Box]]0] direction, the mismatch along the [001] direction leads to a periodic buckling normal to the surface accompanied by a restructuring of the substrate. 相似文献
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Tomohiro?KurataEmail authorView authors OrcID profile Shigeto?Oda Hiroshi?Kawahira Hideaki?Haneishi 《Optical Review》2016,23(6):955-967
We have previously proposed an estimation method of intravascular oxygen saturation \(({\rm SO}_2)\) from the images obtained by sidestream dark-field (SDF) imaging (we call it SDF oximetry) and we investigated its fundamental characteristics by Monte Carlo simulation. In this paper, we propose a correction method for scattering by the tissue and performed experiments with turbid phantoms as well as Monte Carlo simulation experiments to investigate the influence of the tissue scattering in the SDF imaging. In the estimation method, we used modified extinction coefficients of hemoglobin called average extinction coefficients (AECs) to correct the influence from the bandwidth of the illumination sources, the imaging camera characteristics, and the tissue scattering. We estimate the scattering coefficient of the tissue from the maximum slope of pixel value profile along a line perpendicular to the blood vessel running direction in an SDF image and correct AECs using the scattering coefficient. To evaluate the proposed method, we developed a trial SDF probe to obtain three-band images by switching multicolor light-emitting diodes and obtained the image of turbid phantoms comprised of agar powder, fat emulsion, and bovine blood-filled glass tubes. As a result, we found that the increase of scattering by the phantom body brought about the decrease of the AECs. The experimental results showed that the use of suitable values for AECs led to more accurate \({\rm SO}_2\) estimation. We also confirmed the validity of the proposed correction method to improve the accuracy of the \({\rm SO}_2\) estimation. 相似文献