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Hermina Iulia Petkes Emese Gál Luiza Găină Mihaela Sabou Cornelia Majdik Luminiţa Silaghi-Dumitrescu 《Comptes Rendus Chimie》2014,17(10):1050-1056
The synthesis of new phenothiazinyl- and phenyl-nitrones under classical versus microwave heating conditions is described. Better yields were obtained under microwave irradiation in the condensation reactions of phenothiazyl-carbaldehyde with hydroxylamine derivatives. The structures of the new phenothiazinyl-nitrones were assigned on the basis of MS, FT–IR and NMR spectra. The new nitrones and some known phenyl-nitrones were screened for their antibacterial and antifungal activity against several Candida species, Gram negative bacteria, such as E. coli, Citrobacter spp, Morganella spp, Pseudomonas aeruginosa, Klebsiella pneumoniae (± ESBL), Proteus spp, Acinetobacter spp and the Gram positive bacterium Staphylococcus aureus, with moderate results. 相似文献
3.
Mihaela Badea Larisa Calu Mariana Carmen Chifiriuc Coralia Bleotu Alexandra Marin Sebastian Ion Gabriela Ioniţă Nicolae Stanică Luminiţa Măruţescu Veronica Lazăr Dana Marinescu Rodica Olar 《Journal of Thermal Analysis and Calorimetry》2014,118(2):1145-1157
A series of complexes of type [ML(CH3COO)(OH2)2] (M: Co, Ni; HL: 2-[(E)-1H-1,2,4-triazol-3-ylimino)methyl]phenol)) and [M2L2(CH3COO)2(OH2)n] (M: Cu, n = 2; M: Zn, n = 0) were synthesised by template condensation. The compounds were characterised with microanalytical, ESI–MS, IR, electronic, EPR spectra and magnetic data at room temperature. Based on the IR and ESI–MS spectra, a dinuclear structure with the acetate as bridge was proposed for Cu(II) and Zn(II) complexes. The dinuclear structure of Cu(II) complex is also consistent with both magnetic behaviour and EPR spectrum. The thermal analyses have evidenced processes as water elimination, acetate decomposition, as well as oxidative degradation of the Schiff base. The final decomposition product was the most stable metal oxide as indicated by powder X-ray diffraction. The cobalt and copper compounds exhibited a broad spectrum of antibacterial activity towards both planktonic and biofilm-embedded cells. The complexes exhibit a low cytotoxicity except for Cu(II) species that induces the early apoptosis for the HEp 2 cells. 相似文献
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Mihail?MeganEmail author Adina?Lumini?a?Sasu Bogdan?Sasu 《Integral Equations and Operator Theory》2004,50(4):489-504
The aim of this paper is to give necessary and sufficient conditions for pointwise and uniform exponential dichotomy of linear skew-product flows. We shall obtain that the pointwise exponential dichotomy of a linear skew-product flow is equivalent to the pointwise admissibility of the pair
As a consequence, we prove that a linear skew-product flow on
is uniformly exponentially dichotomic if and only if the pair
is uniformly admissible for . 相似文献
5.
Connections between uniform exponential expansiveness and complete admissibility of the pair
are studied. A discrete version for a theorem due to Van Minh, Räbiger and Schnaubelt is presented. Equivalent characterizations of Perron type for uniform exponential expansiveness of evolution families in terms of complete admissibility are given. 相似文献
6.
The purpose of this paper is to provide a new, unified and complete study for uniform dichotomy and exponential dichotomy
on the half-line. First we deduce conditions for the existence of uniform dichotomy, using classes of function spaces over
_+{\mathbb {R}_+} which are invariant under translations. After that, we obtain a classification of the main classes of function spaces over
\mathbb R+{\mathbb {R}_+}, in order to deduce necessary and sufficient conditions for the existence of exponential dichotomy, emphasizing on the main
technical qualitative properties of the underlying spaces. We motivate our approach by illustrative examples and show that
the main hypotheses cannot be dropped. We provide optimal methods regarding the input space in the study of dichotomy and
deduce as particular cases some interesting situations as well as several dichotomy results published in the past few years. 相似文献
7.
Vălean AM Gómez-Ruiz S Lönnecke P Silaghi-Dumitrescu I Silaghi-Dumitrescu L Hey-Hawkins E 《Inorganic chemistry》2008,47(23):11284-11293
The (organo)gallium compounds GaCl{(SC6H4-2-PPh2)-kappa2S,P}2 (1), Ga{(SC6H4-2-PPh2)-kappa2S,P}{(SC6H4-2-PPh2)-kappaS}2 (2), GaMe2{(SC6H4-2-PPh2)-kappa2S,P} (3), GatBu2{(SC6H4-2-PPh2)-kappa2S,P} (4), GatBu{(SC6H4-2-PPh2)-kappa2S,P}{(SC6H4-2-PPh2)-kappaS} (5), [GaMe2{(mu2-SC6H4-2-AsPh2)-kappaS}]2 (6), and GatBu{(SC6H4-2-AsPh2)-kappa2S,As}{(SC6H4-2-AsPh2)-kappaS} (7) were obtained from the reaction of 2-EPh2C6H4SH (E = P (PSH), As (AsSH)) with GaCl3 (1, 2) or GaR3 (R = Me, tBu; 3-7) in different molar ratios and under different reaction conditions. Compound 2 was also obtained from Li(PS) and GaCl3 (3.5:1). While a monomeric structure with a chelating phosphinoarylthiolato ligand is observed in GaMe2{(SC6H4-2-PPh2)-kappa2S,P} (3), a dimeric arsinoarylthiolato-bridged complex [GaMe2{(mu2-SC6H4-2-AsPh2)-kappaS}]2 (6) is obtained with the corresponding AsS- ligand. B3LYP/6-31G(d) calculations show that although the dimer is thermodynamically favored for both ligands, the formation of 3 is due to the combination of higher stability of the chelate compared with the monodentate phosphorus ligand and a higher barrier for the ring opening of the PS- than of the AsS- chelate. 相似文献
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Magdalena Lungu Ştefania Gavriliu Elena Enescu Ioana Ion Alexandra Brătulescu Grigore Mihăescu Luminiţa Măruţescu Mariana Carmen Chifiriuc 《Journal of nanoparticle research》2014,16(1):1-15
Recent studies have revealed the existence of liver cancer stem cells (CSCs). Therefore, there is an urgent need for new and effective treatment strategies specific to liver CSCs. In this work, the poly(d,l-lactide-coglycolide) nanoparticles containing paclitaxel were prepared by emulsification-solvent evaporation method. The nanoparticles decorated with anti-CD133 antibody, termed targeted nanoparticles, were prepared by carbodiimide chemistry for liver CSCs. The physicochemical characteristics of the nanoparticles (i.e., encapsulation efficiency, particle size distribution, morphology, and in vitro release) were investigated. Cellular uptake and accumulation in tumor tissue of nanoparticles were observed. To assess anti-tumor activity of nanoparticles in vitro and in vivo, cell survival assay and tumor regression study were carried out using liver cancer cell lines (Huh7 and HepG2) and their xenografts. Particle size of targeted nanoparticles was 429.26 ± 41.53 nm with zeta potential of ?11.2 mV. Targeted nanoparticles possessed spherical morphology and high encapsulation efficiency (87.53 ± 5.9 %). The accumulation of targeted nanoparticles depends on dual effects of passive and active targeting. Drug-loaded nanoparticles showed cytotoxicity on the tumor cells in vitro and in vivo. Targeted nanoparticles resulted in significant improvement in therapeutic response through selectively eliminating CD133 positive subpopulation. These results suggested that the novel nanoparticles could be a promising candidate with excellent therapeutic efficacy for targeting liver CSCs. 相似文献
9.
Adina Lumini?a Sasu 《Journal of Mathematical Analysis and Applications》2008,344(2):906-920
The aim of this paper is to provide a new approach concerning the characterization of exponential dichotomy of difference equations by means of admissible pair of sequence spaces. We classify the classes of input and output spaces, respectively, and deduce necessary and sufficient conditions for exponential dichotomy applicable for a large variety of systems. By an example we show that the obtained results are the most general in this topic. As an application we deduce a general lower bound for the dichotomy radius of difference equations in terms of input-output operators acting on sequence spaces which are invariant under translations. 相似文献
10.
We present necessary and sufficient conditions for uniform exponential expansiveness of discrete skew-product flows, in terms
of uniform complete admissibility of the pair (c
0(N, X), c
0(N, X)). We give discrete and continuous characterizations for uniform exponential expansiveness of linear skew-product flows,
using the uniform complete admissibility of the pairs (c
0(N, X), c
0(N, X)) and (C
0(R
+, X), C
0(R
+, X)), respectively. We generalize an expansiveness theorem due to Van Minh, R?biger and Schnaubelt, for the case of linear skew-product
flows.
Received August 10, 2001; in revised form June 25, 2002 相似文献