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E. I. Isaeva S. N. Kiryukhina V. V. Gorbunova 《Russian Journal of General Chemistry》2013,83(4):619-623
A procedure was developed for the synthesis of gold and silver nanoparticles in the presence of polyols like ethylene glycol, diethylene glycol, triethylene glycol, and 1,2-propylene glycol. Spectral characteristics of the obtained nanocomposites were mesured and kinetics of the formation of the colloidal phase was studied. The influence of the polyol nature and concentration on the photoinitiated formation of silver and gold nanoparticles was studied. The 1,2-propylene glycol is shown to exhibit maximal stabilizing effect. 相似文献
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G. I. Baram I. N. Azarova A. G. Gorshkov A. L. Vereshchagin B. Lang E. D. Kiryukhina 《Journal of Analytical Chemistry》2000,55(8):750-754
A technique for the direct preconcentration of bis(2-ethylhexyl) phthalate (DEHP) on a reversedphase analytical column was
proposed for the analysis of water samples by high-performance liquid chromatography (HPLC). A procedure for determining DEHP
in surface-water and atmospheric precipitations in the laboratory and in the field was developed (the limit of detection is
0.1 Μg/L, the limit of determination is 0.3 Μg/L, and the relative standard deviation is 20 or 6% at a DEHP concentration
of 0.3 or 10 Μg/L, respectively). The concentration levels of DEHP as a chemical tracer for the transfer and migration of
air and water masses were examined in Lake Baikal water and in the snow cover of the Baikal region. 相似文献
3.
L. D. Butakov É. G. Gal' G. F. Kiryukhina P. P. Krasnonosen'kikh N. A. Lashuk Yu. K. Pastukhov V. I. Tolmachev Z. Sh. Faskhutdinov V. A. Shushpanov 《Russian Physics Journal》1991,34(6):477-479
The radiation-measurement complex associated with the Sirius synchrotron has been operating in the Scientific-Research Institute of Nuclear Physics of the S. M. Kirov Polytechnic Institute in Tomsk since 1985. Research on meson physics, channeling of high-energy electrons in crystals, new types of radiation, and applications of synchrotron radiation is carried out in this complex. The renovation of the synchrotron presently under way will allow these problems to be studied more effectively.Translated from Izvestiya Vysshikh Uchebnykh Zavedenii, Fizika, No. 6, pp. 5–7, June, 1991. 相似文献
4.
Single crystals of Rb2NaAlF6, the Rb analogue of the mineral elpasolite, are obtained in the NaF-Rb2CO3-Al2O3-Rb3PO4-H2O system under hydrothermal conditions, and their structure is determined by X-ray diffraction (R = 0.0188): a = 8.3087(1) Å, space group $Fm\bar 3m$ , Z = 4, and ρcalcd = 3.88 g/cm3. The hypothesis that Rb elpasolite exists in nature in late associations of pegmatites enriched in rubidium is proposed. 相似文献
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Rezchikova T. V. Kurkin E. N. Troitskii V. N. Kiryukhina L. S. Ivanov A. V. 《Russian Journal of Applied Chemistry》2001,74(12):2035-2039
The electrolytic deposition of composite copper-based coatings with an ultradispersed phase(TiN or Al2O3) was studied. Conditions for obtaining coatings with the maximum microhardness were determined. 相似文献
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T. V. Rezchikova E. N. Kurkin L. S. Kiryukhina E. N. Kabachkov 《Russian Journal of Applied Chemistry》2010,83(4):583-587
The photocatalytic activity of crystalline titania nanopowders synthesized in a stream of ultrahigh-frequency discharge oxygen-containing
low-temperature plasma was assessed. To this end, oxidation of an organic dye was carried out in UV-irradiated aqueous suspensions
of TiO2 at different concentrations and varied irradiation times. 相似文献
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The crystal structure of new manganese potassium copper vanadate KCuMn3(VO4)3, which was prepared by the hydrothermal synthesis in the K2CO3–CuO–MnCl2–V2O5–H2O system, was studied by X-ray diffraction (R = 0.0355): a = 12.396(1) Å, b = 12.944(1) Å, c = 6.9786(5) Å, β = 112.723(1)°, sp. gr. C2/c, Z = 4, ρcalc = 3.938 g/cm3. A comparative analysis of the crystal-chemical features of the new representative of the alluaudite family and related structures of minerals and synthetic phosphates, arsenates, and vanadates of the general formula A(1)A(1)′A(1)″A(2)A(2)′M(1)M(2)2(TO4)3 (where A are sites in the channels of the framework composed of MО6 octahedra and TО4 tetrahedra) was performed. A classification of these structures into subgroups according to the occupancy of A sites is suggested. 相似文献
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