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Luis Alvarez‐Thon Carlos Bustos Katherina Espinoza‐Santibaez Maria Teresa Garland Ricardo Baggio 《Acta Crystallographica. Section C, Structural Chemistry》2013,69(10):1200-1204
The title compound, C17H11F5N4O, is described and compared with two closely related analogues in the literature. There are two independent molecules in the asymmetric unit, linked by N—H...O hydrogen bonds and π–π interactions into dimeric entities, presenting a noticeable noncrystallographic C2 symmetry. These dimers are in turn linked by a medium‐strength type‐I C—F...F—C interaction into elongated tetramers. Much weaker C—H...F contacts link the tetramers into broad two‐dimensional substructures parallel to (101). 相似文献
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Fully printed flexible audio system on the basis of low‐voltage polymeric organic field effect transistors with three layer dielectric
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Georg C. Schmidt Daniel Höft Katherina Haase Maxi Bellmann Bahman Kheradmand‐Boroujeni Tomi Hassinen Henrik Sandberg Frank Ellinger Arved C. Hübler 《Journal of Polymer Science.Polymer Physics》2015,53(20):1409-1415
Fully mass printed, flexible and truly polymeric organic field effect transistors consisting of a three layer dielectric made of CYTOP (low‐k), PVA (intermediate) and P(VDF‐TrFE‐CTFE)(high‐k) are introduced. Gravure‐, flexo‐and screen printing were selected as highly productive manufacturing technologies. These OFETs work at strongly reduced voltages and show high field effect mobility (µ = 0.2 cm2/Vs) and remarkable good bias stress stability at very high current density (50 µA/mm). Fully printed OFETs are used for the realization of ring oscillators working in the kHz regime at reduced supply voltage (10 V). In combination with printed fully polymeric piezoelectric loudspeakers, this work shows for the first time fully printed flexible audio systems. © 2015 Wiley Periodicals, Inc. J. Polym. Sci., Part B: Polym. Phys. 2015 , 53, 1409–1415 相似文献
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Igor V. Zatovsky Katherina V. Terebilenko Vyacheslav N. Baumer 《Journal of solid state chemistry》2006,179(11):3550-3555
A new potassium bismuth phosphate-molybdate K2Bi(PO4)(MoO4) has been synthesized by the flux method and characterized by single-crystal and powder X-ray diffraction, IR spectroscopic studies. The compound crystallizes in the orthorhombic system with the space group Ibca and the cell parameters: a=19.7037(10), b=12.4752(10), c=7.0261(10). This phase exhibits an original layered structure, in which the [Bi(PO4)(MoO4)]∞ layers consist of [Bi2Mo2O18]∞ chains linked through single PO4 tetrahedra. The K+ cations interleaved between these layers exhibit a monocapped distorted cubic coordination. 相似文献
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Rühl T Volke D Stembera K Hatanaka Y Hennig H Schumer F Welzel P 《Chemical communications (Cambridge, England)》2002,(15):1630-1631
The photolytic decomposition of trifunctional carbene generating photoaffinity probes in methanolic solution was studied, a cleavage reaction with butylamine in water, the conjugation with a ligand (moenomycin), and experiments that demonstrate that the fully armed probes interact with penicillin-binding protein 1b. 相似文献
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Katherina Tsobkallo Valeria Vasilieva Masaki Kakiage Hiroki Uehara 《Journal of Macromolecular Science: Physics》2013,52(3):407-415
A series of reactor powders of ultrahigh molecular weight (UHMW) polyethylenes with different morphology was melted at 160°C for 5 min and cooled in ice water. Low‐frequency Raman spectroscopy was used to characterize the straight‐chain‐segment (SCS) length distribution of both initial and melt‐crystallized materials. A bimodal SCS length distribution was found in the melt‐crystallized sample originated from the reactor powder with a very tenuous amorphous phase. In other samples recrystallized from powders with more ordered structure, the SCS length distribution was unimodal and approximately identical. The result is explained in terms of perfection of lamellar crystals formed under limited time and thermal conditions from differently organized initial structure. 相似文献
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Dr. Sandra Künzler Saskia Rathjen Katherina Rüger Marie S. Würdemann Marcel Wernke Patrik Tholen Corinna Girschik Dr. Marc Schmidtmann Prof. Dr. Yannick Landais Prof. Dr. Thomas Müller 《Chemistry (Weinheim an der Bergstrasse, Germany)》2020,26(69):16441-16449
Cyclic silylated chalconium borates 13 [B(C6F5)4] and 14 [B(C6F5)4] with peri-acenaphthyl and peri-naphthyl skeletons were synthesized from unsymmetrically substituted silanes 3 , 4 , 6 , 7 , 9 and 10 using the standard Corey protocol (Chalcogen Ch=O, S, Se, Te). The configuration at the chalcogen atom is trigonal pyramidal for Ch=S, Se, Te, leading to the formation of cis- and trans-isomers in the case of phenylmethylsilyl cations. With the bulkier tert-butyl group at silicon, the configuration at the chalcogen atoms is predetermined to give almost exclusively the trans-configurated cyclic silylchalconium ions. The barriers for the inversion of the configuration at the sulfur atoms of sulfonium ions 13 c and 14 a are substantial (72–74 kJ mol−1) as shown by variable temperature NMR spectroscopy. The neighboring group effect of the thiophenyl substituent is sufficiently strong to preserve chiral information at the silicon atom at low temperatures. 相似文献
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The Finite Element Method (FEM) and the Boundary Element Method (BEM) are the most used numerical tools for solid mechanics analysis. Each one of these methods has advantages and drawbacks in different cases. In order to take advantage of both methods, a nonoverlapping domain decomposition method FEM - BEM in elastodynamics is presented. The domain is divided in two subdomains and each one of them is analyzed separately and only the interface information is exchanged. An iterative Neumann - Dirchlet algorithm with relaxation is used, to get continuity and the equilibrium conditions at the interface. The FEM time integration is carried out using the Newmark's method and the BEM approach in time domain is based in the Convolution Quadrature Method developed by Lubich. Numerical examples are presented to show agreement with other available numerical results. (© 2011 Wiley-VCH Verlag GmbH & Co. KGaA, Weinheim) 相似文献
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