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Simon Dochain Jean-Boris Nshimyumuremyi Damien F. Dewez Jean-François Body Benjamin Elias Michael L. Singleton István E. Markó 《Tetrahedron》2019,75(15):2280-2283
Okadaic acid, a potent and selective inhibitor of Protein Phosphatases 1 and 2A (PP1 and PP2A), is widely used as a probe for various biochemical processes. We describe herein two innovative methods for the synthesis of the terminal C28–C38 fragment of the natural polyether. Suárez photochemical oxidative cyclization and electrochemical oxidation of malonates to their ketals equivalents have been successfully applied for the assembly of the key spiroketal core. 相似文献
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