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A procedure was proposed for electrochemical reduction of 2,5-dichloronitrobenzene to 2,5-dichloroaniline in aqueous-ethanolic solution of sulfuric acid. The procedure for preparing 2,5-dichloroanilinium sulfate was optimized. The influence exerted by the cathode material, nature and amount of the organic solvent, sulfuric acid concentration, and electrolysis temperature on the yield and quality of the target product was discussed.  相似文献   
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Electrochemical oxidation of chlorinated alkenylanisoles in anhydrous methanol was studied.  相似文献   
3.
Improvement of a Process for Synthesis of Thioglycolic Acid   总被引:1,自引:0,他引:1  
An environmentally clean process was proposed for synthesis of thioglycolic acid by condensation of monochloroacetic acid with sodium disulfide, followed by electrochemical reduction of the resulting mixture.  相似文献   
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