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1.
2.
3-(4-Phenyl) benzoyl propionic acid was used as the starting material for the synthesisof furanones (2), pyrrolinones (5), pyridazinones (7), benzoxazinones (8) and quinazolinones (9-11). The behaviour of the derivatives of furanones and benzoxazinones toward different nucleophiles is reported.  相似文献   
3.
YBa2Cu3-xVxO7-y(x=0, 0.1, 0.2, 0.3, 0.4, 0.5 and 0.6) superconductors have been prepared. X-ray diffraction shows that the system remains orthorhombic for all compositions studied, but for x > 0.4 V2O5 was detected as an impurity phase. Substitution of V5+ for Cu2+ occurs in the Cu(2) sites on the Cu(2)-O planes. The introduction of the high valence element, vanadium, produces the extra free-electrons. These electrons recombine with the positive carrier of the system. It makes depression of the mobility and the Hall number of YBa2Cu3-xVxO7-v and also results in a depression of TC.  相似文献   
4.
Abstract— Chemiluminescence of the Eu(II)/Eu(III)-adenine nucleotide-H2O2 system and fluorescence of the Eu(III)-adenosine triphosphate system have been investigated. The spectral distribution of the chemiluminescence emission has shown an occurrence of three main bands (Λ=470–480,590–620 and ca. 700 nm). The energy transfer process from the adenosine triphosphate molecules to the Eu(III) ions has been observed in the fluorescence spectrum. The examined chemiluminescence and fluorescence spectra show that these both kinds of emission originate from the 5 D ***τ7F*** ( n =1–4) transitions in the Eu(III) ions.  相似文献   
5.
针对纤维材料变温环境力学性能测试的需要,在华中科技大学研制的纤维材料试验机的基础上引入了温控装置,从而实现纤维材料在高低温环境下的力学性能测试。采用该装置对不同直径微米铜丝在不同温度、不同拉伸速率条件下的力学性能开展实验研究,测试结果表明弹性模量和抗拉强度随温度的降低而线性增加,屈服强度的变化不太明显。另外,低温环境下微米铜丝的力学性能表现出与其直径相关的尺度效应,而这一现象在常温下一直没有观测到。最后,还研究了拉伸速率对微米铜丝的力学性能影响,结果表明,在现有装置的许用范围之内,拉伸速率对其力学性能的影响不大。  相似文献   
6.
We consider two-stage pure integer programs with discretely distributed stochastic right-hand sides. We present an equivalent superadditive dual formulation that uses the value functions in both stages. We give two algorithms for finding the value functions. To solve the reformulation after obtaining the value functions, we develop a global branch-and-bound approach and a level-set approach to find an optimal tender. We show that our method can solve randomly generated instances whose extensive forms are several orders of magnitude larger than the extensive forms of those instances found in the literature. This work is supported by National Science Foundation grants DMI-0217190 and DMI-0355433.  相似文献   
7.
This paper presents an entourage-like theory of quasi-uniformities for frames. The theory comprises the theory of uniformities for frames as well as the classical theory of quasi-uniformities for spaces.  相似文献   
8.

Background  

Urokinase-type plasminogen activator (uPA) plays a major role in extracellular proteolytic events associated with tumor cell growth, migration and angiogenesis. Consequently, uPA is an attractive target for the development of small molecule active site inhibitors. Most of the recent drug development programs aimed at nonpeptidic inhibitors targeted at uPA have focused on arginino mimetics containing amidine or guanidine functional groups attached to aromatic or heterocyclic scaffolds. There is a general problem of limited bioavailability of these charged inhibitors. In the present study, uPA inhibitors were designed on an isocoumarin scaffold containing uncharged substituents.  相似文献   
9.
A classical result in the theory of uniform spaces is that any topological space with a base of clopen sets admits a uniformity with a transitive base and the uniform topology of such a space has a base of clopen sets. This paper presents a pointfree generalization of this, both to uniform and quasi-uniform frames, together with various properties concerning total boundedness, compactifications and completions.  相似文献   
10.
This paper explores the potential benefit of using tuned parameter settings for integer programming instances. Three metrics are considered for selecting parameters: Time-to-Optimality, Proven-Gap and Best-Integer-Solution. Good parameter settings for each metric are found using the open-source software tool Selection Tool for Optimization Parameters. Computational tests are presented using CPLEX solver (version 9.0) on MIPLIB test instances, showing substantial improvements over the default parameter setting. Although the benefit of a tuned parameter setting on an individual instance is outweighed by the cost of identifying the tuned setting, these results indicate that substantial benefit may be achieved in cases where the cost of tuning parameter settings is justified.  相似文献   
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