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1.
Historians have always seen jabr (restoration) and muqābala (confrontation) as technical terms for specific operations in Arabic algebra. This assumption clashes with the fact that the words were used in a variety of contexts. By examining the different uses of jabr, muqābala, ikmāl (completion), and radd (returning) in the worked-out problems of several medieval mathematics texts, we show that they are really nontechnical words used to name the immediate goals of particular steps. We also find that the phrase al-jabr wa'l-muqābala was first used within the solutions of problems to mean al-jabr and/or al-muqābala, and from there it became the name of the art of algebra.  相似文献   
2.
Hollow silica microspheres(HSMSs) have been successfully fabricated via a facile hydrothermal route using D-glucose as the sacrificial template and sodium silicate powder as the silica precursor.The resulting silica hollow particles were characterized by scanning electron microscopy(SEM),transmission electron microscopy(TEM),X-ray diffraction(XRD),and infrared spectroscopy(IR).The surface area was determined using the BET method.SEM and TEM images exhibited micro-sized silica hollow particles with a size of ~1.5μm.  相似文献   
3.
The end‐to‐end cyclization of telechelic polyisobutylenes (PIB's) toward cyclic polyisobutylenes is reported, using either ring‐closing metathesis (RCM) or the azide/alkyne‐“click”‐reaction. The first approach uses bisallyl‐telchelic PIB's (Mn = 1650, 3680, 9770 g mol?1) and Grubbs 1st‐, 2nd‐, and 3rd‐generation catalyst leading to cyclic PIB's in 60–80% yield, with narrow polydispersities (Mw/Mn = 1.25). Azide/alkyne‐“click”‐reactions of bisalkyne‐telechelic PIB's (Mn = 3840 and 9820 g mol?1) with excess of 1,11‐diazido‐undecane leads to the formation of mixtures of linear/cyclic PIB's under formation of oligomeric cycles. Subsequent reaction of the residual azide‐moieties in the linear PIB's with excess of alkyne‐telechelic PEO enables the chromatographic removal of the resulting linear PEO‐PIB‐block copolymers by column chromatography. Thus pure cyclic PIB's can be obtained using this double‐“click”‐method, devoid of linear contaminants. © 2009 Wiley Periodicals, Inc. J Polym Sci Part A: Polym Chem 48: 671–680, 2010  相似文献   
4.
A multi-period stochastic planning model has been developed and implemented for a supply chain network of a petroleum organization operating in an oil producing country under uncertain market conditions. The proposed supply chain network consists of all activities related to crude oil production, processing and distribution. Uncertainties were introduced in market demands and prices. A deterministic optimization model was first developed and tested. The impact of uncertainty on the supply chain was studied by performing a sensitivity analysis in which ±20% deviations were introduced in market demands and prices of different commodities. A stochastic formulation was then proposed, which is based on the two-stage problem with finite number of realizations. The proposed stochastic programming approach proved to be quite effective in developing resilient production plans in light of high degree of uncertainty in market conditions. The anticipated production plans have a considerably lower expected value of perfect information (EVPI). The main conclusion of this study is that for an oil producing country with oil processing capabilities, the impact of economic uncertainties may be tolerated by an appropriate balance between crude exports and processing capacities.  相似文献   
5.
Changes in mechanical and physical properties of polyurethane thermoplastic during aging at 70 °C and 90 °C were investigated. The loss weight response was analyzed by gravimetric measurements under these temperatures. Changes in appearance and morphology of TPU after thermal aging were revealed by optical microscopy. The prolongation of the thermal exposure time, up to 270 days, leads to a progressive increase in tensile strength. In fact, elastic modulus and stress at 200% of strain were increased with thermal exposure time. These results can be explained by the increase of thermal stability due to the increase of material rigidity and the decrease in chain mobility. The evolution of the mechanical properties from tensile tests seems to be well correlated to the creep behavior. Finally, Scanning Electron Microscopy (SEM) revealed the modification of TPU morphology fracture surface after thermal aging.  相似文献   
6.
7.
In this work, a new hybrid material (C5H6N2Cl)2[FeCl4].Cl abbreviated (CAP)2[FeCl4].Cl was prepared using room temperature slow evaporation technique. The X-ray diffraction analysis revealed that the compound is crystallized in the centrosymmetric space group P21/c of the monoclinic system. The crystallographic network consists of an Fe(III) ion located on an inversion center and coordinated by four chlorine, isolated Cl and two (CAP)+ protonated cations linked by N–H...Cl and C–H...Cl hydrogen bonds to form a zero-dimensional network. Hirshfeld surface analysis was used to analyze intermolecular interactions present in the crystal structure. The vibrational properties were inspected by means of Infra-Red absorption and Raman diffusion spectroscopy techniques. In addition, theoretical calculations based on the DFT/B3LYP/LanL2DZ method and the time-dependent density functional theory (TD–DFT) were performed in order to gain more information and help in the examination of over-all properties of the title compound. Good and interesting experimental findings were presented and good consistency was found with the calculated results.  相似文献   
8.
Cycloaddition of the 1‐aza‐2‐azoniaallenes 3 with p‐cyanobenzyl chlorides afforded, after spontaneous rearrangement, the 1,5‐dialkyl‐3‐[4‐chloromethyl)phenyl]‐1H‐[1,2,4]‐triazoles 6 . A series of 1,5‐dialkyl‐1H‐[1,2,4]‐triazol‐3‐yl)benzyl‐piperazines 7 and 8 were prepared from direct condensation of 6 with piperazine and N‐methylpiperazine, respectively. The structures of the newly synthesized products were identified by 2D NMR spectroscopy. © 2005 Wiley Periodicals, Inc. Heteroatom Chem 16:28–32, 2005; Published online in Wiley InterScience (www.interscience.wiley.com). DOI 10.1002/hc.20061  相似文献   
9.
Applied Biochemistry and Biotechnology - The present study aims to evaluate the antidepressant efficacy of curcumin nanoparticles on rat model of depression induced by reserpine. Rats were divided...  相似文献   
10.
We introduce a new class of distributions and provide a comprehensive treatment of its mathematical properties. The maximum likelihood method is discussed to estimate the parameters of the new model by means of Monte-Carlo simulation study. The heteroscedastic regression models with long-term survival are introduced to model data sets with the non homogeneity of the error variances in the presence of cured individuals. The potentiality of the proposed models is illustrated by means of four real data sets.  相似文献   
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