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本文利用荧光光谱和园二色光谱了新开花粉蛋白的盐酸胍去折叠过程。结果显示:新开花粉蛋白的盐酸胍去折叠是一个只包含天然蛋白和变性终态的二态过程,与已经报道的天花粉蛋白的盐酸胍去折叠的过程不同。 相似文献
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Review of nanofluids for heat transfer applications 总被引:2,自引:0,他引:2
Saeid Vafaei 《中国颗粒学报》2009,7(2)
Research on nanofluids has progressed rapidly since its enhanced thermal conductivity was first repotted about a decade ago,though much controversy and inconsistency have been reported,and insufficient understanding of the formulation and mechanism of nanofluids further limits their applications.This work presents a critical review of research on heat transfer applications of nanofluids with the aim of identifying the limiting factors so as to push forward their further development. 相似文献
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Vijay NS Bhagawati-Prasad Evy De Leenheer Nadine P Keefe Lorna A Ryan Jennifer Carlring Andrew W Heath 《Journal of immune based therapies and vaccines》2010,8(1):1
Active vaccination can be effective as a post-exposure prophylaxis, but the rapidity of the immune response induced, relative
to the incubation time of the pathogen, is critical. We show here that CD40mAb conjugated to antigen induces a more rapid
specific antibody response than currently used immunological adjuvants, alum and monophosphoryl lipid A™. 相似文献
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Nura Suleiman Gwaram Hamid Khaledi Hapipah Mohd Ali Marilyn M. Olmstead 《Acta Crystallographica. Section C, Structural Chemistry》2011,67(1):o6-o9
The title compound, C4H6N4O·H2O, crystallized simultaneously as a triclinic and a monoclinic polymorph from an aqueous solution of 2,4‐diaminopyrimidin‐6‐ol. Previously, an orthorhombic polymorph was isolated under the same experimental conditions. The molecular geometric parameters in the two present polymorphs and the previously reported orthorhombic polymorph are similar, but the structures differ in the details of their crystal packing. In the triclinic system, the diaminopyrimidinone molecules are connected to one another via N—H...O and N—H...N hydrogen bonding to form infinite chains in the [011] direction. The chains are further hydrogen bonded to the water molecules, resulting in a three‐dimensional network. In the monoclinic system, the diaminopyrimidinone molecules are hydrogen bonded together into two‐dimensional networks parallel to the bc plane. The water molecules link the planes to form a three‐dimensional polymeric structure. 相似文献
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Arun Kumar NS Prashanth Shivappa Adarakatti Ashoka S Pandurangappa Malingappa 《Journal of Solid State Electrochemistry》2018,22(6):1711-1719
A simple strategy has been proposed to quantify Zn2+ ions using CeO2 nanoparticle-modified glassy carbon electrode. The CeO2 nanoparticles were prepared by sucrose-nitrate decomposition method, and it was characterized by X-ray diffraction (XRD), FT-IR, TEM, and surface area analyzer. The synthesized CeO2 nanoparticles were used as modifier molecules as a thin film on glassy carbon electrode (GCE) in the trace level quantification of Zn2+ by using cyclic voltammetry (CV) and differential pulse anodic stripping voltammetry (DPASV) techniques. The fabricated sensor exhibited a good analytical response towards Zn2+ ions. The modified electrode showed a wide linearity in the concentration range 20–380 μg L?1 with a limit of detection 0.36 μg L?1. The proposed electrochemical sensor was successfully applied to trace level Zn2+ quantification from real sample matrices. 相似文献
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Gwaram NS Ali HM Khaledi H Abdulla MA Hadi AH Lin TK Ching CL Ooi CL 《Molecules (Basel, Switzerland)》2012,17(5):5952-5971
A series of Schiff bases derived from 2-acetylpyridne and their metal complexes were characterized by elemental analysis, NMR, FT-IR and UV-Vis spectral studies. The complexes were screened for anti-bacterial activity against Methicillin-resistant Staphylococcus aureus (MRSA), Acinetobacter baumanni (AC), Klebsiella pneumonie (KB) and Pseudomonas aeruginosa (PA) using the disc diffusion and micro broth dilution assays. Based on the overall results, the complexes showed the highest activities against MRSA while a weak antibacterial activity was observed against A. baumanii and P. aeruginosa. 相似文献
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FTIR光谱法研究天花粉蛋白的热去折叠过程 总被引:4,自引:0,他引:4
本文利用FTIR光谱技术和计算机辅助解析技术(二阶导数、去卷积和曲线拟合)研究了天花粉蛋白的热诱导去折叠过程。结果表明:在25~85℃温度范围内,天花粉蛋白的热去折叠是一个不可逆的分子间聚集的过程;二级结构随温度的变化暗示了折叠中间体的存在。 相似文献
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Gwaram NS Ali HM Abdulla MA Buckle MJ Sukumaran SD Chung LY Othman R Alhadi AA Yehye WA Hadi AH Hassandarvish P Khaledi H Abdelwahab SI 《Molecules (Basel, Switzerland)》2012,17(3):2408-2427
Alzheimer's disease (AD) is the most common form of dementia among older people and the pathogenesis of this disease is associated with oxidative stress. Acetylcholinesterase inhibitors with antioxidant activities are considered potential treatments for AD. Some novel ketone derivatives of gallic hydrazide-derived Schiff bases were synthesized and examined for their antioxidant activities and in vitro and in silico acetyl cholinesterase inhibition. The compounds were characterized using spectroscopy and X-ray crystallography. The ferric reducing antioxidant power (FRAP) and 2,2-diphenyl-1-picrylhydrazyl (DPPH) assays revealed that all the compounds have strong antioxidant activities. N-(1-(5-bromo-2-hydroxyphenyl)-ethylidene)-3,4,5-trihydroxybenzohydrazide (2) was the most potent inhibitor of human acetyl cholinesterase, giving an inhibition rate of 77% at 100 μM. Molecular docking simulation of the ligand-enzyme complex suggested that the ligand may be positioned in the enzyme's active-site gorge, interacting with residues in the peripheral anionic subsite (PAS) and acyl binding pocket (ABP). The current work warrants further preclinical studies to assess the potential for these novel compounds for the treatment of AD. 相似文献
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