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1.
A method of comparing glass fragments of potential application to forensic sicence has been developed and evaluated. A representative
sample of window glass from England and Wales has been collected and analysed for about 25 elements. An automated radiochemical
separation followed by gamma-spectroscopy was used in order to determine the concentration of the maximum number of elements.
Frequency distributions of the elemental concentration are shown and used to assess the discrimination of the technique and
compare it with the measurement of refractive index. A few simulated cases have been included to demonstrate the possible
application to forensic science problems. 相似文献
2.
ABSTRACT Copolymers of 1,5-dioxepan-2-one (DXO) and e-caprolactone (?-CL), δ-valerolactone (δ-VL) or L-lactide (LLA) have been synthesized and characterized. High molecular weight copolymers were obtained using stannous-2-ethyl hexanoate as catalyst in bulk. Reactivity ratios for the copolymerization of DXO and δ-VL were determined at 110°C as rVL=0.5 and rDXO=2.3. At high conversion, depolymerization of δ-VL occurred, resulting in lower molecular weight and variations in the copolymer composition. Physical properties, such as crystallinity and melting temperature of the DXO-copolymers proved to be strongly dependent on the choice of comonomer and on the molar composition of the copolymers. DXO appears to be incorporated into the poly-?-caprolactone (PCL) crystals and to some extent into the poly-δ-valerolactone (PVL) crystals, resulting in a more gradual decrease in crystallinity with increasing amount of DXO. 相似文献
3.
A Mukherjee M Dasgupta DJ Hinde CR Morton AC Berriman RD Butt JO Newton H Timmers 《Pramana》2001,57(1):195-198
Fusion cross-sections for the 7Li + 12C reaction have been measured at energies above the Coulomb barrier by the direct detection of evaporation residues. The heavy
evaporation residues with energies below 3 MeV could not be separated out from the α-particles in the spectrum and hence their
contribution was estimated using statistical model calculations. The present work indicates that suppression of fusion cross-sections
due to the breakup of 7Li may not be significant for 7Li + 12C reaction at energies around the barrier. 相似文献
4.
RD Harris WS Baker Van Stipdonk MJ RM Crooks EA Schweikert 《Rapid communications in mass spectrometry : RCM》1999,13(14):1374-1380
A suite of keV polyatomic or 'cluster' projectiles was used to bombard unoxidized and oxidized self-assembled monolayer surfaces. Negative secondary ion yields, collected at the limit of single ion impacts, were measured and compared for both molecular and fragment ions. In contrast to targets that are orders of magnitude thicker than the penetration range of the primary ions, secondary ion yields from polyatomic projectile impacts on self-assembled monolayers show little to no enhancement when compared with monatomic projectiles at the same velocity. This unusual trend is most likely due to the structural arrangement and bonding characteristics of the monolayer molecules with the Au(111). Copyright 1999 John Wiley & Sons, Ltd. 相似文献
5.
K. A. Goode 《Chromatographia》1977,10(9):521-528
Summary A simple in-situ fractionation technique, offering several advantages over conventional heart-cutting techniques, is described in which discrete, controlled fractions of effluent from one chromatographic column are transferred sequentially to a second column having diffierent selectively characteristics. Prior to transfer, solutes are stored in-situ on the first column, so that each fraction transferred can be analysed separatley on the second column. In-situ storage and fractionation is achieved using a simple flow-switching arrangement that can be installed in any routine chromatograph without extensive instrument modification. The gas chromatographic determination of aromatics in fuels having final boiling points up to 400° C is used to illustrate the technique. Its potential usefulness in gas chromatography and its possible uses in liquid chromatography are discussed. 相似文献
6.
A precise constant-current coulometer is described suitable for manual or automatic coulometric titrations. The apparatus provides II increments of current in the range 250 μA to 200 mA and gives a standard deviation of better than 30 p.p.m. for the total measurement of coulombs. 相似文献
7.
Carter EB Culver SL Fox PA Goode RD Ntai I Tickell MD Traylor RK Hoffman NW Davis JH 《Chemical communications (Cambridge, England)》2004,(6):630-631
The anions of the sweeteners saccharin and acesulfame form ionic liquids when paired with a variety of organic cations. 相似文献
8.
Powell has shown that the cyclic coordinate method with exact searches may not converge to a stationary point. In this note we consider a more general class of algorithms for unconstrained minimization, and establish their convergence under the assumption that the objective function has a unique minimum along any line. 相似文献
9.
W. E. Garner C. A. Waters H. Lüers C. W. G. Hetterschy Aristides Kanitz F. Liebert A. Uhl W. Kestranek J. M. Kolthoff B. D. Hartong J. Pinkhof E. Biilmann A. Klit F. Haber Z. Klemensiewicz W. S. Hughes A. L. v. Steiger W. E. L. Brown Phyllis M. T. Kerridge Th. Arnd W. Siemers K. H. Goode W. D. Treadwell J. W. Williams Th. A. Whitenack U. Ehrhardt und E. Linde 《Fresenius' Journal of Analytical Chemistry》1930,80(5-6):203-213
Ohne Zusammenfassung 相似文献
10.