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Ishmuratov G. Yu. Yakovleva M. P. Galyautdinova A. V. Muslukhov R. R. Tolstikov G. A. 《Russian Chemical Bulletin》2003,52(3):740-744
A new procedure was developed for the synthesis of racemic analogs of 1,5-dimethyl-branched insect pheromones based on monoalkylation of ethyl acetoacetate with 1-acetoxy-5-bromo-3-methylpentane produced upon decyclization of 4-methyltetrahydropyran. 相似文献
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E. N. Klimovitskii A. N. Galyautdinova A. B. Dobrynin V. V. Gavrilov S. G. Gnevashev R. M. Vafina I. A. Litvinov Yu. G. Shtyrlin 《Russian Journal of Organic Chemistry》2009,45(10):1442-1444
(Z)-But-2-ene-1,4-dithiol was found to undergo isomerization into the E isomer. Condensation of (Z)- and (E)-but-2-ene-1,4-dithiols with acetaldehyde gave isomeric fourteen-membered bis-dithioacetals whose structure was determined
by X-ray analysis. 相似文献
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Davletbaeva I. M. Gumerov A. M. Galyautdinova A. F. Davletbaev R. S. Krasil’nikova O. K. 《Russian Journal of Applied Chemistry》2011,84(9):1587-1590
Russian Journal of Applied Chemistry - Polymers prepared from a polyether, 2,4-toluene diisocyanate, and octamethylcyclotetrasiloxane were studied using thermomechanical analysis, mechanical tests,... 相似文献
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A. N. Galyautdinova R. M. Vafina O. N. Kataeva O. A. Lodochnikova S. G. Gnevashev O. I. Gnezdilov V. V. Gavrilov Yu. G. Shtyrlin G. A. Chmutova E. N. Klimovitskii 《Russian Journal of Organic Chemistry》2010,46(2):246-251
By oxidation of (Z)-4,7-dihydro-1,3-dithiepines with meta-chloroperbenzoic acid the corresponding 4,7-dihydro-1λ4,3-dithiepine 1-oxides were synthesized in ∼85% yield. A complete assignment of signals in the 1H and 13C NMR spectra of the compounds obtained was established. According to XRD analysis the seven-membered heterocycles crystallized
in conformations chair or boat. The calculations by DFT method in the B3LYP/6-31G(d,p) version showed the possibility of conformational equilibrium of these forms in the gas phase. 相似文献
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G. Yu. Ishmuratov M. P. Yakovleva A. V. Galyautdinova L. V. Faifer R. Ya. Kharisov V. V. Zorin G. A. Tolstikov 《Chemistry of Natural Compounds》2001,37(5):486-489
A universal approach to the synthesis of juvenoid hydroprene and methoprene was developed on the basis of monoalkylation of acetoacetate by 1-acetoxy-5-bromo-3-methylpentane, the product of acidic decyclization of 4-methyltetrahydropyran. 相似文献
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G. Yu. Ismuratov M. P. Yakovleva A. V. Galyautdinova G. A. Tolstikov 《Chemistry of Natural Compounds》2003,39(1):31-33
Optically active (4R,8RS)-dimethyldecanal, an analog of the aggregation pheromone of the flour beetles Tribolium confusum and T. Castaneum, and (4R)-methylnonan-1-ol, the sex pheromone of the yellow mealworm Tenebrio molitor L., are synthesized using ozonolytic transformation of (6R,10)-dimethyl-9-undecen-2-one to (6R)-methyl-9-hydroxynonan-2-one in the key step. The starting compound is available as enantiomerically enriched (ee ~50%) (S)-(+)-3,7-dimethyl-1,6-octadiene. 相似文献
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G. Yu. Ishmuratov R. Ya. Kharisov M. P. Yakovleva A. V. Galyautdinova R. R. Gazetdinov R. R. Muslukhov G. A. Tolstikov 《Chemistry of Natural Compounds》2005,41(6):715-718
Synthetic approaches to (±)- and (3S)-analogs of the AI component of the Aonidiella aurantii sex pheromone (3S)-methyl-6R-isopropenyldec-9-en-1-ylacetate based on stepwise alkylation of acetoacetic ester by 3-butenylbromide
and 1,5-bifunctional 3-methylpentanes were investigated.
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Translated from Khimiya Prirodnykh Soedinenii, No. 6, pp. 589–591, November–December, 2005. 相似文献
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T. V. Khomova S. D. Gusakova A. I. Glushenkova R. M. Galyautdinova 《Chemistry of Natural Compounds》1995,31(1):26-28
It has been established that the wastes from the production of the drug allapinin from the epigeat pan ofAconitum leucostomum consist of nonpolar and polar lipids with a high content of phospho- and glycolipids and free fatty acids.Translated from Khimiya Prirodnykh Soedinenii, No. 1, pp. 37–40, January–February, 1995. 相似文献
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