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排序方式: 共有89条查询结果,搜索用时 468 毫秒
1.
Polyfunctional quinolines were synthesized using Friedlander method catalyzed by molecular iodine in high yields at 60 °C under solvent‐free conditions. 相似文献
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Polyvinylpolypyrrolidone-supported boron trifluoride has been studied for synthesis of 4-methyl coumarin by the Pechmann reaction. The reaction proceeded smoothly with hydroxyl phenols and ethyl acetoacetate in good yields in ethanol at reflux conditions. The polyvinylpolypyrrolidone-boron trifluoride complex is a non-corrosive and stable solid catalyst elevated Lewis acid property. 相似文献
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Jean M. J. Tronchet Françoise Barbalat-Rey Jeannine F. Tronchet Faranak Raehidzadeh 《Journal of carbohydrate chemistry》2013,32(2):193-204
Replacement of the alkyl group of l-aryl-3-alkyltriazenes with a sugar moiety did not significantly modify their tautomeric behaviour. The same replacement done on 1-aryl-3-alkyl-3-methyl-triazenes did not affect to any large extent their rotameric properties. In contrast, the most prominent biological properties, anticancer activity and toxicity, of 1-aryl-3-methyltria-zenes disappeared on replacement of the methyl group with a sugar moiety. Unexpectedly, the N-acetyltriazene 15 was highly cyto-toxic. 相似文献
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Hamed Rashidi Ali Ahmadpour Fatemeh F. Bamoharram Seyed Mojtaba Zebarjad Majid M. Heravi Faranak Tayari 《Chemical Papers》2014,68(4):516-524
ZnO nanostructures were synthesised in a hydrothermal reaction of zinc acetate in the presence of molybdophosphoric acid (H3[PMo12O40]) as well as its vanadium-substituted acid (H4[PMo11VO40]) at various times, temperatures, and concentrations. The ZnO nanostructures were characterised by X-ray diffraction, transmission electron microscopy, and Fourier transform infrared spectroscopy. The results demonstrated that the synthesised products are crystalline with a zincite hexagonal phase. Various ZnO nanostructures, such as nanoparticles, microrods, and nanosheets, were produced by changing the experimental conditions. The photocatalytic degradation of methyl orange was also investigated using the ZnO nanoparticles thus prepared. These particles exhibited high performance in the photocatalytic degradation of MO and almost 100 % decolourisation occurred within only 20 min. 相似文献
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Gutt C Ghaderi T Chamard V Madsen A Seydel T Tolan M Sprung M Grübel G Sinha SK 《Physical review letters》2003,91(7):076104
We report measurements of propagating capillary waves on a liquid water surface at T=5 degrees C with x-ray photon correlation spectroscopy. The experiment has been performed under grazing incidence conditions with an incoming x-ray beam below the critical angle of total external reflection. In the q region investigated the measured intensity-intensity autocorrelation functions of the liquid water surface were found to be heterodyne signals, i.e., a combination of first- and second-order correlation functions g(1)(tau) and g(2)(tau). 相似文献
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Microstructure of nickel nanoparticles embedded in carbon films: case study on annealing effect by micromorphology analysis 下载免费PDF全文
Ştefan Ţălu Miroslaw Bramowicz Slawomir Kulesza Azizollah Shafiekhani Maryam Rahmati Atefeh Ghaderi Mohammad Ahmadirad Shahram Solaymani 《Surface and interface analysis : SIA》2017,49(3):153-160
The presented study is aimed at analyzing the surface texture of amorphous hydrogenated carbon layers containing nickel nanoparticles (Ni‐NPs@a‐C:H) within their structure, which were deposited by Radio Frequency (RF) sputtering and RF‐Plasma Enhanced Chemical Vapor Deposition (RF‐PECVD) methods on glass substrates. Prepared films were then used as research material following their annealing at two different temperatures of 250 °C and 350 °C in an inert argon atmosphere. Series of height samples were taken with the help of atomic force microscopy (AFM) operating in a non‐contact mode and examined in order to determine their fractal characteristics. Raw AFM data were first plane‐fitted to remove the surface bow exhibiting the so‐called residual surface, and then numerically processed to calculate the Areal Autocorrelation Function (AACF), which was later used to compute the Structure Function (SF). The log–log plots of the latter served for calculation of fractal properties of surfaces under investigation, including fractal dimension D, and pseudo‐topothesy K. The analysis of 3‐D surface texture helps to understand their essential characteristics and their implications as well as graphical models and their implementation in computer simulation. Copyright © 2016 John Wiley & Sons, Ltd. 相似文献
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Applications of traditional data envelopments analysis (DEA) models require knowledge of crisp input and output data. However, the real-world problems often deal with imprecise or ambiguous data. In this paper, the problem of considering uncertainty in the equality constraints is analyzed and by using the equivalent form of CCR model, a suitable robust DEA model is derived in order to analyze the efficiency of decision-making units (DMUs) under the assumption of uncertainty in both input and output spaces. The new model based on the robust optimization approach is suggested. Using the proposed model, it is possible to evaluate the efficiency of the DMUs in the presence of uncertainty in a fewer steps compared to other models. In addition, using the new proposed robust DEA model and envelopment form of CCR model, two linear robust super-efficiency models for complete ranking of DMUs are proposed. Two different case studies of different contexts are taken as numerical examples in order to compare the proposed model with other approaches. The examples also illustrate various possible applications of new models. 相似文献
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