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CM Silva MF Duarte ML Mira MH Florêncio K Versluis AJ Heck 《Rapid communications in mass spectrometry : RCM》1999,13(12):1098-1103
Fast atom bombardment, combined with high-energy collision-induced tandem mass spectrometry, has been used to investigate gas-phase metal-ion interactions with captopril, enalaprilat and lisinopril, all angiotensin-converting enzyme inhibitors.Suggestions for the location of metal-binding sites are presented. For captopril, metal binding occurs most likely at both the sulphur and the nitrogen atom. For enalaprilat and lisinopril, binding preferably occurs at the amine nitrogen. Copyright 1999 John Wiley & Sons, Ltd. 相似文献
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E. Andrási A. Dózsa L. Bezur L. Ernyei Zs. Molnár 《Fresenius' Journal of Analytical Chemistry》1993,345(2-4):340-342
Summary In order to investigate the precision and accuracy obtainable with instrumental neutron activation analysis (INAA) and inductively coupled plasma atomic emission spectrometry (ICP-AES), five different biological reference materials were analyzed. Four of them originated from the US National Institute of Standards and Technology (NIST) (Bovine Liver (SRM 1577; 1577/a; 185/A), Orchard Leaves (SRM 1571)) and one of them came from the International Atomic Energy Agency (IAEA) (Animal muscle (H-4)). The decomposition efficiency of microwave acid digestion was examined in comparison to digestions carried out in a Parrbomb. Five to ten subsamples of each material were subjected to the two digestion procedures and the solutions were analyzed by ICP-AES. The dried samples were analyzed by INAA. Up to 16 elements (Al, B, Ca, Co, Cr, Cu, Fe, K, Mg, Mn, Na, Ni, P, Pb, S, Zn) were determined in various materials. 相似文献
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W. Möslinger F. Reiss F. Utz R. Hefelmann J. Tillmanns A. Splittgerber A. Reinsch E. Fritzmann A. W. Kaniss N. Gerber P. Wieske M. Riegel M. Siegfeld J. Adorjan H. Lührig F. Wiedmann A. Behre O. Jensen M. Henseval G. Mullie G. Benz S. Rothenfusser E. von Ernyei F. Reissu und P. Sommerfeld 《Fresenius' Journal of Analytical Chemistry》1912,51(7-8):519-527
Ohne Zusammenfassung 相似文献
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A procedure is explained to determined the amount of several pairs of diametrical loads applied to the outside boundary of
a ring when stresses at selected points of the inside or outside boundaries are known. Coefficients of influence are used,
following an approach similar to the one presented in a previous paper. Examples of application are given and the possible
increase in precision is shown when the number of points of measurements is larger than the number of loads to be determined. 相似文献