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1.
The reaction of 2-(2 pyridytcarbonyl)benzoic acid with thionyl chloride affords an unexpected product of the intramolecular acylation of the pyridine nitrogen atom, namely, 6,11-dioxo-6,11-dihydrobenzo[blquinotizinium chloride. At the same time, 2-(2-quinotylcarbonyl)benzoic acid forms the expected cyclic acid chloride, namely, 3-(2-gitinotyl)-3-chlorophthalide in this reaction. Both compounds acylate ammonia and primary amines, including those with bulky alkyl groups (tert-butyl, 1-adamantyl, and 1,1,3,3-tetramethylbutyl) with the formation of 2-R-3-hydroxy-3-(2pyridyl- or 2-quinolyl)isoindolines. The protonation of the pyridine nitrogen atom of N-(1,1,3,3-tetramethylbutyl)-2-(2pyridylcarbonyl)benzamide, obtained in the open amide form, is accompanied by the closing of the isoindotinone ring; the deprotonation is accompanied by ring opening.Riga Technical University, Riga LV-1048. Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 4, pp. 499–504, April, 1994. Original article submitted March 17, 1994. 相似文献
2.
3.
Ya. A. Éyubov 《International Applied Mechanics》1991,27(1):48-55
Azerbaidzhan Institute of Construction Engineering, Baku. Translated from Prikladnaya Mekhanika, Vol. 27, No. 1, pp. 55–64, January, 1991. 相似文献
4.
T. Grenet J. Delahaye M. Sabra F. Gay 《The European Physical Journal B - Condensed Matter and Complex Systems》2007,56(3):183-197
We present a study of non-equilibrium phenomena observed
in the electrical conductance of insulating granular aluminium thin films.
An anomalous field effect and its slow relaxation are studied in some
detail. The phenomenology is very similar to the one already observed in
indium oxide. The origin of the phenomena is discussed. In granular systems,
the present experiments can naturally be interpreted along two different
lines. One relies on a slow polarisation in the dielectric surrounding the
metallic islands. The other one relies on a purely electronic mechanism: the
formation of an electron Coulomb glass in the granular metal. More selective
experiments and/or quantitative predictions about the Coulomb glass
properties are still needed to definitely distinguish between the two
scenarios. 相似文献
5.
6.
7.
S. B. Érenburg L. N. Mazalov N. V. Bausk M. K. Drozdova 《Journal of Structural Chemistry》1994,35(4):517-522
SKα, SKβ, ClKβ, ClKβ, and PdLβ2 X-ray fluorescent and PdK EXAFS spectra were obtained for some organic solutions of dialkyl sulfide complexes with palladium
chloride. Solvent effects on the electronic and spatial structure of complexes in solution are discussed. In the benzene solution
of [PdCl22(C6H13)2S], complex molecules interact with solvent molecules along a coordinate that is perpendicular to the plane of the complex
molecule.
Institute of Inorganic Chemistry, Siberian Branch, Russian Academy of Sciences. Translated fromZhurmal Strukturnoi Khimii, Vol. 35, No. 4, pp. 105c111, July–August, 1994.
Translated by L. Smolina 相似文献
8.
A. A. Afanas'ev V. M. Katarkevich A. N. Rubinov T. Sh. Éfendiev 《Journal of Applied Spectroscopy》2002,69(5):782-787
Spatial redistribution of microparticles in a suspension on exposure to the interference laser field depending on the parameters of the particles and the field characteristics has been analyzed theoretically. Results of experimental investigations are presented that illustrate the capture of an ensemble of polymeric small spheres and also of the lymphocytes of human blood and other microparticles in a liquid in the interference radiation bands of the He–Ne laser. 相似文献
9.
F. F. Éfendiev 《Mathematical Notes》1992,51(2):204-207
Translated from Matematicheskie Zametki, Vol. 51, No. 2, pp. 139–143, February, 1992. 相似文献
10.
Institut des Hautes Études Scientifiques 《Publications Mathématiques de L'IHéS》2004,100(1):271-282
Sans résumé 相似文献