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1.
We present here a methodology for searching a robust pore size distribution (PSD) for adsorbent materials. The method is based on a combination of individual adsorption isotherms, obtained from Grand Canonical Monte Carlo simulations, a regularization procedure to invert the adsorption integral equation (Tikhonov regularization solved by singular value decomposition), and the needed experimental adsorption isotherm. The selection of several parameters from the available choices to start the procedure are discussed here: the size of the kernel (number of individual pores and number of experimental adsorption points to be included), the fulfillment of the Discrete Picard condition, and the L-curve criteria, all leading to find a reliable and robust PSD. The procedure is applied to plugged hexagonal templated silicas (PHTS), synthesized, and characterized in our laboratory. 相似文献
2.
3.
Karla J. Moreno Miroslaw Maczka Ulises Amador 《Journal of solid state chemistry》2006,179(12):3805-3813
The structural and microstructural characteristics of metastable Gd2(Ti1−yZry)2O7 powders prepared by mechanical milling have been studied by a combination of XRD and Raman spectroscopy. Irrespective of their Zr content, as-prepared powder phases present an anion-deficient fluorite-type of structure as opposed to the pyrochlore equilibrium configuration obtained for the same solid solution by other synthetic routes. These fluorites are stable versus thermal activation, at least up to temperatures of 800 °C. For the Ti-rich compositions, thermal treatments at higher temperatures facilitate the rearrangement of the cation and anion substructures and the relaxation of mechanochemically induced defects whereas for compositions with high Zr content, the fluorite crystal structure is retained even at temperatures as high as 1200 °C. Interestingly enough, transient pyrochlores showing a very unusual cation distribution were observed during the thermally induced defect-recovery process. 相似文献
4.
V. A. Sadovnichy V. V. Alexandrov E. Soto T. B. Alexandrova T. G. Astakhova R. Vega N. V. Kulikovskaya V. I. Kurilov S. S. Migunov N. E. Shulenina 《Journal of Mathematical Sciences》2007,146(3):5938-5947
A mathematical model of the system composed of two sensors, the semicircular canal and the sacculus, is suggested. The model
is described by three lines of blocks, each line of which has the following structure: a biomechanical block, a mechanoelectrical
transduction mechanism, and a block describing the hair cell ionic currents and membrane potential dynamics. The response
of this system to various stimuli (head rotation under gravity and falling) is investigated. Identification of the model parameters
was done with the experimental data obtained for the axolotl (Ambystoma tigrinum) at the Institute of Physiology, Autonomous
University of Puebla, Mexico. Comparative analysis of the semicircular canal and sacculus membrane potentials is presented.
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Translated from Fundamentalnaya i Prikladnaya Matematika, Vol. 11, No. 7, pp. 207–220, 2005. 相似文献
5.
We introduce new classes of 2-weight cyclic codes which are direct sums of 1-weight irreducible cyclic codes
相似文献
6.
Ph. Laurent M. Abgrall Ch. Jentsch P. Lemonde G. Santarelli A. Clairon I. Maksimovic S. Bize Ch. Salomon D. Blonde J.F. Vega O. Grosjean F. Picard M. Saccoccio M. Chaubet N. Ladiette L. Guillet I. Zenone Ch. Delaroche Ch. Sirmain 《Applied physics. B, Lasers and optics》2006,84(4):683-690
In this paper we describe the cold atom clock PHARAO, designed for microgravity operation. All elements of the PHARAO engineering model have been manufactured and delivered to CNES, the French space agency. We present the clock design, its main characteristics, and initial science operation. PHARAO is one of the main components of the Atomic Clock Ensemble in Space payload that is scheduled to fly on board the International Space Station in 2010. PACS 07.87.+v; 06.30.Ft; 95.55.Sh; 32.80.Pj 相似文献
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8.
Ignacio Moreno Pablo Velásquez Daniel Puerto Asticio Vargas 《Optics Communications》2006,260(1):12-18
In this work, we show a very simple birefringent filter useful to modulate a broadband light spectrum. We first show the generation of various oscillating spectra using two identical multiple-order waveplates. In particular a sinusoidal broadband spectrum with a rapid oscillation is obtained. This spectrum is amplitude modulated by adding another waveplate to the system. This waveplate has a small phase shift, and with the proper orientation generates amplitude beats on the broadband spectrum. Finally, we show how this system can be voltage controlled by means of a ferroelectric liquid crystal modulator. We experimentally demonstrate this behavior with the aid of a portable spectrophotometer, and we provide a theoretical explanation on the basis of the Jones matrix formalism. 相似文献
9.
In order to determine the energetic driving forces for surface segregation in bimetallic clusters, we use a combined approach coupling numerical simulations within an N-body interatomic potential and a lattice-gas model. This approach, which has been used successfully to study both the superficial segregation in semi-infinite alloys and the intergranular segregation, allows us to determine the relative contributions of the three elementary driving forces for the different sites of the cluster surface (vertices, edges and facets) in both dilute limits for the Cu-Ag system. We show that the segregation hierarchy based on broken-bond arguments (preferential segregation to the vertex sites, less to edge sites, and least to facet sites) is not at all universal. In particular, unusual hierarchies are predicted when the sizes of the constituents are strongly different. Furthermore, we compare the segregation driving forces for cubo-octahedral and icosahedral clusters. They are similar for the vertex sites and edge sites, whereas they differ significantly for the sites of the triangular facets. The segregation of the species with the largest atomic radius (Ag) is indeed largely enhanced in the icosahedral structure due to dilations of the orthoradial distances. 相似文献
10.
The critical limit of the eight-vertex model eigenvectors obtained by means of the generalized Bethe Ansatz is shown to give the six-vertex eigenvectors as constructed in a previous paper by two of the authors. Furthermore, an explicit mapping is established between these eigenvectors and the usual Bethe Ansatz eigenvectors of the six-vertex model. This allows one to show that the indexv labeling the eight-vertex eigenstates becomes exactly the third component of the total spin in the critical limit. 相似文献