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A. N. Yunuskhodzhaev EB. Shamuratov A. S. Batsanov S. A. Talipov 《Chemistry of Natural Compounds》1992,27(6):743-744
A single crystal of (RS)-carnitine hydrochloride has been obtained, and its crystal structure has been refined by an x-ray structural experiment.Tashkent Pharmaceutical Institute. Translated from Khimiya Prirodnykh Soedinenii, No. 6, pp. 842–844, November–December, 1991. 相似文献
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Trapped modes in acoustic waveguides 总被引:2,自引:0,他引:2
Davies EB; Parnovski L 《The Quarterly Journal of Mechanics and Applied Mathematics》1998,51(3):477-492
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Dugal-Tessier J Serin SC Castillo-Contreras EB Conrad ED Dake GR Gates DP 《Chemistry (Weinheim an der Bergstrasse, Germany)》2012,18(20):6349-6359
The design of a synthetic route to a class of enantiomerically pure phosphaalkene-oxazolines (PhAk-Ox) is presented. The condensation of a lithium silylphosphide and a ketone (the phospha-Peterson reaction) was used as the P=C bond-forming step. Attempted condensation of PhC(=O)Ox (Ox = CNOCH(iPr)CH(2)) and MesP(SiMe(3))Li gave the unusual heterocycle (MesP)(2)C(Ph)=CN-(S)-CH(iPr)CH(2)O (3). However, PhAk-Ox (S,E)-MesP=C(Ph)CMe(2)Ox (1?a) was successfully prepared by treating MesP(SiMe(3))Li with PhC(=O)CMe(2)Ox (52?%). To demonstrate the modularity and tunability of the phospha-Peterson synthesis several other phosphaalkene-oxazolines were prepared in an analogous manner to 1?a: TripP=C(Ph)CMe(2)Ox (1?b; Trip = 2,4,6-triisopropylphenyl), 2-iPrC(6)H(4)P=C(Ph)CMe(2)Ox (1?c), 2-tBuC(6)H(4)P=C(Ph)CMe(2)Ox (1?d), MesP=C(4-MeOC(6)H(4))CMe(2)Ox (1?e), MesP=C(Ph)C(CH(2))(4)Ox (1?f), and MesP=C(3,5-(CF(3))(2)C(6)H(3))C(CH(2))(4)Ox (1?g). To evaluate the PhAk-Ox compounds as prospective precursors to chiral phosphine polymers, monomer 1?a and styrene were subjected to radical-initiated copolymerization conditions to afford [{MesPC(Ph)(CMe(2)Ox)}(x){CH(2)CHPh}(y)](n) (9?a: x = 0.13n, y = 0.87n; GPC: M(w) = 7400?g mol(-1) , PDI = 1.15). 相似文献
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A. N. Yunuskhodzhaev EB. Shamuratov A. S. Batsanov S. A. Talipov 《Chemistry of Natural Compounds》1991,27(6):743-744
A single crystal of (RS)-carnitine hydrochloride has been obtained, and its crystal structure has been refined by an x-ray structural experiment. 相似文献
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