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Dennis W. Bennett Tasneem A. Siddiquee Daniel T. Haworth Shariff E. Kabir Farzana K. Camellia 《Journal of chemical crystallography》2004,34(6):343-345
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Index abstracts 相似文献2.
Camellia Panatarani 《Journal of Physics and Chemistry of Solids》2004,65(11):1843-1847
A europium doped ZnO (ZnO:Eu) particle was directly synthesized by the spray pyrolysis method. The crystal structure of samples was designated by the europium ion and the synthesis temperature. We identified the coexistence of Eu2+ and Eu3+ ions in the as prepared ZnO, which was strongly influenced by the doping concentration and the synthesis temperature. With addition of a 0.5 mol% concentration of europium ions, only the Eu2+ ion existed in particles, while both Eu2+ and Eu3+ ions existed in sample using 1 mol% or higher concentration of europium ions. Changing the wavelength of the excitation source, we also found that both the blue and red luminescence can be obtained. 相似文献
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Panatarani Camellia Lenggoro I. Wuled Okuyama Kikuo 《Journal of nanoparticle research》2003,5(1-2):47-53
LiNO3 was used as a shield in the preparation of single crystalline ZnO particles by a spray pyrolysis process in order to prevent agglomeration and enhance the crystallinity of the ZnO. LiNO3 was added to a precursor solution of zinc acetate dihydrate prior to its atomization by means of an ultrasonic transducer. Agglomerate-free particles having a mean particle size of 26 nm were successfully obtained after washing the product. X-ray diffractometry, field-emission scanning electron micrograph and transmission electron micrograph data indicate that the size and morphology of ZnO were strongly influenced by the operating temperature used and the residence time of the particle in the reactor. 相似文献
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Dennis W. Bennett Tasneem A. Siddiquee Daniel T. Haworth Shariff E. Kabir Farzana K. Camellia 《Journal of chemical crystallography》2004,34(6):353-359
The crystal and molecular structure of trans-Cr(CO)4(PPh3)2 has been determined by single crystal X-ray diffraction. The structure differs from one previously reported, packing in a different unit cell with no molecular center of symmetry. This asymmetry, coupled with the noncoplanarity of the four equatorial carbonyl ligands indicates that the structure is dominated by steric interactions. In spite of this, density functional calculations oncis-M(CO)4(PPh3)2 vs. trans-M(CO)4(PPh3)2, M = Cr, Mo, and W, predict that the gas phase cis conformer is more stable than the trans conformer for all three metals. The complex crystallizes in the triclinic space group
with lattice parameters a = 10.139(5) Å, b = 10.583(5) Å, c =17.911(5) Å, = 75.860(5)°, = 77.410(5)°, = 65.930(5)°, V =1686.3(12) Å3, Z =2. 相似文献
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Shishir Ghosh Shariff E. Kabir Farzana K. Camellia Md. Kamal Hossain Daniel T. Haworth Sergey V. Lindeman Tasneem A. Siddiquee Dennis W. Bennett 《Journal of chemical crystallography》2010,40(8):712-715
Abstract
Treatment of [Mo(CO)3(NCMe)3] with bis(diphenylphosphino)methane (dppm) and triphenylphosphine (PPh3) at 50 °C afforded mer-[Mo(CO)3(PPh3)(κ 2-dppm)] (1) in 55% yield which has been characterized by single crystal X-ray diffraction studies and spectroscopic measurements. Compound 1 crystallizes in the triclinic space group P−1 with a = 10.3449(6), b = 11.1570(6), c = 17.8961(10) ?, β = 80.8400(10)°, Z = 2 and V = 1959.8(2) ?3. 相似文献6.
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Ahmad Pourahadi Ali Farahani Saied Saeed Hosseiny Davarani Saeed Nojavan Camellia Tashakori 《Journal of separation science》2019,42(19):3126-3133
Herein, electromembrane extraction was combined with ultraviolet spectrophotometry using a customized manifold for preconcentration and simultaneous determination of morphine, codeine, and papaverine in water and human urine samples. Absorption spectra of the extracts were recorded inside the lumen of the hollow fiber using two fiber optics connected to a miniature spectrophotometer. Partial least squares regression was applied to resolve the overlapped spectra of the analytes. Performance of the model was validated by an independent test set. Central composite design was applied to optimize the extraction parameters. The optimized extraction conditions are as follows; supporting liquid membrane: 2‐nitrophenyl octyl ether containing 15% v/v bis(2‐ethylhexyl) phosphate, applied voltage: 80 V, donor pH: 3.0, acceptor pH: 1.0, extraction time: 20 min. Finally, the optimized extraction method was validated for determination of the mentioned alkaloids in human urine samples. The method showed good linearity (R2 > 0.995) for all of the mentioned alkaloids. The limits of detection for morphine, codeine, and papaverine in diluted human urine were found to be 0.6, 1.1, and 0.6 ng/mL, respectively with acceptable relative standard deviations. Enrichment factors of 104, 108, and 102 were achieved for morphine, codeine, and papaverine, respectively. 相似文献
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Shima Majidansari Negin Vahedi Mahmood Rekabgardan Camellia Ganjoury Najmeh Najmoddin Mohammad Tabatabaei Faraz Sigaroodi Paniz Naraghi-Bagherpour Seyed Amir Ali Taheri Mohammad-Mehdi Khani 《先进技术聚合物》2023,34(2):740-747
Cardiovascular diseases have always been one of the main causes of death worldwide and eventually one of the major medical concerns. Tissue engineering is promising strategies of treating cardiovascular, which can be an effective approach with the design of appropriate scaffold. In this study, to develop engineering basement membrane for endothelial differentiation with good cell attachment, we produced polycaprolactone (PCL)/poly (glycerol sebacate) (PGS)/gelatin nanofibrous scaffold via electrospinning. Attenuated total reflectance-Fourier transform infrared and the proton nuclear magnetic resonance results confirmed the chemical structure of synthesized PGS. Scanning electron microscope images of the electrospun scaffold revealed that the nanofibers are smooth, continues and uniform. Moreover, due to the presence of hydrophilic functional groups in the scaffold, the contact angle is in the appropriate range for cell adhesion especially endothelial cells. The elastic modulus and ultimate tensile stress of electrospun scaffold were calculated 1.32 ± 0.27 MPa and 1.23 ± 0.18 MPa respectively. Quantitative polymerase chain reaction was performed for evaluation of endothelial differentiation of mesenchymal stem cells cultured on standard plate and fibrous scaffold under chemical stimulation with growth factor. Specific endothelial gene expression results postulated that our modified scaffold could support and significantly promote endothelial differentiation of MSCs. 相似文献
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