乳糖修饰壳聚糖微载体的制备及对培养肝细胞代谢活性的影响

液体石蜡作分散介质。戊二醛作交联刑，通过反相悬浮聚合制备了微米级的壳聚糖微载体．环氧氟丙烷活化后，乳糖进行修饰．用孔糖修饰的微载体进行原代大鼠肝细胞培养，利用相差显微镜对培养细胞进行形态观察，并测定肝细胞的代谢活性，结果显示，乳糖修饰壳聚糖微载体是一种优良的肝细胞培养支架．     

Annealing effect on soft magnetic properties and magnetoimpedance of Finemet Fe73.5Si13.5B9Nb3Au1 alloy

Effect of annealing on the soft magnetic properties of Fe_73.5Si_13.5B₉Nb₃Au₁ amorphous ribbon has been investigated by means of structure examination, magnetoimpedance ratio (MIR) and incremental permeability ratio (PR) spectra measured in the frequency range of 1–10 MHz at a fixed current of 10 mA X-ray diffraction analysis showed that the as-cast sample was amorphous and it became nanocrystalline under a proper heat treatment. When annealing amorphous alloy at 530 °C for 30, 60, 90 min, soft magnetic properties have been improved drastically. Among the samples investigated, the sample annealed at 530 °C for 90 min showed the softest magnetic behavior. The MIR and PR curves revealed the desirable changes in anisotropy field depending upon annealing.     

Convergence estimates of Galerkin-wavelet solutions to a Cauchy problem for a class of periodic pseudodifferential equations

A class of Cauchy problems for interesting complicated periodic pseudodifferential equations is considered. By the Galerkin-wavelet method and with weak solutions one can find sufficient conditions to establish convergence estimates of weak Galerkin-wavelet solutions to a Cauchy problem for this class of equations.

     

利用模式的对称性研究光子晶体光纤的色散

由光子晶体光纤的对称性可以得到模式分布的对称性，根据模式的对称性选择适当的展开函数，可以使计算量大大减少。计算了六角结构光子晶体光纤的色散特性，得到了波长在1．55pm处色散为零时，光子晶体光纤的结构参量所满足的方程。     

Improved search for $B_{s}^{0} - \overline{B}_{s}^{0}$ oscillations

An improved search for B _s ⁰ oscillations is performed in the ALEPH data sample collected during the first phase of LEP, and reprocessed in 1998. Three analyses based on complementary event selections are presented. First, decays of B _s ⁰ mesons into hadronic flavour eigenstates are fully reconstructed. This selection yields a small sample of candidates with excellent decay length and momentum resolution and hi gh average B _s ⁰ purity. Semileptonic decays with a reconstructed D _s ^- meson provide a second sample with larger statistics, high average B _s ⁰ purity, but a poorer momentum and decay length resolution due to the partial decay reconstruction. Finally, semileptonic b-hadron decays are inclusively selected and yield the data sample with the highest sensitivity to B _s ⁰ oscillations, as the much higher statistics compensate for the low average B _s ⁰ purity and poorer time resolution. A lower limit is set atps^-1 at 95% C.L., significantly lower than the expected limit of 15.2 ps^-1. Received: 21 February 2003 / Published online: 11 June 2003     

Lattice QCD: The case of parton densities

The accuracy of structure functions computations on the lattice may become comparable to experimental determinations. We discuss the strategy followed by the Ze-Ro Collaboration that allows the reconstruction of the running of the leading-twist non-singlet operator in the continuum and fully non-perturbatively renormalized.Received: 1 November 2002, Published online: 15 July 2003PACS: 11.15.Ha Lattice gauge theory - 12.38.Gc Lattice QCD calculations     

Measurement of the neutron electric form factor via recoil polarimetry

The ratio G _e ⁿ /G _m ⁿ of the electric to the magnetic form factor of the neutron has been measured by analyzing the polarization of the recoiling neutron in quasi-elastic scattering of longitudinally polarized electrons from deuterium at the Q ² values of 0.45, 1.15, and 1.47 (GeV/c)². The experiment has been performed in Hall C of the Thomas Jefferson National Accelerator Facility. With G _m ⁿ being known G _e ⁿ can be deduced. The preliminary results show that the lowest Q ² points follow the Galster parametrization and that the 1.47 (GeV/c)² point rises above this parametrization.Received: 30 September 2002, Published online: 22 October 2003PACS: 13.40.Gp Electromagnetic form factors - 14.20.Dh Protons and neutrons - 24.70. + s Polarization phenomena in reactions     

Structure and catalytic activity of some soluble polyethylene glycol-peptide conjugates

Soluble catalysts for the Juliá-Colonna asymmetric epoxidation reaction have been constructed in three different ways, using NH₂-PEG-OMe as the support system: suitable solvents have been identified and it is shown that the degree of helicity of the conjugates correlates with the extent of conversion and (to a lesser extent) the enantioselectivity of epoxidation.     

Synthesis and characterization of norbornene–ethylene–styrene terpolymers with a substituted ansa‐fluorenylamidodimethyltitanium‐based catalyst

This article reports a synthetic method for a norbornene–ethylene–styrene (N‐E‐S) terpolymer, which has not been well investigated so far, via incorporation of styrene (S) into vinyl‐type norbornene–ethylene (N‐E) copolymers catalyzed by a substituted ansa‐fluorenylamidodimethyltitanium [Me₂Si(3,6‐tBu₂Flu)(tBuN)]TiMe₂ catalyst ( I ) activated with a [Ph₃C][B(C₆F₅)₄]/Al(iBu)₃ cocatalyst at room temperature in toluene. The resulting terpolymerization product contained the targeted N‐E‐S terpolymer and the contaminated homopolymers, which were then able to be completely removed by solvent fractionation techniques. While homopolystyrene was easily extracted by fractionation with methylethylketone as a soluble part, homopolyethylene and a trace amount of homopolynorbornene could be perfectly separated by fractionation with chloroform as insoluble parts. The detail characterizations of a chloroform‐soluble polymer with gel permeation chromatography, nuclear magnetic resonance, and differential scanning calorimetry analyses proved that it contained a true N‐E‐S terpolymer with long N‐E sequences incorporated with isolated or short styrene sequences. The homogeneity of the morphology together with a single glass transition temperature that proportionally decreased with the increase of the styrene contents indicated that the N‐E‐S terpolymer obtained in this work is a random polymer with an amorphous structure. © 2007 Wiley Periodicals, Inc. J Polym Sci Part A: Polym Chem 45: 2765–2773, 2007