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1.
Room temperature transmission Mössbauer spectra of Fe62Ni16B14Si8 ribbons, annealed in vacuum for time periods ranging from 5 to 60 minutes at the crystallization temperatureT
x=720 K, have been used to investigate the crystallization mechanism by isothermal annealing. Reorientation of the magnetic anisotropy almost normal to the ribbon plane was observed and correlated to the annealing time dependence of the mean hyperfine field (HF) of the amorphous component. Crystallization started at the surface before the bulk and was found to occur in two steps: a metastable equilibrium of the amorphous phase with (FeNi), (FeNi)Si and t-(FeNi)3B, followed by the decomposition of t-(FeNi)3B into t-(FeNi)2B and (FeNi). The increase of the mean magnetic moment at the Fe sites as compared to related iron-based alloys was attributed to compositional small Ni additions. 相似文献
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Lee CJ Liang X Chen X Zeng D Joo SH Chung HS Barb AW Swanson SM Nicholas RA Li Y Toone EJ Raetz CR Zhou P 《Chemistry & biology》2011,18(1):38-47
LpxC is an essential enzyme in the lipid A biosynthetic pathway in gram-negative bacteria. Several promising antimicrobial lead compounds targeting LpxC have been reported, though they typically display a large variation in potency against different gram-negative pathogens. We report that inhibitors with a diacetylene scaffold effectively overcome the resistance caused by sequence variation in the LpxC substrate-binding passage. Compound binding is captured in complex with representative LpxC orthologs, and structural analysis reveals large conformational differences that mostly reflect inherent molecular features of distinct LpxC orthologs, whereas ligand-induced structural adaptations occur at a smaller scale. These observations highlight the need for a molecular understanding of inherent structural features and conformational plasticity of LpxC enzymes for optimizing LpxC inhibitors as broad-spectrum antibiotics against gram-negative infections. 相似文献
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R.-A. Barb C. Hrelescu L. Dong J. Heitz J. Siegel P. Slepicka V. Vosmanska V. Svorcik B. Magnus R. Marksteiner M. Schernthaner K. Groschner 《Applied Physics A: Materials Science & Processing》2014,117(1):295-300
Frequently observed coherent structures in laser-surface processing are ripples, also denoted as laser-induced periodic surface structures (LIPSS). For polyethylene terephthalate (PET) and polystyrene (PS), LIPSS can be induced by irradiation with linearly polarized ns-pulsed UV laser light. Under an angle of incidence of θ, their lateral period is close to the laser wavelength λ divided by (n eff ? sinθ). Here, n eff is the effective refractive index which is 1.32 and 1.23 for PET and PS, respectively. We describe potential applications of LIPSS for alignment and activation of human cells cultivated on polymer substrates, as well as for formation of separated gold nanowires which show pronounced surface plasmon resonances, e.g., at 775 nm for PET. 相似文献
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Magnetic phase transitions in disordered crystalline iron germanates of the type Sr2LnFe3Ge3O14 (Ln=La; Nd) were observed at low temperatures by means of57Fe Mössbauer spectroscopy. The hyperfine interaction of Fe3+ magnetic moments ordered in one octahedral and two tetrahedral magnetic sublattices is discussed. A local environment computation on the octahedral sites confirms the assumption that the wide distribution found for the 4.2 K octahedral hyperfine fields is due to the random occupation by Fe3+ and Ge4+ ions of the nearest cation environment of the octahedral iron. The effect of substituting Ln rare earth ions in the Thompson cubes on the magnetic behaviour of these compounds is pointed out. 相似文献
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The effects of high-energy electron beam and pulsed excimer laser irradiation on the magnetic properties of Fe80B20 amorphous alloy are investigated by means of transmission and conversion electron Mössbauer spectroscopy (CEMS) and scanning electron microscopy (SEM). Both types of irradiation were found to induce changes in the magnetic anisotropy of Fe80B20, but the influence of high-energy electron beam irradiation was weaker. Depending on the number of applied laser pulses and repetition rate, controlled magnetic anisotropy and/or relaxation of internal stresses could be obtained by excimer laser irradiation. The presence of molten zones subsequently solidified and of laser-induced internal stresses supports the model of closúre domain structure. 相似文献