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排序方式: 共有45条查询结果,搜索用时 15 毫秒
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SOLIMAN A.Y. BAKEER H.M. ATTIA LA.Science Department Faculty of Teachers P.O.Box Alhasa Saudi Arabia Chemistry Department Faculty of Science Fayoum Cairo University EgyptFaculty of Engineering Ain Shames University Egypt 《中国化学》1996,14(6):532-540
3-(4-Phenyl) benzoyl propionic acid was used as the starting material for the synthesisof furanones (2), pyrrolinones (5), pyridazinones (7), benzoxazinones (8) and quinazolinones (9-11). The behaviour of the derivatives of furanones and benzoxazinones toward different nucleophiles is reported. 相似文献
3.
MENG Jian REN Yu-Fang LI Xiao-GuangLaboratory of Rare Earth Chemistry Physics Changchun Institute of Applied Chemistry Chinese Academy of Sciences Changchun Jilin ChinaPopov V.V. Repin S.M. Smirnov LA. loffe Physicotechnical Institute Russian Academy of Sciences Saint Petersburg Russia 《中国化学》1994,12(5):419-424
YBa2Cu3-xVxO7-y(x=0, 0.1, 0.2, 0.3, 0.4, 0.5 and 0.6) superconductors have been prepared. X-ray diffraction shows that the system remains orthorhombic for all compositions studied, but for x > 0.4 V2O5 was detected as an impurity phase. Substitution of V5+ for Cu2+ occurs in the Cu(2) sites on the Cu(2)-O planes. The introduction of the high valence element, vanadium, produces the extra free-electrons. These electrons recombine with the positive carrier of the system. It makes depression of the mobility and the Hall number of YBa2Cu3-xVxO7-v and also results in a depression of TC. 相似文献
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MARIAN ELBANOWSKI MARIA PAETZ JANUSZ SIAWINSKI LESZEK CIELA 《Photochemistry and photobiology》1988,47(3):463-466
Abstract— Chemiluminescence of the Eu(II)/Eu(III)-adenine nucleotide-H2 O2 system and fluorescence of the Eu(III)-adenosine triphosphate system have been investigated. The spectral distribution of the chemiluminescence emission has shown an occurrence of three main bands (Λ=470–480,590–620 and ca. 700 nm). The energy transfer process from the adenosine triphosphate molecules to the Eu(III) ions has been observed in the fluorescence spectrum. The examined chemiluminescence and fluorescence spectra show that these both kinds of emission originate from the 5 D *** τ7 F*** ( n =1–4) transitions in the Eu(III) ions. 相似文献
5.
针对纤维材料变温环境力学性能测试的需要,在华中科技大学研制的纤维材料试验机的基础上引入了温控装置,从而实现纤维材料在高低温环境下的力学性能测试。采用该装置对不同直径微米铜丝在不同温度、不同拉伸速率条件下的力学性能开展实验研究,测试结果表明弹性模量和抗拉强度随温度的降低而线性增加,屈服强度的变化不太明显。另外,低温环境下微米铜丝的力学性能表现出与其直径相关的尺度效应,而这一现象在常温下一直没有观测到。最后,还研究了拉伸速率对微米铜丝的力学性能影响,结果表明,在现有装置的许用范围之内,拉伸速率对其力学性能的影响不大。 相似文献
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This paper deals with robustness of adaptive control of continuoussystems subject to known output delay, input saturation, unmodelledlinear dynamics, and bounded disturbances. A simple gradient-typealgorithm with a relative deadzone is used. The relative deadzoneis built with an estimated contribution of the unmodelled dynamicsto the system output. The basic tool used for stability androbustness analysis is Gronwall's lemma. 相似文献
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电感耦合等离子体-发射光谱法(ICP-AES)快速测定饮用水中8种微量元素 总被引:4,自引:0,他引:4
用电感耦合等离子体-发射光谱法(ICP-AES)同时快速测定饮用水中微量的铜、铅、锌、铁、锰、镉、铬、砷,具有快速、简便、灵敏度高等优点,精密度为1.2%~8.2%(RSD,n=5).回收率为90%~110%. 相似文献
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乙酸铵离心交换法测定酸性和中性土壤阳离子交换量是经典方法,但此方法的蒸馏过程繁琐、时间长、效率低。本文引用纳氏试剂分光光度法测定土壤CEC值,并将结果与乙酸铵离心法常用的几种传统测定方法进行了实验对比和总结。通过对国家标准样品及实际土壤样品的CEC值测定,纳氏试剂比色法的精密度在2-4%之间,准确度与经典方法一致。与传统滴定法比较,取代了蒸馏的步骤,测定方法简单,干扰少,结果可靠,可操作性强。 相似文献
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Coastal erosion, accelerated by sea level rise, and subsidence are major Louisiana issues. With current sea-level-rise projections, coupled with the state's eroding barrier islands and coastal wetlands, the region's estuarine environments are in jeopardy of being lost, redefined, or permanently altered. As the coast erodes, Louisiana is endangered of losing valuable wetland's habitat. In addition, if the barrier islands disappear, the region's wetland-oriented oil and gas wells and associated infrastructure will be at risk to open Gulf conditions. If this should occur, each well, pipeline, and storage battery represents a potential environmental catastrophe. 相似文献
10.
CHEN Hong-jie LI Sheng LI Zhi-wei WU Zhi-shen ZHANG Ping-yu ZHANG Zhi-jun 《高等学校化学研究》2005,21(6):646-649
IntroductionMetal or alloy nanoparticles,because of their con-spicuous physicochemical properties,have been widelyapplied to various fields such as electronics,catalysis,magnetism,and corrosion-resistant materialsfields[1—4].It has been estimated that the particle sizeand the properties of nanoparticles depend strongly onthe specific method of fabrication and the applied ex-periment conditions,which makes the controlled syn-thesis of nanomaterials become an increasingly activeand important ar… 相似文献