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1.
We investigate magnetic and crystalline microstructures of melt-spun (Fe0.675Pt0.325)100-xBx (x=12, 14, 16, 18,20) nanocomposite ribbons after optimal thermal treatment using a magnetic force microscope. The magnetic microstructures are characterized by darker spots adjacent to brighter ones in a sub-micro scale and in random distribution. It is found that the strength of the exchange coupling interaction between the crystals in the 10-100 nm scale, implied by the maximum value (δM)max of the Henkel plot, could be roughly described by the ratio of the average width of the magnetic spots w^- to the average crystal size D^- for the ribbons. Moreover, we find that the intrinsic coercivity jHc of the ribbons is sensitive to their crystal sizes, and the smaller D^-, the higher jHc. Finally, by using roughness analysis, the curve of the root mean square values (δФ)rms of the phase shift of the magnetic force images versus the boron content x is obtained, which is qualitatively consistent with that of the magnetization σ12 kOe of the ribbons versus x. 相似文献
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HDDR过程中三元和多元Nd-Fe-B合金磁畴结构的MFM研究 总被引:1,自引:1,他引:1
用磁力显微镜研究了三元Nd-Fe-B合金在HDDR过程的不同阶段(铸态、不充分吸氢歧化、充分吸氢歧化和脱氢再复合)的破畴结构。在铸态样品表面清楚地观察到了易磁化轴互相垂直的柱状晶表面的两类磁畴图型。当样品不充分吸氢歧化和充分吸氢歧化时,破畴结构明显发生变化,反映了Nd-Fe-B的分解产物NdH2,α-Fe和Fe2B及其微晶结构的变化。脱氢再复合后形成的微晶的磁畴结构则表明样品保留了铸态样品柱状晶的构型。此外,还对比研究了多元Nd-Fe-B合金在HDDR过程中的磁畴结构,并根据微磁结构分析,指出过量的Ga元素添加可抑制Nd2(Fe,M)14B相的吸氢歧化,从而导致相应HDDR粘结磁体性能降低。 相似文献
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Magnetic domain structures of precipitation-hardened SmCo 2:17-type sintered magnets: Heat treatment effect 下载免费PDF全文
The typical magnetic domains of Sm(CObalFe0.25Cuo.07Zr0.02)7.4 magnets quenched through various heattreatment steps have been revealed by using magnetic force microscopy (MFM). For the specimens in which the nominal c-axis is perpendicular to the imaging plane, the domain configurations change from plate-like for the as-sintered magnet to corrugation and spike-like for the homogenized one, and then to a coarse and finally to a finer domain structure when isothermally aged at 830℃ and then annealed at 400℃. However, only plate-like domains can be detected on the surfaces with the nominal c-axis parallel to the imaging plane. The finer domain (so-called interaction domain) is a characteristic magnetic domain pattern of the SmCo 2:IT-type magnets with high coercivities. Domain walls in a zigzag shape are revealed by means of MFM in final bulk SraCo 2:17-type sintered magnets. 相似文献
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An investigation of phase separation by magnetic force microscopy in La0.45Sr0.55MnO3-δ(δ≈0.01) 下载免费PDF全文
We have found phase separation in La0.45Sr0.55MnO3-δ (LSMO) by means of electron spin resonance, magnetic force microscopy (MFM) and magnetic measurements. Ferromagnetic and antiferromagnetic phases can coexist at low temperatures, and ferromagnetic and paramagnetic phases coexist when the temperature lies between the Néel and Curie temperatures. The size and shape of the ferromagnetic phases (the minority phases) was first observed directly from MFM images. It is suggested that the phase separation in LSMO is not the charge segregation type, but an electroneutral type due perhaps to the nonuniform distribution of oxygen vacancies. 相似文献
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前 言 磁泡技术于1969年问世.由于磁泡存贮器有单片容量大,存贮密度高,体积小,可靠性高,信息存贮的非易失性以及速度超过机械磁存贮器(如磁盘、磁鼓等)等显著的特点,所以九年来发展迅速,成为一种大有希望的新型存贮器. 畴壁运动矫顽力Hc,即畴壁开始移动所需的磁场,是磁泡材料最重要的特性参数之一.磁泡的运动实质上就是围绕磁泡的畴壁的运动.磁泡动力学告诉我们,Hc的大小决定着使磁泡开始运动所需外加驱动磁场的大小.可见,对于磁泡材料,Hc越小越好.降低Hc是磁泡材料研究中的一个重要课题. 测量畴壁运动矫顽力的方法有几种.在磁泡技术发展… 相似文献
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