化学气相沉积法制备金刚石膜截面微区Raman分析

采用微区Raman散射分析方法研究化学气相沉积法制备的金刚石膜的横截面.金刚石膜从衬底面到生长面不同位置具有不同特征的Raman谱,依此对膜中的金刚石、石墨和非晶碳成分进行分析.衬底面附近区域对应金刚石膜生长过程的成核阶段,非晶碳成分含量较高,相应于1200—1600cm^-1波段较大的散射强度和存在较强的荧光背底.膜厚增大,非晶碳成分中sp³结构成分首先减少,而sp²结构成分和石墨成分的减少相对缓慢.而生长面附近区域只有比较单纯的晶体金刚石 关键词：     

High-Pressure Single-Crystal Neutron Scattering Study of Magnetic and Fe Vacancy Orders in （T1,Rb）：Fe4Se5 Superconductor

The recently discovered metal-intercalated iron selenide superconductors A2Fe4Se5 （A=K, Cs, T1- K, Rb, T1-Rb） （245） compounds, with Tc ～30K, have attracted much interest A high transition- temperature （TN ≈ 470-560K） and large magnetic moment （3.3μB/Fe） block antiferromagnetic （AFM） order exists in the superconducting samples. Mag- netic order-parameter experiences an anomaly when Tc is approached. The superconductors crystal- lize with a highly ordered √5 × √5 superstructure, in which the Fel site of the I4/m structure is only a few percents occupied and the Fe2 site is fully occupied. The non-superconducting samples at low-T also crystallize in the I4/m structure, while both Fe sites are fractionally occupied, since the numbers of the Fe vacancies in the samples and the vacant sites in the √5 × √5 pattern are mismatched. The partially ordered √5× √5 vacancy order becomes one of three competing phases for temperature below room temperature up to ～ 500K, namely, these sam- ples are phase-separated and in the miscibility gap 1lacier the n,mhi~nt condition.     

重离子加速器冷却储存环高频腔体设计

 通过二维高频电磁场的计算，设计了兰州重离子加速器冷却储存环（HIRFL–CSR）的铁氧体加载腔，给出了高频系统主要参数及加速电场的分布。     

金刚石薄膜的蓝光发射

利用氮化铝陶瓷作为衬底，在不同甲烷与氢气的配比流量下，利用热丝ＣＶＤ方法制备了一个系列的金刚石薄膜，通过测量样品在４３０ｎｍ处的光致荧光（ＰＬ）谱及其Ｒａｍａｎ光谱，给出了金刚石薄膜的结构与生长信息，薄膜ＰＬ强度随甲烷浓度增加到３％时达到最大，继续增加了甲烷浓度ＰＬ强度下降。     

Recalculation of the HIRFL-SSC injection and extraction system

In order to further improve beam transmission efficiency at the SSC, the beam center trajectory and injection and extraction system are recalculated based on the program group used in the final design of the GANIL accelerator, with some necessary changes and the addition of some auxiliary programs. The two different types of injection and extraction elements (the bending magnet and the inductive septum) are distinguished, and their interaction with the ambient field is considered. More focus is placed on considering the differences in the magnet field inhomogeneity of the ambient field in the located area of the inductive septum where the ends are situated in the ambient field (between the main magnet poles). Thus the gradient magnetic field problem of the inductive septum is solved perfectly. As well as preparing the necessary auxiliary programs and taking the structural integration of the SSC magnetic field maps, the measured magnet field correction is completed. Therefore, the trajectory and a variety of injection and extraction system parameters are obtained. According to the recalculation results, the SSC beam transmission efficiency will be enhanced significantly.     

Beam transmission efficiency of the HIRFL-SSC

In this paper we address the problem of the low beam transmission efficiency of the HIRFL-SSC. The influence of the SFC-SSC energy match, the SSC RF voltage, and harmonic field in the injection area of the SSC, and the SSC central trajectory on the beam transmission efficiency have been analyzed both from the theoretical side and from the actual operating data. The main reason is that the soft-edge approximation of the magnet field (the so-called theoretical field) and the simplified calculation programs were adopted when calculating the beam center trajectory and designing the injection and extraction system, and the measured magnetic field was not used to correct the calculation results. These led to large deviations of the calculated center trajectory, and then resulted in low efficiency of the SSC beam transmission. Therefore, the re-calculation of SSC beam center trajectory and injection and extraction system, as well as the measured magnet field correction are the key points required to solve the problem.     

油炸圈饼状Cd(OH)2微结构的合成与可控生长机理

聚丙烯酰胺（PAM）表面活性剂的作用下,在温和的低温水溶液中,合成了Cd(OH)2油炸圈饼状微米结构。这种结构是由单晶结构的六方片状Cd(OH)2按一定排列方式自组装而成。在羰基修饰的PAM（PAM-COOH）表面活性剂作用下,得到中心有孔的油炸圈饼纳米结构。可能的生长机理为表面活性剂控制下Cd(OH)2纳米片经历有序连接过程,最终形成油炸圈饼状结构。聚合物诱引晶体生长与调控纳米晶自组装将提供了一条有效的路径来合成具有复杂形貌与特殊结构的无机和无机-有机杂化材料。     

Nonparaxial propagation properties of the chirped Airy Gaussian vortex beams in uniaxial crystals orthogonal to the optical axis

In this article, we investigate the nonparaxial propagation properties of the chirped Airy Gaussian vortex(CAiGV)beams in uniaxial crystals orthogonal to the optical axis analytically and numerically. We discuss how the linear chirp parameters, the quadratic chirp parameters, and the Gaussian factors influence the nonparaxial propagation dynamics of the CAiGV beams. The intensity, the energy flow, the beam center, and the angular momentum of the CAiGV beams are deeply investigated. It is shown that the Gaussian factors have a great effect on the intensity and the centroid positions of the CAiGV beams. With the Gaussian factors increasing, the intensity of CAiGV beams decreases rapidly. The main lobes of the transverse intensity distribution of the CAiGV beams are similar to triangles.     

聚类分析橡胶炭黑填充量与Yeoh模型参数的关联

为了探索橡胶炭黑填充量和Yeoh模型参数的关联,提出一种利用聚类分析对不同填充量参数的分类方法.本方法基于三参数Yeoh模型拟合炭黑填充橡胶的单轴拉伸应力应变曲线,从而得到3个准确描述力学性能的参数C10、C20和C30.利用聚类的方法对参数进行无监督分类,聚类数设置为3～8,以探究不同类别对结果的影响.结果表明,所有...     

"京亚"葡萄种子萌发特性及其卡那霉素抗性的研究

探讨了不同消毒条件下"京亚"葡萄种子在培养瓶中萌发的情况,获得"京亚"葡萄种子最佳消毒条件是70%乙醇15 S,o.1%升汞5 min;通过对"京亚"葡萄种子进行不同浓度GA3 浸种、不同浸种时间、不同培养基质和不同光照条件处理,得到优化的"京亚"葡萄种子萌发条件是GA34 000 mg/L浸种48 h,置于1/2MS培养基中暗光培养,萌发率为79.4%;对"京亚"葡萄种子抗卡那霉察特性的研究得到"京亚"种子抗卡那霉紊的临界浓度为40 mg/L.